CA2506708A1 - Water-soluble products and methods of making and using the same - Google Patents
Water-soluble products and methods of making and using the same Download PDFInfo
- Publication number
- CA2506708A1 CA2506708A1 CA002506708A CA2506708A CA2506708A1 CA 2506708 A1 CA2506708 A1 CA 2506708A1 CA 002506708 A CA002506708 A CA 002506708A CA 2506708 A CA2506708 A CA 2506708A CA 2506708 A1 CA2506708 A1 CA 2506708A1
- Authority
- CA
- Canada
- Prior art keywords
- coverall
- product
- water
- soluble
- washed
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Granted
Links
- 238000000034 method Methods 0.000 title claims abstract 32
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims abstract 2
- 239000002195 soluble material Substances 0.000 claims 23
- 238000005406 washing Methods 0.000 claims 17
- 239000004744 fabric Substances 0.000 claims 12
- 239000000463 material Substances 0.000 claims 9
- 239000000356 contaminant Substances 0.000 claims 6
- 238000004980 dosimetry Methods 0.000 claims 6
- 230000002285 radioactive effect Effects 0.000 claims 6
- 239000004372 Polyvinyl alcohol Substances 0.000 claims 4
- 239000000853 adhesive Substances 0.000 claims 4
- 230000001070 adhesive effect Effects 0.000 claims 4
- 229920002451 polyvinyl alcohol Polymers 0.000 claims 4
- 125000002777 acetyl group Chemical group [H]C([H])([H])C(*)=O 0.000 claims 3
- SMZOUWXMTYCWNB-UHFFFAOYSA-N 2-(2-methoxy-5-methylphenyl)ethanamine Chemical compound COC1=CC=C(C)C=C1CCN SMZOUWXMTYCWNB-UHFFFAOYSA-N 0.000 claims 2
- NIXOWILDQLNWCW-UHFFFAOYSA-N 2-Propenoic acid Natural products OC(=O)C=C NIXOWILDQLNWCW-UHFFFAOYSA-N 0.000 claims 2
- CERQOIWHTDAKMF-UHFFFAOYSA-N Methacrylic acid Chemical compound CC(=C)C(O)=O CERQOIWHTDAKMF-UHFFFAOYSA-N 0.000 claims 2
- 229920002472 Starch Polymers 0.000 claims 2
- 238000011109 contamination Methods 0.000 claims 2
- 238000001035 drying Methods 0.000 claims 2
- 239000004745 nonwoven fabric Substances 0.000 claims 2
- 230000035699 permeability Effects 0.000 claims 2
- 239000002901 radioactive waste Substances 0.000 claims 2
- 239000008107 starch Substances 0.000 claims 2
- 235000019698 starch Nutrition 0.000 claims 2
- 229920002134 Carboxymethyl cellulose Polymers 0.000 claims 1
- 229920003171 Poly (ethylene oxide) Polymers 0.000 claims 1
- 229920002845 Poly(methacrylic acid) Polymers 0.000 claims 1
- 229920002125 Sokalan® Polymers 0.000 claims 1
- 239000003513 alkali Substances 0.000 claims 1
- 235000010948 carboxy methyl cellulose Nutrition 0.000 claims 1
- 125000002057 carboxymethyl group Chemical group [H]OC(=O)C([H])([H])[*] 0.000 claims 1
- 229920002678 cellulose Polymers 0.000 claims 1
- 239000001913 cellulose Substances 0.000 claims 1
- 235000010980 cellulose Nutrition 0.000 claims 1
- 239000012459 cleaning agent Substances 0.000 claims 1
- 239000003086 colorant Substances 0.000 claims 1
- 239000003599 detergent Substances 0.000 claims 1
- 235000019325 ethyl cellulose Nutrition 0.000 claims 1
- 229920001249 ethyl cellulose Polymers 0.000 claims 1
- 229920001038 ethylene copolymer Polymers 0.000 claims 1
- 229920005648 ethylene methacrylic acid copolymer Polymers 0.000 claims 1
- 239000000835 fiber Substances 0.000 claims 1
- 235000010985 glycerol esters of wood rosin Nutrition 0.000 claims 1
