CA2188262A1 - Method for fractionating a solution - Google Patents

Method for fractionating a solution

Info

Publication number
CA2188262A1
CA2188262A1 CA002188262A CA2188262A CA2188262A1 CA 2188262 A1 CA2188262 A1 CA 2188262A1 CA 002188262 A CA002188262 A CA 002188262A CA 2188262 A CA2188262 A CA 2188262A CA 2188262 A1 CA2188262 A1 CA 2188262A1
Authority
CA
Canada
Prior art keywords
phase
packing material
fractionating
material beds
sectional packing
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Granted
Application number
CA002188262A
Other languages
French (fr)
Other versions
CA2188262C (en
Inventor
Heikki Heikkila
Jarmo Kuisma
Hannu Paananen
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Xyrofin Oy
Original Assignee
Heikki Heikkila
Jarmo Kuisma
Hannu Paananen
Xyrofin Oy
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Heikki Heikkila, Jarmo Kuisma, Hannu Paananen, Xyrofin Oy filed Critical Heikki Heikkila
Publication of CA2188262A1 publication Critical patent/CA2188262A1/en
Application granted granted Critical
Publication of CA2188262C publication Critical patent/CA2188262C/en
Anticipated expiration legal-status Critical
Expired - Fee Related legal-status Critical Current

Links

Classifications

    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01D—SEPARATION
    • B01D15/00—Separating processes involving the treatment of liquids with solid sorbents; Apparatus therefor
    • B01D15/08—Selective adsorption, e.g. chromatography
    • B01D15/10—Selective adsorption, e.g. chromatography characterised by constructional or operational features
    • B01D15/18—Selective adsorption, e.g. chromatography characterised by constructional or operational features relating to flow patterns
    • B01D15/1814—Selective adsorption, e.g. chromatography characterised by constructional or operational features relating to flow patterns recycling of the fraction to be distributed
    • B01D15/1821—Simulated moving beds
    • B01D15/1828—Simulated moving beds characterized by process features
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01D—SEPARATION
    • B01D15/00—Separating processes involving the treatment of liquids with solid sorbents; Apparatus therefor
    • B01D15/08—Selective adsorption, e.g. chromatography
    • C—CHEMISTRY; METALLURGY
    • C12—BIOCHEMISTRY; BEER; SPIRITS; WINE; VINEGAR; MICROBIOLOGY; ENZYMOLOGY; MUTATION OR GENETIC ENGINEERING
    • C12F—RECOVERY OF BY-PRODUCTS OF FERMENTED SOLUTIONS; DENATURED ALCOHOL; PREPARATION THEREOF
    • C12F3/00—Recovery of by-products
    • C12F3/06—Recovery of by-products from beer and wine
    • D—TEXTILES; PAPER
    • D21—PAPER-MAKING; PRODUCTION OF CELLULOSE
    • D21C—PRODUCTION OF CELLULOSE BY REMOVING NON-CELLULOSE SUBSTANCES FROM CELLULOSE-CONTAINING MATERIALS; REGENERATION OF PULPING LIQUORS; APPARATUS THEREFOR
    • D21C11/00—Regeneration of pulp liquors or effluent waste waters
    • D21C11/0007—Recovery of by-products, i.e. compounds other than those necessary for pulping, for multiple uses or not otherwise provided for
    • D—TEXTILES; PAPER
    • D21—PAPER-MAKING; PRODUCTION OF CELLULOSE
    • D21C—PRODUCTION OF CELLULOSE BY REMOVING NON-CELLULOSE SUBSTANCES FROM CELLULOSE-CONTAINING MATERIALS; REGENERATION OF PULPING LIQUORS; APPARATUS THEREFOR
    • D21C11/00—Regeneration of pulp liquors or effluent waste waters
    • D21C11/0042—Fractionating or concentration of spent liquors by special methods
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01D—SEPARATION
    • B01D15/00—Separating processes involving the treatment of liquids with solid sorbents; Apparatus therefor
    • B01D15/08—Selective adsorption, e.g. chromatography
    • B01D15/26—Selective adsorption, e.g. chromatography characterised by the separation mechanism
    • B01D15/36—Selective adsorption, e.g. chromatography characterised by the separation mechanism involving ionic interaction
    • B01D15/361—Ion-exchange
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01D—SEPARATION
    • B01D2215/00—Separating processes involving the treatment of liquids with adsorbents
    • B01D2215/02—Separating processes involving the treatment of liquids with adsorbents with moving adsorbents
    • B01D2215/023—Simulated moving beds

