CA2109801A1 - Method for producing fullerenes - Google Patents

Method for producing fullerenes

Info

Publication number
CA2109801A1
CA2109801A1 CA2109801A CA2109801A CA2109801A1 CA 2109801 A1 CA2109801 A1 CA 2109801A1 CA 2109801 A CA2109801 A CA 2109801A CA 2109801 A CA2109801 A CA 2109801A CA 2109801 A1 CA2109801 A1 CA 2109801A1
Authority
CA
Canada
Prior art keywords
fullerenes
fullerene
yields
flame
producing fullerenes
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Granted
Application number
CA2109801A
Other languages
French (fr)
Other versions
CA2109801C (en
Inventor
Jack B. Howard
J. Thomas Mckinnon
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Massachusetts Institute of Technology
Original Assignee
Jack B. Howard
J. Thomas Mckinnon
Massachusetts Institute Of Technology
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Family has litigation
First worldwide family litigation filed litigation Critical https://patents.darts-ip.com/?family=24832897&utm_source=google_patent&utm_medium=platform_link&utm_campaign=public_patent_search&patent=CA2109801(A1) "Global patent litigation dataset” by Darts-ip is licensed under a Creative Commons Attribution 4.0 International License.
Application filed by Jack B. Howard, J. Thomas Mckinnon, Massachusetts Institute Of Technology filed Critical Jack B. Howard
Publication of CA2109801A1 publication Critical patent/CA2109801A1/en
Application granted granted Critical
Publication of CA2109801C publication Critical patent/CA2109801C/en
Anticipated expiration legal-status Critical
Expired - Lifetime legal-status Critical Current

Links

Classifications

    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B82—NANOTECHNOLOGY
    • B82Y—SPECIFIC USES OR APPLICATIONS OF NANOSTRUCTURES; MEASUREMENT OR ANALYSIS OF NANOSTRUCTURES; MANUFACTURE OR TREATMENT OF NANOSTRUCTURES
    • B82Y30/00—Nanotechnology for materials or surface science, e.g. nanocomposites
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B82—NANOTECHNOLOGY
    • B82Y—SPECIFIC USES OR APPLICATIONS OF NANOSTRUCTURES; MEASUREMENT OR ANALYSIS OF NANOSTRUCTURES; MANUFACTURE OR TREATMENT OF NANOSTRUCTURES
    • B82Y40/00—Manufacture or treatment of nanostructures
    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01B—NON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
    • C01B32/00—Carbon; Compounds thereof
    • C01B32/15—Nano-sized carbon materials
    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01B—NON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
    • C01B32/00—Carbon; Compounds thereof
    • C01B32/15—Nano-sized carbon materials
    • C01B32/152—Fullerenes
    • C01B32/154—Preparation
    • Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y10—TECHNICAL SUBJECTS COVERED BY FORMER USPC
    • Y10S—TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y10S977/00—Nanotechnology
    • Y10S977/84—Manufacture, treatment, or detection of nanostructure
    • Y10S977/842—Manufacture, treatment, or detection of nanostructure for carbon nanotubes or fullerenes

Abstract

A method for synthesizing fullerenes in flames is provided. Fullerenes are prepared by burning carbon-containing compounds in a flame and collecting the condensibles. The condensible contain the desired fullerenes. Fullerene yields can be optimized and fullerene composition can be selectively varied. Fullerene yields and compositions are determined by selectively controlling flame conditions and parameters such as C/O ratio, pressure, temperature, residence time, diluent concentration and gas velocity.
CA002109801A 1991-05-24 1992-05-22 Method for producing fullerenes Expired - Lifetime CA2109801C (en)

Applications Claiming Priority (2)

Application Number Priority Date Filing Date Title
US07/705,310 US5273729A (en) 1991-05-24 1991-05-24 Combustion method for producing fullerenes
US07/705,310 1991-05-24

Publications (2)