- 239000001341 hydroxy propyl starch Substances 0.000 claims 1
- 229920003063 hydroxymethyl cellulose Polymers 0.000 claims 1
- 229920003088 hydroxypropyl methyl cellulose Polymers 0.000 claims 1
- 235000010979 hydroxypropyl methyl cellulose Nutrition 0.000 claims 1
- 235000013828 hydroxypropyl starch Nutrition 0.000 claims 1
- 230000003116 impacting effect Effects 0.000 claims 1
- 229920000554 ionomer Polymers 0.000 claims 1
- 229920000609 methyl cellulose Polymers 0.000 claims 1
- 235000010981 methylcellulose Nutrition 0.000 claims 1
- 238000012544 monitoring process Methods 0.000 claims 1
- 229920002401 polyacrylamide Polymers 0.000 claims 1
- 239000004584 polyacrylic acid Substances 0.000 claims 1
- 229920000036 polyvinylpyrrolidone Polymers 0.000 claims 1
- 239000001267 polyvinylpyrrolidone Substances 0.000 claims 1
- 235000013855 polyvinylpyrrolidone Nutrition 0.000 claims 1
- 230000001681 protective effect Effects 0.000 claims 1
- 239000012857 radioactive material Substances 0.000 claims 1
- 150000003839 salts Chemical class 0.000 claims 1
- 230000003068 static effect Effects 0.000 claims 1
- 239000000126 substance Substances 0.000 claims 1
- 239000004094 surface-active agent Substances 0.000 claims 1
- 239000002759 woven fabric Substances 0.000 claims 1
Classifications
-
- A—HUMAN NECESSITIES
- A41—WEARING APPAREL
- A41D—OUTERWEAR; PROTECTIVE GARMENTS; ACCESSORIES
- A41D1/00—Garments
-
- A—HUMAN NECESSITIES
- A41—WEARING APPAREL
- A41D—OUTERWEAR; PROTECTIVE GARMENTS; ACCESSORIES
- A41D13/00—Professional, industrial or sporting protective garments, e.g. surgeons' gowns or garments protecting against blows or punches
- A41D13/12—Surgeons' or patients' gowns or dresses
- A41D13/1236—Patients' garments
- A41D13/1263—Suits
-
- A—HUMAN NECESSITIES
- A41—WEARING APPAREL
- A41D—OUTERWEAR; PROTECTIVE GARMENTS; ACCESSORIES
- A41D13/00—Professional, industrial or sporting protective garments, e.g. surgeons' gowns or garments protecting against blows or punches
- A41D13/0002—Details of protective garments not provided for in groups A41D13/0007 - A41D13/1281
-
- A—HUMAN NECESSITIES
- A41—WEARING APPAREL
- A41D—OUTERWEAR; PROTECTIVE GARMENTS; ACCESSORIES
- A41D13/00—Professional, industrial or sporting protective garments, e.g. surgeons' gowns or garments protecting against blows or punches
- A41D13/02—Overalls, e.g. bodysuits or bib overalls
-
- A—HUMAN NECESSITIES
- A41—WEARING APPAREL
- A41D—OUTERWEAR; PROTECTIVE GARMENTS; ACCESSORIES
- A41D31/00—Materials specially adapted for outerwear
- A41D31/04—Materials specially adapted for outerwear characterised by special function or use
-
- A—HUMAN NECESSITIES
- A62—LIFE-SAVING; FIRE-FIGHTING
- A62B—DEVICES, APPARATUS OR METHODS FOR LIFE-SAVING
- A62B17/00—Protective clothing affording protection against heat or harmful chemical agents or for use at high altitudes
- A62B17/006—Protective clothing affording protection against heat or harmful chemical agents or for use at high altitudes against contamination from chemicals, toxic or hostile environments; ABC suits
-
- A—HUMAN NECESSITIES
- A41—WEARING APPAREL
- A41D—OUTERWEAR; PROTECTIVE GARMENTS; ACCESSORIES
- A41D2500/00—Materials for garments
- A41D2500/30—Non-woven
Abstract
Water-soluble products and methods of making and using water~soluble product s are disclosed.