Abstract

The invention relates to a method for fractionating a solution by a chromatographic simulated moving bed method in which the liquid flow is effected an a system comprising at least two sectional packing material beds in different ionic forms. The fractions enriched with different components are recovered during a multi-step sequence comprising the following operations, i.e. phases: feeding phase, eluting phase and recycling phase. The liquid present in the sectional packing material beds with its dry solids concentration profile is recycled during the recycling phase in a loop comprising one, two or more sectional packing material beds. The method can be employed for fractionating sulphite cooking liquor, molasses and vinasse, for example.
CA002188262A 1994-04-21 1995-04-19 Method for fractionating a solution Expired - Fee Related CA2188262C (en)

Applications Claiming Priority (3)

Application Number Priority Date Filing Date Title
FI941866 1994-04-21
FI941866A FI98791C (en) 1994-04-21 1994-04-21 Process for fractionating a solution
PCT/FI1995/000224 WO1995029002A1 (en) 1994-04-21 1995-04-19 Method for fractionating a solution

Publications (2)

Publication Number Publication Date
CA2188262A1 true CA2188262A1 (en) 1995-11-02
CA2188262C CA2188262C (en) 2006-08-29

Family

ID=8540572

Family Applications (1)

Application Number Title Priority Date Filing Date
CA002188262A Expired - Fee Related CA2188262C (en) 1994-04-21 1995-04-19 Method for fractionating a solution

Country Status (19)

Country Link
US (1) US5730877A (en)
EP (1) EP0756511B1 (en)
JP (1) JP3903266B2 (en)
KR (1) KR100372962B1 (en)
AT (1) ATE187657T1 (en)
AU (1) AU2260795A (en)
CA (1) CA2188262C (en)
DE (1) DE69513966T2 (en)
DK (1) DK0756511T3 (en)
ES (1) ES2141931T3 (en)
FI (1) FI98791C (en)
GR (1) GR3032860T3 (en)
HU (1) HU216319B (en)
PT (1) PT756511E (en)
RU (1) RU2136345C1 (en)
TW (1) TW351678B (en)
UA (1) UA39135C2 (en)
WO (1) WO1995029002A1 (en)
ZA (1) ZA953242B (en)