Publication Number Publication Date
CA2109801A1 true CA2109801A1 (en) 1992-11-26
CA2109801C CA2109801C (en) 1998-11-17

Family

ID=24832897

Family Applications (1)

Application Number Title Priority Date Filing Date
CA002109801A Expired - Lifetime CA2109801C (en) 1991-05-24 1992-05-22 Method for producing fullerenes

Country Status (6)

Country Link
US (1) US5273729A (en)
EP (2) EP0586533B1 (en)
JP (1) JP3404632B2 (en)
CA (1) CA2109801C (en)
DE (2) DE69232066T2 (en)
WO (1) WO1992020622A1 (en)

Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN110342499A (en) * 2019-07-26 2019-10-18 广西科学院 A kind of method that the biomass high-temperature carbonization micro- oxygen ablation in end prepares fullerene carbon ball

Families Citing this family (41)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US7494638B1 (en) * 1990-08-30 2009-02-24 Mitsubishi Corporation Form of carbon
US5304366A (en) * 1991-12-24 1994-04-19 Sri International Process and apparatus for producing and separating fullerenes
CA2091665C (en) * 1992-04-07 2003-01-07 Peter George Tsantrizos Process for the synthesis of fullerenes
DE59301138D1 (en) * 1992-05-06 1996-01-25 Hoechst Ag Separation of fullerenes
US5393955A (en) * 1993-01-14 1995-02-28 Simmons; Walter N. Preparation of fullerenes and apparatus therefor
US5350569A (en) * 1993-03-30 1994-09-27 The United States Of America As Represented By The United States Department Of Energy Storage of nuclear materials by encapsulation in fullerenes
US5510098A (en) * 1994-01-03 1996-04-23 University Of Central Florida CVD method of producing and doping fullerenes
WO1995026925A1 (en) * 1994-03-30 1995-10-12 Massachusetts Institute Of Technology Production of fullerenic nanostructures in flames
US6472705B1 (en) 1998-11-18 2002-10-29 International Business Machines Corporation Molecular memory & logic
US6806397B1 (en) 1999-09-17 2004-10-19 Ut-Battelle, Llc Synthesis of condensed phases containing polycyclic aromatic hydrocarbons fullerenes and nanotubes
US6645438B1 (en) 2000-05-05 2003-11-11 New Jersey Institute Of Technology Methods and apparatus for producing fullerenes in large quantities from liquid hydrocarbons
US6923915B2 (en) * 2001-08-30 2005-08-02 Tda Research, Inc. Process for the removal of impurities from combustion fullerenes
US7150863B2 (en) * 2001-08-30 2006-12-19 Tda Research, Inc. Polynuclear aromatic hydrocarbons for fullerene synthesis in flames
US6887291B2 (en) * 2001-08-30 2005-05-03 Tda Research, Inc. Filter devices and methods for carbon nanomaterial collection
US7279137B2 (en) 2001-08-30 2007-10-09 Tda Research, Inc. Burners and combustion apparatus for carbon nanomaterial production
JP4208714B2 (en) * 2001-08-31 2009-01-14 ナノ−シー，インク． Method for combustion synthesis of fullerenes
JP3926333B2 (en) * 2001-12-05 2007-06-06 ティーディーエイ リサーチ インコーポレイテッド Combustion method for the synthesis of carbon nanomaterials from liquid hydrocarbons
KR100519418B1 (en) * 2002-02-28 2005-10-07 재단법인서울대학교산학협력재단 Carbon nano particle having novel structure and properties
US20050232846A1 (en) * 2002-03-13 2005-10-20 Naoki Noguchi Process for production of fullerenes and method for separation thereof
AU2003301691B2 (en) * 2002-07-03 2009-01-22 Nano-C, Inc. Separation and purification of fullerenes
US7335344B2 (en) * 2003-03-14 2008-02-26 Massachusetts Institute Of Technology Method and apparatus for synthesizing filamentary structures