Claims (66)
1. A multiple-use, launderable coverall comprising water-soluble material.
2. The coverall of Claim 1, wherein the coverall is pre-washed.
3. The coverall of Claim 1, wherein the coverall is capable of being washed in an aqueous bath up to about 20 times without negatively impacting structural integrity of the coverall.
4. The coverall of Claim 1, wherein the water-soluble material comprises polyvinyl alcohol with or without acetyl groups, cross-linked or uncross linked.
5. The coverall of Claim 1, wherein the coverall consists essentially of water-soluble material.
6. The coverall of Claim 1, wherein the coverall consists of water-soluble material.
7. The coverall of Claim 1, wherein the coverall comprises a close system.
8. The coverall of Claim 7, wherein the closure system comprises one or more zippers, drawstrings, snaps, buttons, adhesives, hoop and loop materials, or a combination thereof.
9. The coverall of Claim 7, wherein the closure system comprises water-soluble material, water-dispersible material, or a combination thereof.
10. The coverall of Claim 1, wherein the coverall comprises two or more fabric sheets joined to one another with one or more sheet fastening devices.
11. The cover all of Claim 10, wherein the one or more sheet fastening devices comprise thread, adhesives, hoop and loop materials, or a combination thereof.
12. The coverall of Claim 10, wherein the one or more sheet fastening devices comprises water-soluble material, water-dispersible material, or a combination thereof.
13. The coverall of Claim 1, wherein the coverall comprises at least one single ply fabric, double ply fabric, fabric/film laminate, or combination thereof.
14. The coverall of Claim 1, wherein the coverall is pre-treated with a chemical treatment to enhance one or more properties selected from impermeability, permeability, flame resistance, moisture vapor permeability, tear strength, and stain resistance.
15. The coverall of Claim 1, wherein the coverall comprises one or more pockets.
16. The coverall of Claim 15, wherein the coverall comprises up to 15 pockets.
17. The coverall of Claim 15, wherein the coverall comprises 11 pockets for dosimetry use.
18. The coverall of Claim 17, wherein the pockets are located along the coverall as shown in Figures 2A and 2B.
19. The coverall of Claim 15, wherein at least one of the one or more pockets has a flap closure.
20. The coverall of Claim 1, wherein the coverall comprises pre-shrunk fabrics having a fabric shrinkage of less than about 5% when exposed to a washing cycle.
21. The coverall of Claim 1, wherein the coverall comprises nonwoven fabric substantially free of lint and static.
22. The coverall of Claim 1, wherein at least a portion of the coverall is dyed or printed.
23. The coverall of Claim 1, wherein the coverall further comprises at least one of an integral hood, integral booties, or a combination thereof.
24. The coverall of Claim 1, wherein the coverall further comprises a wash counter integrally connected to the coverall.
25. The coverall of Claim 24, wherein the wash counter comprises water-soluble material, water-dispersible material, or a combination thereof.
26. The coverall of Claim 24, wherein the wash counter comprises a detachable strip of coverall material.
27. A dosimetry coverall having eleven pockets as shown in FIGS. 2A-2B.
28. The dosimetry coverall of Claim 27, wherein the coverall is a single-use coverall.
29. The single-use dosimetry coverall of Claim 28, wherein the coverall comprises at least 50 parts by weight (pbw) of water-soluble materials, based on a total weight of the single-use coverall.
30. The single-use dosimetry coverall of Claim 28, wherein the coverall consists essentially of water-soluble materials.
31. The single-use dosimetry coverall of Claim 28, wherein the coverall consists of water-soluble materials.
32. A reusable coverall for use in the nuclear industry, wherein after the coverall is (i) exposed to one or more radioactive materials at an exposure level of at least 1,000,000 disintegrations per minute as measured by an automatic laundry monitor and (ii) subsequently washed, the washed reusable coverall has a contamination level of less than 25,000 disintegrations per minute as measured by the same automatic laundry monitor.
33. The reusable coverall of Claim 32, wherein the washed reusable coverall has a contamination level of less than 5,000 disintegrations per minute as measured by the same automatic laundry monitor.
