CA2267058A1 - Preparation of sulphonic fluorinated polymer solutions - Google Patents
Preparation of sulphonic fluorinated polymer solutions Download PDFInfo
- Publication number
- CA2267058A1 CA2267058A1 CA002267058A CA2267058A CA2267058A1 CA 2267058 A1 CA2267058 A1 CA 2267058A1 CA 002267058 A CA002267058 A CA 002267058A CA 2267058 A CA2267058 A CA 2267058A CA 2267058 A1 CA2267058 A1 CA 2267058A1
- Authority
- CA
- Canada
- Prior art keywords
- preparation
- fluorinated polymer
- polymer solutions
- ionomers
- fluorinated
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Granted
Links
Classifications
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08J—WORKING-UP; GENERAL PROCESSES OF COMPOUNDING; AFTER-TREATMENT NOT COVERED BY SUBCLASSES C08B, C08C, C08F, C08G or C08H
- C08J3/00—Processes of treating or compounding macromolecular substances
- C08J3/12—Powdering or granulating
- C08J3/16—Powdering or granulating by coagulating dispersions
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08J—WORKING-UP; GENERAL PROCESSES OF COMPOUNDING; AFTER-TREATMENT NOT COVERED BY SUBCLASSES C08B, C08C, C08F, C08G or C08H
- C08J3/00—Processes of treating or compounding macromolecular substances
- C08J3/02—Making solutions, dispersions, lattices or gels by other methods than by solution, emulsion or suspension polymerisation techniques
- C08J3/09—Making solutions, dispersions, lattices or gels by other methods than by solution, emulsion or suspension polymerisation techniques in organic liquids
- C08J3/091—Making solutions, dispersions, lattices or gels by other methods than by solution, emulsion or suspension polymerisation techniques in organic liquids characterised by the chemical constitution of the organic liquid
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08J—WORKING-UP; GENERAL PROCESSES OF COMPOUNDING; AFTER-TREATMENT NOT COVERED BY SUBCLASSES C08B, C08C, C08F, C08G or C08H
- C08J2327/00—Characterised by the use of homopolymers or copolymers of compounds having one or more unsaturated aliphatic radicals, each having only one carbon-to-carbon double bond, and at least one being terminated by a halogen; Derivatives of such polymers
- C08J2327/02—Characterised by the use of homopolymers or copolymers of compounds having one or more unsaturated aliphatic radicals, each having only one carbon-to-carbon double bond, and at least one being terminated by a halogen; Derivatives of such polymers not modified by chemical after-treatment
- C08J2327/12—Characterised by the use of homopolymers or copolymers of compounds having one or more unsaturated aliphatic radicals, each having only one carbon-to-carbon double bond, and at least one being terminated by a halogen; Derivatives of such polymers not modified by chemical after-treatment containing fluorine atoms
Abstract
A process for preparing a solution and/or dispersion containing sulphonic (per)fluorinated ionomers having -SO3M functional groups, wherein M is selected from H, Li, Na, K, NR4 (R equal to or different from each other are selected from H, CH3, C2H5) , characterized in that it dissolves the above defined ionomers at a temperature comprised between the room temperature and about 150°C, in a monophasic ternary mixture essentially constituted by water, by a C1-C4 alcohol and by a fluoro(poly)oxyalkylene having one hydrogen atom in at least a fluorinated end group; the dispersed polymer particle sizes are in the range 30-100 nm.
