CA2103770A1 - Plasma-Enhanced Magnetron-Sputtered Deposition of Materials - Google Patents
Plasma-Enhanced Magnetron-Sputtered Deposition of MaterialsInfo
- Publication number
- CA2103770A1 CA2103770A1 CA2103770A CA2103770A CA2103770A1 CA 2103770 A1 CA2103770 A1 CA 2103770A1 CA 2103770 A CA2103770 A CA 2103770A CA 2103770 A CA2103770 A CA 2103770A CA 2103770 A1 CA2103770 A1 CA 2103770A1
- Authority
- CA
- Canada
- Prior art keywords
- plasma
- deposition
- metal
- substrate
- gas
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Granted
Links
Classifications
-
- H—ELECTRICITY
- H01—ELECTRIC ELEMENTS
- H01J—ELECTRIC DISCHARGE TUBES OR DISCHARGE LAMPS
- H01J37/00—Discharge tubes with provision for introducing objects or material to be exposed to the discharge, e.g. for the purpose of examination or processing thereof
- H01J37/32—Gas-filled discharge tubes
- H01J37/32431—Constructional details of the reactor
- H01J37/32697—Electrostatic control
- H01J37/32706—Polarising the substrate
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- C—CHEMISTRY; METALLURGY
- C23—COATING METALLIC MATERIAL; COATING MATERIAL WITH METALLIC MATERIAL; CHEMICAL SURFACE TREATMENT; DIFFUSION TREATMENT OF METALLIC MATERIAL; COATING BY VACUUM EVAPORATION, BY SPUTTERING, BY ION IMPLANTATION OR BY CHEMICAL VAPOUR DEPOSITION, IN GENERAL; INHIBITING CORROSION OF METALLIC MATERIAL OR INCRUSTATION IN GENERAL
- C23C—COATING METALLIC MATERIAL; COATING MATERIAL WITH METALLIC MATERIAL; SURFACE TREATMENT OF METALLIC MATERIAL BY DIFFUSION INTO THE SURFACE, BY CHEMICAL CONVERSION OR SUBSTITUTION; COATING BY VACUUM EVAPORATION, BY SPUTTERING, BY ION IMPLANTATION OR BY CHEMICAL VAPOUR DEPOSITION, IN GENERAL
- C23C14/00—Coating by vacuum evaporation, by sputtering or by ion implantation of the coating forming material
- C23C14/0021—Reactive sputtering or evaporation
- C23C14/0036—Reactive sputtering
-
- C—CHEMISTRY; METALLURGY
- C23—COATING METALLIC MATERIAL; COATING MATERIAL WITH METALLIC MATERIAL; CHEMICAL SURFACE TREATMENT; DIFFUSION TREATMENT OF METALLIC MATERIAL; COATING BY VACUUM EVAPORATION, BY SPUTTERING, BY ION IMPLANTATION OR BY CHEMICAL VAPOUR DEPOSITION, IN GENERAL; INHIBITING CORROSION OF METALLIC MATERIAL OR INCRUSTATION IN GENERAL
- C23C—COATING METALLIC MATERIAL; COATING MATERIAL WITH METALLIC MATERIAL; SURFACE TREATMENT OF METALLIC MATERIAL BY DIFFUSION INTO THE SURFACE, BY CHEMICAL CONVERSION OR SUBSTITUTION; COATING BY VACUUM EVAPORATION, BY SPUTTERING, BY ION IMPLANTATION OR BY CHEMICAL VAPOUR DEPOSITION, IN GENERAL
- C23C14/00—Coating by vacuum evaporation, by sputtering or by ion implantation of the coating forming material
- C23C14/06—Coating by vacuum evaporation, by sputtering or by ion implantation of the coating forming material characterised by the coating material
- C23C14/0635—Carbides
-
- C—CHEMISTRY; METALLURGY
- C23—COATING METALLIC MATERIAL; COATING MATERIAL WITH METALLIC MATERIAL; CHEMICAL SURFACE TREATMENT; DIFFUSION TREATMENT OF METALLIC MATERIAL; COATING BY VACUUM EVAPORATION, BY SPUTTERING, BY ION IMPLANTATION OR BY CHEMICAL VAPOUR DEPOSITION, IN GENERAL; INHIBITING CORROSION OF METALLIC MATERIAL OR INCRUSTATION IN GENERAL