34. The reusable coverall of Claim 32, wherein the reusable coverall comprises water-soluble material.
35. The reusable coverall of Claim 34, wherein the water-soluble material comprises polyvinyl alcohol with or without acetyl groups, cross-linked or uncross-linked.
36. A method of reducing an amount of radioactive waste generated by at least one contaminated product, wherein the at least one contaminated product comprises (i) the multiple-use, launderable coverall of Claim 1, (ii) the reusable coverall of Claim 32, or (iii) a combination thereof, wherein said method comprises:
(a) washing the at least one contaminated product in an aqueous bath under washing condition such that the at least one product does not become soluble, producing a washed product;
(b) using the washed product for an intended purpose;
(c) optionally, repeating steps (a) and (b) one or more times; and (d) disposing of the washed product by placing the washed product in an aqueous bath under condition such that at least a portion of the product becomes soluble.
(a) washing the at least one contaminated product in an aqueous bath under washing condition such that the at least one product does not become soluble, producing a washed product;
(b) using the washed product for an intended purpose;
(c) optionally, repeating steps (a) and (b) one or more times; and (d) disposing of the washed product by placing the washed product in an aqueous bath under condition such that at least a portion of the product becomes soluble.
37. A method of reducing an amount of radioactive waste generated by at least one contaminated product, wherein said method comprises:
(a) washing the at least one contaminated product in an aqueous bath under washing condition such that the at least one product does not become soluble, producing a washed product;
(b) using the washed product for an intended purpose;
(c) optionally, repeating steps (a) and (b) one or more times; and (d) disposing of the washed product by placing the washed product in an aqueous bath under condition such that at least a portion of the product becomes soluble.
(a) washing the at least one contaminated product in an aqueous bath under washing condition such that the at least one product does not become soluble, producing a washed product;
(b) using the washed product for an intended purpose;
(c) optionally, repeating steps (a) and (b) one or more times; and (d) disposing of the washed product by placing the washed product in an aqueous bath under condition such that at least a portion of the product becomes soluble.
38. A method of removing one or more radioactive contaminants from a product containing water-soluble material, wherein said method comprises:
(a) washing the product in an aqueous bath under washing condition such that the water-soluble material does not become soluble; and (b) drying the washed product.
(a) washing the product in an aqueous bath under washing condition such that the water-soluble material does not become soluble; and (b) drying the washed product.
39. The method of claim 38, wherein said method further comprises:
(c) using the washed product for an intended purpose that exposes the washed product to one or more radioactive contaminants;
(d) optionally, repeating steps (a) to (c) one or more times; and (e) disposing of the washed product by placing the washed product in an aqueous bath under condition such that at least a portion of the product becomes soluble.
(c) using the washed product for an intended purpose that exposes the washed product to one or more radioactive contaminants;
(d) optionally, repeating steps (a) to (c) one or more times; and (e) disposing of the washed product by placing the washed product in an aqueous bath under condition such that at least a portion of the product becomes soluble.
40. The method of Claim 38, wherein the washing step is repeated two or more times.
41. The method of Claim 38, wherein the washing step is repeated up to about 20 times.
42. The method of Claim 38, wherein the washing step is repeated up to about 10 times.
43. The method of Claim 38, wherein the aqueous bath has a bath temperature of less than about 90°C during the washing step.
44. The method of Claim 38, wherein the aqueous bath has a bath temperature of less than about 75°C during the washing step.
45. The method of Claim 38, wherein the aqueous bath has a bath temperature of less than about 50°C during the washing step.
46. The method of Claim 38, wherein the aqueous bath has a bath temperature of less than about 37°C during the washing step.
47. The method of Claim 38, wherein the aqueous bath contains one or more surfactants, detergents, or other cleaning agents.