Families Citing this family (45)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US6663780B2 (en) 1993-01-26 2003-12-16 Danisco Finland Oy Method for the fractionation of molasses
FI96225C (en) 1993-01-26 1996-05-27 Cultor Oy Process for fractionation of molasses
US5795398A (en) 1994-09-30 1998-08-18 Cultor Ltd. Fractionation method of sucrose-containing solutions
FI97625C (en) * 1995-03-01 1997-01-27 Xyrofin Oy Method for crystallization of xylose from aqueous solutions
US6224776B1 (en) 1996-05-24 2001-05-01 Cultor Corporation Method for fractionating a solution
FI102962B1 (en) * 1996-06-24 1999-03-31 Xyrofin Oy Process for the preparation of xylitol
EP1017467B1 (en) 1997-01-29 2014-07-16 Amalgamated Research LLC Method of displacement chromatography
AU9094698A (en) * 1997-09-22 1999-04-12 Organo Corporation Method and equipment for chromatographic separation
FI974625A0 (en) * 1997-12-23 1997-12-23 Xyrofin Oy Foerfarande Foer framstaellning av xylos
JP3478325B2 (en) * 1997-12-25 2003-12-15 オルガノ株式会社 Chromatographic separation method
FI117465B (en) 2000-02-03 2006-10-31 Danisco Sweeteners Oy Procedure for hard coating of chewable cores
GB0022713D0 (en) * 2000-09-15 2000-11-01 Xyrofin Oy Method for fractionating liquid mixtures
PT1366198E (en) * 2000-12-28 2012-03-28 Danisco Separation process
FI111960B (en) 2000-12-28 2003-10-15 Danisco Sweeteners Oy separation Process
CN1250733C (en) * 2001-04-20 2006-04-12 纳幕尔杜邦公司 A product removal process for use i na biofermentation system
FI20010977A (en) * 2001-05-09 2002-11-10 Danisco Sweeteners Oy Chromatographic separation method
WO2003010339A1 (en) * 2001-07-24 2003-02-06 Arkenol, Inc. Separation of xylose and glucose
US7566556B2 (en) * 2002-03-01 2009-07-28 Academia Sinica Enhancing enzyme thermostability by mixing with sorghum liquor waste
FI20020592A (en) * 2002-03-27 2003-09-28 Danisco Sweeteners Oy Method for separating sugars, sugar alcohols, carbohydrates and mixtures thereof from solutions containing them
JP5826445B2 (en) * 2003-02-25 2015-12-02 フィンフィーズ フィンランド オイ Simulated moving floor system and method
US20060251761A1 (en) * 2005-05-03 2006-11-09 Robert Jansen Grain wet milling process for producing dextrose
US20060251762A1 (en) * 2005-05-03 2006-11-09 Robert Jansen Grain wet milling process for producing ethanol
US7544293B2 (en) 2005-09-26 2009-06-09 Semba Inc. Valve and process for interrupted continuous flow chromatography
FI120590B (en) * 2005-10-28 2009-12-15 Danisco Sweeteners Oy Difference method
EP2181194A1 (en) * 2007-08-03 2010-05-05 Tate & Lyle Ingredients Americas, Inc. Cereal refining process
WO2009094418A2 (en) * 2008-01-24 2009-07-30 Tate And Lyle Ingredients Americas, Inc. Corn wet milling process
US9109265B2 (en) * 2008-06-26 2015-08-18 Dupont Nutrition Biosciences Aps Process for separation of Ca- or Mg-sulfite spent liquor to yield crystalline xylose
DK2401046T3 (en) 2009-02-25 2020-08-03 Dupont Nutrition Biosci Aps SEPARATION PROCESS
EP2292803B1 (en) 2009-07-07 2013-02-13 DuPont Nutrition Biosciences ApS Separation process
RS53549B1 (en) * 2010-03-30 2015-02-27 Dupont Nutrition Biosciences Aps Separation process
ES2862178T3 (en) 2010-06-26 2021-10-07 Virdia Llc Sugar mixtures production methods
IL206678A0 (en) 2010-06-28 2010-12-30 Hcl Cleantech Ltd A method for the production of fermentable sugars
IL207329A0 (en) 2010-08-01 2010-12-30 Robert Jansen A method for refining a recycle extractant and for processing a lignocellulosic material and for the production of a carbohydrate composition
IL207945A0 (en) 2010-09-02 2010-12-30 Robert Jansen Method for the production of carbohydrates
GB2505148B8 (en) 2011-04-07 2016-12-07 Virdia Ltd Lignocellulose conversion processes and products
US9617608B2 (en) 2011-10-10 2017-04-11 Virdia, Inc. Sugar compositions
US9493851B2 (en) 2012-05-03 2016-11-15 Virdia, Inc. Methods for treating lignocellulosic materials
GB2517338B (en) 2012-05-03 2020-03-25 Virdia Inc A method for fractionating a liquid sample
JP2016531584A (en) * 2013-09-05 2016-10-13 ダウ グローバル テクノロジーズ エルエルシー Chromatographic separation of sugars using a cation exchange resin formulation.
CN104611476B (en) * 2013-11-04 2018-04-27 南京工业大学 A kind of xylose method separated with arabinose
CN103923130B (en) * 2014-04-18 2016-02-24 黑龙江八一农垦大学 Be separated the method for glucose and xylose in stalk fibre enzymolysis solution
CN112226466A (en) 2015-01-07 2021-01-15 威尔迪亚公司 Method for extracting and converting hemicellulose sugars
US10258903B2 (en) * 2015-03-12 2019-04-16 Dow Global Technologies Llc Chromatographic separation of saccharides using polymeric macroporous alkylene-bridged resin
BR112019013005A2 (en) 2016-12-21 2019-10-08 Creatus Biosciences Inc metschnikowia species isolated, method for producing xylitol, bioderivated xylitol and composition
EP3722501A1 (en) * 2019-04-12 2020-10-14 Lenzing Aktiengesellschaft Method for the recovery of alkaline solution and method for producing regenerated cellulose moulded parts comprising such a method