- C23C—COATING METALLIC MATERIAL; COATING MATERIAL WITH METALLIC MATERIAL; SURFACE TREATMENT OF METALLIC MATERIAL BY DIFFUSION INTO THE SURFACE, BY CHEMICAL CONVERSION OR SUBSTITUTION; COATING BY VACUUM EVAPORATION, BY SPUTTERING, BY ION IMPLANTATION OR BY CHEMICAL VAPOUR DEPOSITION, IN GENERAL
- C23C14/00—Coating by vacuum evaporation, by sputtering or by ion implantation of the coating forming material
- C23C14/06—Coating by vacuum evaporation, by sputtering or by ion implantation of the coating forming material characterised by the coating material
- C23C14/0641—Nitrides
-
- C—CHEMISTRY; METALLURGY
- C23—COATING METALLIC MATERIAL; COATING MATERIAL WITH METALLIC MATERIAL; CHEMICAL SURFACE TREATMENT; DIFFUSION TREATMENT OF METALLIC MATERIAL; COATING BY VACUUM EVAPORATION, BY SPUTTERING, BY ION IMPLANTATION OR BY CHEMICAL VAPOUR DEPOSITION, IN GENERAL; INHIBITING CORROSION OF METALLIC MATERIAL OR INCRUSTATION IN GENERAL
- C23C—COATING METALLIC MATERIAL; COATING MATERIAL WITH METALLIC MATERIAL; SURFACE TREATMENT OF METALLIC MATERIAL BY DIFFUSION INTO THE SURFACE, BY CHEMICAL CONVERSION OR SUBSTITUTION; COATING BY VACUUM EVAPORATION, BY SPUTTERING, BY ION IMPLANTATION OR BY CHEMICAL VAPOUR DEPOSITION, IN GENERAL
- C23C14/00—Coating by vacuum evaporation, by sputtering or by ion implantation of the coating forming material
- C23C14/22—Coating by vacuum evaporation, by sputtering or by ion implantation of the coating forming material characterised by the process of coating
- C23C14/24—Vacuum evaporation
- C23C14/32—Vacuum evaporation by explosion; by evaporation and subsequent ionisation of the vapours, e.g. ion-plating
-
- C—CHEMISTRY; METALLURGY
- C23—COATING METALLIC MATERIAL; COATING MATERIAL WITH METALLIC MATERIAL; CHEMICAL SURFACE TREATMENT; DIFFUSION TREATMENT OF METALLIC MATERIAL; COATING BY VACUUM EVAPORATION, BY SPUTTERING, BY ION IMPLANTATION OR BY CHEMICAL VAPOUR DEPOSITION, IN GENERAL; INHIBITING CORROSION OF METALLIC MATERIAL OR INCRUSTATION IN GENERAL
- C23C—COATING METALLIC MATERIAL; COATING MATERIAL WITH METALLIC MATERIAL; SURFACE TREATMENT OF METALLIC MATERIAL BY DIFFUSION INTO THE SURFACE, BY CHEMICAL CONVERSION OR SUBSTITUTION; COATING BY VACUUM EVAPORATION, BY SPUTTERING, BY ION IMPLANTATION OR BY CHEMICAL VAPOUR DEPOSITION, IN GENERAL
- C23C14/00—Coating by vacuum evaporation, by sputtering or by ion implantation of the coating forming material
- C23C14/22—Coating by vacuum evaporation, by sputtering or by ion implantation of the coating forming material characterised by the process of coating
- C23C14/34—Sputtering
- C23C14/35—Sputtering by application of a magnetic field, e.g. magnetron sputtering
-
- C—CHEMISTRY; METALLURGY
- C23—COATING METALLIC MATERIAL; COATING MATERIAL WITH METALLIC MATERIAL; CHEMICAL SURFACE TREATMENT; DIFFUSION TREATMENT OF METALLIC MATERIAL; COATING BY VACUUM EVAPORATION, BY SPUTTERING, BY ION IMPLANTATION OR BY CHEMICAL VAPOUR DEPOSITION, IN GENERAL; INHIBITING CORROSION OF METALLIC MATERIAL OR INCRUSTATION IN GENERAL