48. The method of Claim 38, wherein the product is a fiber, a fabric, a film, or a combination thereof.
49. The method of Claim 38, wherein the product is a non-woven fabric.
50. The method of Claim 38, wherein the product is a woven fabric.
51. The method of Claim 38, wherein the product is a knitted fabric.
52. The method of Claim 38, wherein the product comprises a garment, protective clothing, coveralls, booties, a face mash, gloves, apparel, linen, a drape, a towel, a fabric, a film, a laminate containing at least one fabric or film, a sponge, a mop head, a web, a bag, a gauze, a pad, a wipe, a pillow, or a bandage.
53. The method of Claim 38, wherein the product comprises coveralls.
54. The method of Claim 38, wherein the water-soluble material comprises polyvinyl alcohol; polyacrylic acid; polymethacrylic acid;
polyacrylamide;
water-soluble cellulose derivatives comprising methyl celluloses, ethyl celluloses, hydroxymethyl celluloses, hydroxypropyl methyl celluloses, and carboxymethyl celluloses; carboxymethylchitin; polyvinyl pyrrolidone; ester gum; water-soluble derivatives of starch comprising hydroxypropyl starch and carboxymethyl starch;
water-soluble polyethylene oxides; alkali water-soluble materials comprising ethylene copolymers of acrylic acid (EAA) and methacrylic acid (EMAA), and salts thereof; and ionomers containing acrylic acid and/or methacrylic acid.
polyacrylamide;
water-soluble cellulose derivatives comprising methyl celluloses, ethyl celluloses, hydroxymethyl celluloses, hydroxypropyl methyl celluloses, and carboxymethyl celluloses; carboxymethylchitin; polyvinyl pyrrolidone; ester gum; water-soluble derivatives of starch comprising hydroxypropyl starch and carboxymethyl starch;
water-soluble polyethylene oxides; alkali water-soluble materials comprising ethylene copolymers of acrylic acid (EAA) and methacrylic acid (EMAA), and salts thereof; and ionomers containing acrylic acid and/or methacrylic acid.
55. The method of Claim 53, wherein the water-soluble material comprises polyvinyl alcohol with or without acetyl groups, cross-linked or uncross-linked.
56. The method of claim 38, further comprising one or more steps comprising:
(i) agitating the product or aqueous bath during the washing step;
(ii) extracting water from the product;
(iii) monitoring the dried product for one or more radioactive contaminants;
(iv) marking the washed product to identify the number of wash cycles that the product has experienced;
(v) using the washed product for a particular purpose, wherein the particular purpose exposes the washed product to one or more radioactive contaminants; and (vi) repeating any of the above steps.
(i) agitating the product or aqueous bath during the washing step;
(ii) extracting water from the product;
(iii) monitoring the dried product for one or more radioactive contaminants;
(iv) marking the washed product to identify the number of wash cycles that the product has experienced;
(v) using the washed product for a particular purpose, wherein the particular purpose exposes the washed product to one or more radioactive contaminants; and (vi) repeating any of the above steps.
57. A method of removing one or more radioactive contaminants from a coverall containing water-soluble material, wherein said method comprises:
(a) washing the coverall in an aqueous bath under washing condition such that the water-soluble material does not become soluble; and (b) drying the washed coverall.
(a) washing the coverall in an aqueous bath under washing condition such that the water-soluble material does not become soluble; and (b) drying the washed coverall.
58. The method of claim 57, wherein said method further comprises:
(c) using the washed coverall for an intended purpose that exposes the washed coverall to one or more radioactive contaminants;
(d) optionally, repeating steps (a) to (c) one or more times; and (e) disposing of the washed coverall by placing the washed coverall in an aqueous bath under condition such that at least a portion of the coverall becomes soluble.
(c) using the washed coverall for an intended purpose that exposes the washed coverall to one or more radioactive contaminants;
(d) optionally, repeating steps (a) to (c) one or more times; and (e) disposing of the washed coverall by placing the washed coverall in an aqueous bath under condition such that at least a portion of the coverall becomes soluble.
59. The method of claim 57, wherein the coverall comprises (a) two or more fabric sheets joined to one another with (b) one or more sheet fastening devices comprising thread, adhesive, hoop and loop material, or a combination thereof, and (c) a closure system comprising one or more zippers, drawstrings, snaps, buttons, adhesives, hoop and loop materials, or a combination thereof; wherein (a) the two or more fabric sheets, (b) the one or more sheet fastening devices, and (c) the closure system each independently comprise water-soluble material, water-dispersible material, or a combination thereof.