Family Cites Families (9)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US4631129A (en) * 1985-10-04 1986-12-23 Suomen Sokeri Oy Production of pure sugars and lignosulfonates from sulfite spent liquor
JPS62235014A (en) * 1986-04-04 1987-10-15 株式会社　南部電機製作所 Selecting packer for egg
US5122275A (en) * 1986-05-08 1992-06-16 A. E. Staley Manufacturing Company Simulated moving bed chromatographic separation
US5177008A (en) * 1987-12-22 1993-01-05 Kampen Willem H Process for manufacturing ethanol and for recovering glycerol, succinic acid, lactic acid, betaine, potassium sulfate, and free flowing distiller's dry grain and solubles or a solid fertilizer therefrom
US4990259A (en) * 1988-12-16 1991-02-05 The Amalgamated Sugar Company Chromatographic separator sorbent bed preparation
US4940548A (en) * 1989-04-17 1990-07-10 Uop Chromatographic separation process for recovering individual diethyltoluene isomers
US5198120A (en) * 1989-12-26 1993-03-30 Japan Organo Co., Ltd. Process for fractional separation of multi-component fluid mixture
US5225580A (en) * 1990-08-16 1993-07-06 Uop Process for separating fatty acids and triglycerides
FI932108A (en) * 1993-05-10 1994-11-11 Xyrofin Oy Method for fractionating sulphite broth

Also Published As

Publication number Publication date
DE69513966T2 (en) 2000-05-04
HU216319B (en) 1999-06-28
UA39135C2 (en) 2001-06-15
KR100372962B1 (en) 2003-04-21
EP0756511B1 (en) 1999-12-15
JP3903266B2 (en) 2007-04-11
FI941866A (en) 1995-10-22
WO1995029002A1 (en) 1995-11-02
RU2136345C1 (en) 1999-09-10
HU9602906D0 (en) 1996-12-30
EP0756511A1 (en) 1997-02-05
JPH09511946A (en) 1997-12-02
ATE187657T1 (en) 2000-01-15
HUT75293A (en) 1997-05-28
CA2188262C (en) 2006-08-29
FI98791C (en) 1997-08-25
KR970702093A (en) 1997-05-13
GR3032860T3 (en) 2000-07-31
DE69513966D1 (en) 2000-01-20
PT756511E (en) 2000-04-28
FI941866A0 (en) 1994-04-21
TW351678B (en) 1999-02-01
FI98791B (en) 1997-05-15
ES2141931T3 (en) 2000-04-01
US5730877A (en) 1998-03-24
ZA953242B (en) 1996-01-18
DK0756511T3 (en) 2000-05-01
AU2260795A (en) 1995-11-16

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Effective date: 20140422