Applications Claiming Priority (2)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
ITMI98A002523 | 1998-11-23 | ||
IT1998MI002523A IT1303779B1 (en) | 1998-11-23 | 1998-11-23 | PREPARATION OF SOLUTIONS OF SULPHONIC FLUORINATED POLYMERS. |
Publications (2)
Publication Number | Publication Date |
---|---|
CA2267058A1 true CA2267058A1 (en) | 2000-05-23 |
CA2267058C CA2267058C (en) | 2009-02-03 |
Family
ID=11381103
Family Applications (1)
Application Number | Title | Priority Date | Filing Date |
---|---|---|---|
CA002267058A Expired - Fee Related CA2267058C (en) | 1998-11-23 | 1999-03-29 | Preparation of sulphonic fluorinated polymer solutions |
Country Status (8)
Country | Link |
---|---|
US (1) | US6197903B1 (en) |
EP (1) | EP1004615B1 (en) |
JP (1) | JP4226722B2 (en) |
KR (1) | KR100604427B1 (en) |
CN (1) | CN1150255C (en) |
CA (1) | CA2267058C (en) |
DE (1) | DE69928899T2 (en) |
IT (1) | IT1303779B1 (en) |
Families Citing this family (22)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
US6921482B1 (en) * | 1999-01-29 | 2005-07-26 | Mykrolis Corporation | Skinned hollow fiber membrane and method of manufacture |
ITMI20010383A1 (en) | 2001-02-26 | 2002-08-26 | Ausimont Spa | POROUS HYDROPHILIC MEMBRANES |
ITMI20010384A1 (en) | 2001-02-26 | 2002-08-26 | Ausimont Spa | POROUS HYDROPHILIC MEMBRANES |
ITMI20020056A1 (en) | 2002-01-15 | 2003-07-15 | Ausimont Spa | AQUEOUS COMPOSITIONS OF PERFLUOROPOLYETHER PHOSPHATES AND THEIR USE TO CONFER THE PAPER WITH OIL REPELLENCE |
ITMI20020057A1 (en) | 2002-01-15 | 2003-07-15 | Ausimont Spa | AQUEOUS COMPOSITIONS OF PERFLUOROPOLYETHER PHOSPHATES AND THEIR USE TO CONFER THE PAPER WITH OIL REPELLENCE |
EP2365008B1 (en) * | 2002-06-17 | 2016-10-19 | Daikin Industries, Ltd. | Fluoropolymer dispersion and process for producing fluoropolymer dispersion |
JP2005082748A (en) * | 2003-09-10 | 2005-03-31 | Asahi Kasei Corp | Method for producing dispersion liquid containing fluorine-based copolymer |
ITMI20050444A1 (en) | 2005-03-17 | 2006-09-18 | Solvay Solexis Spa | IONOMERIC MEMBRANE |
ITMI20050445A1 (en) | 2005-03-17 | 2006-09-18 | Solvay Solexis Spa | COMPONENT IONOMERIC MEMBRANE |
ITMI20050446A1 (en) | 2005-03-17 | 2006-09-18 | Solvay Solexis Spa | COMPOSITE CCM |
ITMI20052508A1 (en) | 2005-12-28 | 2007-06-29 | Solvay Solexis Spa | PROCESS TO OBTAIN CCM WITH SUBGASKET |
ITMI20052509A1 (en) | 2005-12-28 | 2007-06-29 | Solvay Solexis Spa | ASSEMBLED FOR ELECTROCHEMICAL DEVICES |
EP2062933A1 (en) | 2007-11-26 | 2009-05-27 | Solvay Solexis S.p.A. | Fluoroionomer liquid composition |
EP2264085B1 (en) * | 2008-04-09 | 2014-12-17 | Asahi Kasei E-materials Corporation | Fluorine-containing ion exchange resin dispersed composition |
US9217045B2 (en) | 2008-12-11 | 2015-12-22 | Solvay Specialty Polymers Italy S.P.A. | Purification of fluoroionomer compositions |
SG175044A1 (en) * | 2009-04-06 | 2011-11-28 | Entegris Inc | Non-dewetting porous membranes |
US9450262B2 (en) | 2009-06-12 | 2016-09-20 | Solvay Specialty Polymers Italy S.P.A. | Fluoroionomers dispersions having a low surface tension, low liquid viscosity and high solid content |
US20120063952A1 (en) * | 2010-09-10 | 2012-03-15 | Hong Keith C | Uv resistant clear laminates |
EP2643387B1 (en) | 2010-11-26 | 2019-03-06 | Solvay Specialty Polymers Italy S.p.A. | Liquid compositions of fluorinated ion exchange polymers |
US20140315121A1 (en) | 2011-11-04 | 2014-10-23 | SolvCore GmbH & Co. KG | Method for the preparation of catalyst-coated membranes method for the preparation of catalyst-coated membranes |
EP2842620A1 (en) | 2013-08-26 | 2015-03-04 | Agfa-Gevaert | A method for preparing a composite membrane |
KR102601806B1 (en) | 2017-09-14 | 2023-11-14 | 쓰리엠 이노베이티브 프로퍼티즈 컴파니 | Fluorinated copolymers having sulfonyl pendant groups and compositions and articles containing the same |
Family Cites Families (18)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