- C23C—COATING METALLIC MATERIAL; COATING MATERIAL WITH METALLIC MATERIAL; SURFACE TREATMENT OF METALLIC MATERIAL BY DIFFUSION INTO THE SURFACE, BY CHEMICAL CONVERSION OR SUBSTITUTION; COATING BY VACUUM EVAPORATION, BY SPUTTERING, BY ION IMPLANTATION OR BY CHEMICAL VAPOUR DEPOSITION, IN GENERAL
- C23C14/00—Coating by vacuum evaporation, by sputtering or by ion implantation of the coating forming material
- C23C14/22—Coating by vacuum evaporation, by sputtering or by ion implantation of the coating forming material characterised by the process of coating
- C23C14/34—Sputtering
- C23C14/35—Sputtering by application of a magnetic field, e.g. magnetron sputtering
- C23C14/354—Introduction of auxiliary energy into the plasma
- C23C14/355—Introduction of auxiliary energy into the plasma using electrons, e.g. triode sputtering
-
- H—ELECTRICITY
- H01—ELECTRIC ELEMENTS
- H01J—ELECTRIC DISCHARGE TUBES OR DISCHARGE LAMPS
- H01J37/00—Discharge tubes with provision for introducing objects or material to be exposed to the discharge, e.g. for the purpose of examination or processing thereof
- H01J37/32—Gas-filled discharge tubes
- H01J37/34—Gas-filled discharge tubes operating with cathodic sputtering
- H01J37/3402—Gas-filled discharge tubes operating with cathodic sputtering using supplementary magnetic fields
- H01J37/3405—Magnetron sputtering
Landscapes
- Chemical & Material Sciences (AREA)
- Engineering & Computer Science (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Materials Engineering (AREA)
- Mechanical Engineering (AREA)
- Metallurgy (AREA)
- Organic Chemistry (AREA)
- Physics & Mathematics (AREA)
- Plasma & Fusion (AREA)
- Analytical Chemistry (AREA)
- Physical Vapour Deposition (AREA)
Abstract
Plasma-enhanced magnetron-sputtered deposition (PMD) of materials is employed for low-temperature deposition of hard, wear-resistant thin films, such as metal nitrides, metal carbides, and metal carbo-nitrides, onto large, three-dimensional, irregularly shaped objects (20) without the requirement for substrate manipulation. The deposition is done by using metal sputter targets (18) as the source of the metal and immersing the metal sputter targets in a plasma (16) that is random in direction and fills the deposition chamber (12) by diffusion. The plasma is generated from at least two gases, the first gas comprising an inert gas, such as argon, and the second gas comprising a nitrogen source, such a nitrogen, and/or a carbon source, such as methane. Simultaneous with the deposition, the substrate is bombarded with ions from the plasma by biasing the substrate negative with respect to the plasma to maintain the substrate temperature and control the film microstructure. The substrate, metal targets, and plasma are all electrically decoupled from each other and from walls (14) of the deposition chamber, so as to provide independent electrical control of each component. The PMD process is applicable not only to the deposition of hard coatings, but also can be applied to any thin film process such as for electrically and thermally conductive coatings and optical coatings, requiring simultaneous, high-flux, ion-bombardment to control film properties.