US20060140845A1 (en) * 2003-06-10 2006-06-29 Hiroaki Takehara Method for producing fullerene
EP1642928A4 (en) * 2003-07-04 2006-07-05 Bridgestone Corp Rubber composition and tire produced from the same
RU2240182C1 (en) * 2003-07-10 2004-11-20 Украинцев Валерий Борисович Palladium-containing hydrogenation catalyst preparation method
JP4316344B2 (en) * 2003-10-08 2009-08-19 フロンティアカーボン株式会社 Fullerene separation method
US20050129608A1 (en) * 2003-12-16 2005-06-16 Hiroaki Takehara Method for producing fullerenes
US20050129607A1 (en) * 2003-12-16 2005-06-16 Hiroaki Takehara Method for producing fullerenes
US20060078488A1 (en) * 2004-01-14 2006-04-13 Frontier Carbon Corporation Carbon material and process for producing the same
US20050230240A1 (en) * 2004-03-09 2005-10-20 Roman Dubrovsky Method and apparatus for carbon allotropes synthesis
DE102005003167B4 (en) * 2005-01-21 2007-07-12 Manfred PETERMÜLLER Fire retardant, and method of use
DE102005010766A1 (en) * 2005-03-02 2006-09-07 Deutsches Zentrum für Luft- und Raumfahrt e.V. Apparatus and method for the controlled production of nano soot particles
CN100488872C (en) * 2006-02-24 2009-05-20 厦门大学 Carbon cluster synthesizing apparatus
CN103227289B (en) * 2006-06-13 2016-08-17 索尔维美国有限公司 Comprise the organic photovoltaic devices of fullerene and derivative thereof
US8883113B2 (en) 2006-08-31 2014-11-11 Nano-C, Inc. Direct liquid-phase collection and processing of fullerenic materials
TWI473761B (en) * 2007-12-21 2015-02-21 索爾維美國有限公司 Organic photovoltaic devices comprising fullerenes and derivatives thereof and improved methods of making fullerene derivatives
US20100249447A1 (en) * 2009-03-17 2010-09-30 Nano-C, Inc. Purification of fullerene derivatives from various impurities
US9340697B2 (en) 2009-08-14 2016-05-17 Nano-C, Inc. Solvent-based and water-based carbon nanotube inks with removable additives
CN102648249B (en) * 2009-08-14 2016-04-13 Nano-C公司 There is the solvent-based of removable property additive and water base carbon nanotube ink
JP5119219B2 (en) * 2009-08-24 2013-01-16 Ｊｆｅケミカル株式会社 Method for producing carbon fine particles
KR101939874B1 (en) 2012-12-21 2019-01-17 나노-씨, 인크. Solvent-based and water-based carbon nanotube inks with removable additives
US9685600B2 (en) 2015-02-18 2017-06-20 Savannah River Nuclear Solutions, Llc Enhanced superconductivity of fullerenes

Family Cites Families (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
SU1707433A1 (en) * 1986-07-14 1992-01-23 Научно-Производственное Объединение "Техэнергохимпром" Method of flame neutralization of liquid halogen containing waste

Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN110342499A (en) * 2019-07-26 2019-10-18 广西科学院 A kind of method that the biomass high-temperature carbonization micro- oxygen ablation in end prepares fullerene carbon ball

Also Published As

Publication number Publication date
US5273729A (en) 1993-12-28
EP0586533A1 (en) 1994-03-16
EP0586533A4 (en) 1994-03-22
WO1992020622A1 (en) 1992-11-26
EP0586533B1 (en) 2001-09-19
CA2109801C (en) 1998-11-17
DE69233790D1 (en) 2010-08-19
EP1127841A3 (en) 2003-09-03
JP3404632B2 (en) 2003-05-12
DE69232066D1 (en) 2001-10-25
EP1127841B1 (en) 2010-07-07
JPH06507879A (en) 1994-09-08
DE69232066T2 (en) 2002-07-25
EP1127841A2 (en) 2001-08-29

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