60. Scrubs comprising water-soluble materials.
61. The scrubs of Claim 60, wherein the scrubs are single-use scrubs.
62. The scrubs of Claim 60, wherein the scrubs comprise (i) a smock-like, shirt having a V-neck, sleeves, and up to about six pockets, and (ii) a pair of pants having pant legs, and up to about four pockets.
63. The scrubs of Claim 62, wherein the scrubs comprise shout sleeves and long pant legs.
64. The scrubs of Claim 60, wherein the scrubs comprise at least 50 parts by weight (pbw) of water-soluble materials, based on a total weight of the scrubs.
65. The scrubs of Claim 60, wherein the scrubs consist essentially of water-soluble materials and at least one colorant to provide a desired color.
66. The scrubs of Claim 65, wherein the desired color is blue or green.
Applications Claiming Priority (5)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
US43159002P | 2002-12-06 | 2002-12-06 | |
US60/431,590 | 2002-12-06 | ||
US10/369,170 | 2003-02-18 | ||
US10/369,170 US6854135B2 (en) | 2002-12-06 | 2003-02-18 | Reusable, launderable water-soluble coveralls |
PCT/US2003/038478 WO2004052522A2 (en) | 2002-12-06 | 2003-12-04 | Water-soluble products and methods of making and using the same |
Publications (2)
Publication Number | Publication Date |
---|---|
CA2506708A1 true CA2506708A1 (en) | 2004-06-24 |
CA2506708C CA2506708C (en) | 2011-05-10 |
Family
ID=32474187
Family Applications (1)
Application Number | Title | Priority Date | Filing Date |
---|---|---|---|
CA2506708A Expired - Lifetime CA2506708C (en) | 2002-12-06 | 2003-12-04 | Water-soluble products and methods of making and using the same |
Country Status (10)
Country | Link |
---|---|
US (3) | US6854135B2 (en) |
EP (1) | EP1583603B1 (en) |
JP (1) | JP5021206B2 (en) |
KR (1) | KR100794982B1 (en) |
AT (1) | ATE440511T1 (en) |
AU (1) | AU2003299585A1 (en) |
CA (1) | CA2506708C (en) |
DE (1) | DE60329027D1 (en) |
RU (1) | RU2357775C2 (en) |
WO (1) | WO2004052522A2 (en) |
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2003
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- 2003-12-04 CA CA2506708A patent/CA2506708C/en not_active Expired - Lifetime
- 2003-12-04 EP EP03799871A patent/EP1583603B1/en not_active Expired - Lifetime
- 2003-12-04 JP JP2005508456A patent/JP5021206B2/en not_active Expired - Lifetime
- 2003-12-04 AU AU2003299585A patent/AU2003299585A1/en not_active Abandoned
- 2003-12-04 DE DE60329027T patent/DE60329027D1/en not_active Expired - Lifetime
- 2003-12-04 RU RU2005121270/12A patent/RU2357775C2/en active
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- 2003-12-04 WO PCT/US2003/038478 patent/WO2004052522A2/en active Application Filing
- 2003-12-04 KR KR1020057010138A patent/KR100794982B1/en active IP Right Grant
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2004
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2005
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RU2357775C2 (en) | 2009-06-10 |
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AU2003299585A8 (en) | 2004-06-30 |
DE60329027D1 (en) | 2009-10-08 |
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KR100794982B1 (en) | 2008-01-16 |
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US20040216217A1 (en) | 2004-11-04 |
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JP2006512512A (en) | 2006-04-13 |
US7203974B2 (en) | 2007-04-17 |
US20040107473A1 (en) | 2004-06-10 |
WO2004052522A3 (en) | 2004-08-19 |
RU2005121270A (en) | 2006-01-20 |
KR20050091711A (en) | 2005-09-15 |
EP1583603A4 (en) | 2006-05-17 |
WO2004052522A2 (en) | 2004-06-24 |
US20050235391A1 (en) | 2005-10-27 |
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