US3706773A (en) | 1967-04-25 | 1972-12-19 | Allied Chem | Fluorocarbon compounds |
NL160013C (en) | 1968-11-26 | 1979-09-17 | Du Pont | PROCESS FOR PREPARING SOLUTIONS OF A SULFONYL GROUPS CONTAINING FLUORO CARBON POLYMER. |
US3674800A (en) | 1969-04-14 | 1972-07-04 | Allied Chem | Derivatives pyridinium of polyfluoroisoalkoxyalkanamides |
US4275226A (en) * | 1978-08-25 | 1981-06-23 | Asahi Glass Company, Ltd. | Process for producing fluorovinyl ether |
US4348310A (en) * | 1979-09-26 | 1982-09-07 | E. I. Du Pont De Nemours And Company | Solutions of sulfonyl fluoride compounds and fluoropolymers |
US4341685A (en) | 1979-11-20 | 1982-07-27 | Asahi Glass Company, Ltd. | Process for preparing organic dispersion of acid type fluorinated polymer |
US4453991A (en) | 1981-05-01 | 1984-06-12 | E. I. Du Pont De Nemours And Company | Process for making articles coated with a liquid composition of perfluorinated ion exchange resin |
US4433082A (en) * | 1981-05-01 | 1984-02-21 | E. I. Du Pont De Nemours And Company | Process for making liquid composition of perfluorinated ion exchange polymer, and product thereof |
US4540716A (en) * | 1983-01-13 | 1985-09-10 | Diamond Shamrock Chemicals Company | Method for making finely divided perfluorocarbon copolymer |
DE3650465T2 (en) * | 1985-02-09 | 1996-09-12 | Asahi Chemical Ind | Permeable polymer membrane for gas drying |
FR2597491B1 (en) * | 1986-04-22 | 1988-06-10 | Commissariat Energie Atomique | PROCESS FOR MANUFACTURING COLLOIDS OF CATIONIC CONDUCTIVE PERFLUOROUS IONOMERS AND COLLOIDS OBTAINED |
JPH02188569A (en) * | 1988-10-28 | 1990-07-24 | Minnesota Mining & Mfg Co <3M> | Fluoroaliphatic sulfonamide poly(oxyalkylene) compound |
EP0545068A3 (en) * | 1991-11-08 | 1993-12-22 | Du Pont | Wetting of diaphragms |
US5658962A (en) | 1994-05-20 | 1997-08-19 | Minnesota Mining And Manufacturing Company | Omega-hydrofluoroalkyl ethers, precursor carboxylic acids and derivatives thereof, and their preparation and application |
IT1271075B (en) | 1994-11-21 | 1997-05-26 | Ausimont Spa | TERNARY SOLVENT MIXTURES, AND THEIR USE FOR THE REMOVAL OF OIL SUBSTANCES |
US5532310A (en) * | 1995-04-28 | 1996-07-02 | Minnesota Mining And Manufacturing Company | Surfactants to create fluoropolymer dispersions in fluorinated liquids |
WO1997011081A1 (en) * | 1995-09-19 | 1997-03-27 | E.I. Du Pont De Nemours And Company | Modified fluorosulfonic acids |
DE69705854T2 (en) * | 1996-10-15 | 2002-04-11 | Du Pont | COMPOSITIONS CONTAINING HIGH-FLUORINE ION EXCHANGER POLYMER PARTICLES |
-
1998
- 1998-11-23 IT IT1998MI002523A patent/IT1303779B1/en active
-
1999
- 1999-03-24 EP EP99105912A patent/EP1004615B1/en not_active Expired - Lifetime
- 1999-03-24 DE DE69928899T patent/DE69928899T2/en not_active Expired - Lifetime
- 1999-03-29 CA CA002267058A patent/CA2267058C/en not_active Expired - Fee Related
- 1999-03-30 JP JP08989899A patent/JP4226722B2/en not_active Expired - Fee Related
- 1999-03-31 US US09/281,913 patent/US6197903B1/en not_active Expired - Lifetime
- 1999-03-31 CN CNB99105928XA patent/CN1150255C/en not_active Expired - Fee Related
- 1999-03-31 KR KR1019990011357A patent/KR100604427B1/en not_active IP Right Cessation
Also Published As
Publication number | Publication date |
---|---|
CA2267058C (en) | 2009-02-03 |
ITMI982523A1 (en) | 2000-05-23 |
KR100604427B1 (en) | 2006-07-25 |
DE69928899D1 (en) | 2006-01-19 |
KR20000034833A (en) | 2000-06-26 |
IT1303779B1 (en) | 2001-02-23 |
CN1254727A (en) | 2000-05-31 |
DE69928899T2 (en) | 2006-08-17 |
JP2000159965A (en) | 2000-06-13 |
EP1004615B1 (en) | 2005-12-14 |
EP1004615A2 (en) | 2000-05-31 |
JP4226722B2 (en) | 2009-02-18 |
EP1004615A3 (en) | 2000-09-13 |
US6197903B1 (en) | 2001-03-06 |
CN1150255C (en) | 2004-05-19 |
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Legal Events
Date | Code | Title | Description |
---|---|---|---|
EEER | Examination request | ||
MKLA | Lapsed |
Effective date: 20160329 |