Applications Claiming Priority (2)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
US07/929,986 US5346600A (en) | 1992-08-14 | 1992-08-14 | Plasma-enhanced magnetron-sputtered deposition of materials |
US929,986 | 1992-08-14 |
Publications (2)
Publication Number | Publication Date |
---|---|
CA2103770A1 true CA2103770A1 (en) | 1994-02-15 |
CA2103770C CA2103770C (en) | 1997-12-16 |
Family
ID=25458794
Family Applications (1)
Application Number | Title | Priority Date | Filing Date |
---|---|---|---|
CA002103770A Expired - Fee Related CA2103770C (en) | 1992-08-14 | 1993-08-10 | Plasma-enhanced magnetron-sputtered deposition of materials |
Country Status (6)
Country | Link |
---|---|
US (1) | US5346600A (en) |
EP (1) | EP0583736B1 (en) |
JP (1) | JPH0751752B2 (en) |
KR (1) | KR960002632B1 (en) |
CA (1) | CA2103770C (en) |
DE (1) | DE69306690T2 (en) |
Cited By (2)
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---|---|---|---|---|
CN113718219A (en) * | 2021-08-30 | 2021-11-30 | 长江先进存储产业创新中心有限责任公司 | Thin film deposition method and thin film deposition apparatus |
CN113755807A (en) * | 2021-09-13 | 2021-12-07 | 苏州龙盛电子有限公司 | Optical filter coating device and coating process |
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DE69310493T2 (en) * | 1992-08-14 | 1997-12-18 | Hughes Aircraft Co | SURFACE PREPARATION AND COATING METHOD FOR TITANNITRID ON CAST IRON |
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DE59309954D1 (en) * | 1992-12-21 | 2000-03-16 | Balzers Hochvakuum | Optical component, method for producing a layer, layer or layer system and use of the component |
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Family Cites Families (10)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CH631743A5 (en) * | 1977-06-01 | 1982-08-31 | Balzers Hochvakuum | METHOD FOR EVAPORATING MATERIAL IN A VACUUM EVAPORATION SYSTEM. |
JPS5983767A (en) * | 1982-11-04 | 1984-05-15 | Kawasaki Heavy Ind Ltd | Surface treatment of iron or steel |
JPS59123768A (en) * | 1982-12-28 | 1984-07-17 | Toyota Central Res & Dev Lab Inc | Method and device for simultaneous multi-element sputtering |
FR2557149B1 (en) * | 1983-12-27 | 1989-11-17 | France Etat | METHOD AND DEVICE FOR THE DEPOSITION ON A SUPPORT OF A THIN FILM OF A MATERIAL FROM A REACTIVE PLASMA |
DE3503397A1 (en) * | 1985-02-01 | 1986-08-07 | W.C. Heraeus Gmbh, 6450 Hanau | Sputtering plant for the reactive coating of a substrate with hard materials |
US4992153A (en) * | 1989-04-26 | 1991-02-12 | Balzers Aktiengesellschaft | Sputter-CVD process for at least partially coating a workpiece |
US4990229A (en) * | 1989-06-13 | 1991-02-05 | Plasma & Materials Technologies, Inc. | High density plasma deposition and etching apparatus |
DE3920835C2 (en) * | 1989-06-24 | 1997-12-18 | Leybold Ag | Device for coating substrates |
US5234560A (en) * | 1989-08-14 | 1993-08-10 | Hauzer Holdings Bv | Method and device for sputtering of films |
DE4038497C1 (en) * | 1990-12-03 | 1992-02-20 | Leybold Ag, 6450 Hanau, De |
-
1992
- 1992-08-14 US US07/929,986 patent/US5346600A/en not_active Expired - Lifetime
-
1993
- 1993-08-10 CA CA002103770A patent/CA2103770C/en not_active Expired - Fee Related
- 1993-08-12 DE DE69306690T patent/DE69306690T2/en not_active Expired - Fee Related
- 1993-08-12 EP EP93112909A patent/EP0583736B1/en not_active Expired - Lifetime
- 1993-08-13 KR KR1019930015680A patent/KR960002632B1/en not_active IP Right Cessation
- 1993-08-16 JP JP5202265A patent/JPH0751752B2/en not_active Expired - Lifetime
Cited By (4)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN113718219A (en) * | 2021-08-30 | 2021-11-30 | 长江先进存储产业创新中心有限责任公司 | Thin film deposition method and thin film deposition apparatus |
CN113718219B (en) * | 2021-08-30 | 2023-11-14 | 长江先进存储产业创新中心有限责任公司 | Thin film deposition method and thin film deposition apparatus |
CN113755807A (en) * | 2021-09-13 | 2021-12-07 | 苏州龙盛电子有限公司 | Optical filter coating device and coating process |
CN113755807B (en) * | 2021-09-13 | 2024-02-09 | 苏州龙盛电子有限公司 | Optical filter coating device and coating process |
Also Published As
Publication number | Publication date |
---|---|
DE69306690D1 (en) | 1997-01-30 |
CA2103770C (en) | 1997-12-16 |
US5346600A (en) | 1994-09-13 |
KR940004075A (en) | 1994-03-14 |
EP0583736A1 (en) | 1994-02-23 |
JPH0751752B2 (en) | 1995-06-05 |
DE69306690T2 (en) | 1997-07-24 |
KR960002632B1 (en) | 1996-02-24 |
JPH06192834A (en) | 1994-07-12 |
EP0583736B1 (en) | 1996-12-18 |
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