CA2552615A1 - Process device with improved power generation - Google Patents

Process device with improved power generation Download PDF

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Publication number
CA2552615A1
CA2552615A1 CA002552615A CA2552615A CA2552615A1 CA 2552615 A1 CA2552615 A1 CA 2552615A1 CA 002552615 A CA002552615 A CA 002552615A CA 2552615 A CA2552615 A CA 2552615A CA 2552615 A1 CA2552615 A1 CA 2552615A1
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Canada
Prior art keywords
field device
coupled
conversion module
energy conversion
field
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Granted
Application number
CA002552615A
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French (fr)
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CA2552615C (en
Inventor
Robert J. Karschnia
Marcos Peluso
Adrian C. Toy
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Rosemount Inc
Original Assignee
Rosemount Inc.
Robert J. Karschnia
Marcos Peluso
Adrian C. Toy
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Application filed by Rosemount Inc., Robert J. Karschnia, Marcos Peluso, Adrian C. Toy filed Critical Rosemount Inc.
Publication of CA2552615A1 publication Critical patent/CA2552615A1/en
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Classifications

    • G—PHYSICS
    • G08—SIGNALLING
    • G08C—TRANSMISSION SYSTEMS FOR MEASURED VALUES, CONTROL OR SIMILAR SIGNALS
    • G08C17/00—Arrangements for transmitting signals characterised by the use of a wireless electrical link
    • G08C17/02—Arrangements for transmitting signals characterised by the use of a wireless electrical link using a radio link
    • G—PHYSICS
    • G08—SIGNALLING
    • G08C—TRANSMISSION SYSTEMS FOR MEASURED VALUES, CONTROL OR SIMILAR SIGNALS
    • G08C17/00—Arrangements for transmitting signals characterised by the use of a wireless electrical link
    • Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y02—TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
    • Y02E—REDUCTION OF GREENHOUSE GAS [GHG] EMISSIONS, RELATED TO ENERGY GENERATION, TRANSMISSION OR DISTRIBUTION
    • Y02E10/00—Energy generation through renewable energy sources
    • Y02E10/50—Photovoltaic [PV] energy
    • Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y02—TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
    • Y02E—REDUCTION OF GREENHOUSE GAS [GHG] EMISSIONS, RELATED TO ENERGY GENERATION, TRANSMISSION OR DISTRIBUTION
    • Y02E70/00—Other energy conversion or management systems reducing GHG emissions
    • Y02E70/30—Systems combining energy storage with energy generation of non-fossil origin
    • Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y02—TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
    • Y02T—CLIMATE CHANGE MITIGATION TECHNOLOGIES RELATED TO TRANSPORTATION
    • Y02T10/00—Road transport of goods or passengers
    • Y02T10/10—Internal combustion engine [ICE] based vehicles
    • Y02T10/12—Improving ICE efficiencies

Abstract

A wireless field device (34, 50, 70, 80, 91, 100) is disclosed. The field device (34, 50, 70, 80, 91, 100) includes a wireless communications module (32) and an energy conversion module (38) . The wireless communications modu le (32) is configured to wirelessly communicate process-related information wit h another device. The energy conversion module (38) is coupled to the wireless communications module (32) . The energy conversion module (38) is configured to couple to a thermal source, and to generate electricity from thermal potential energy in the thermal source.

Description

PROCESS DEVICE WITH IMPROVED POWER
GEf3ER~T I0~3 BACKGROUND OF THE INVENTION
The present invention relates to .industrial process control and monitoring systems. More specifically, the present invention Jrelates to the generation of electrical power for field devices within such systems.
In industrial settings, control systems are used to monitor and control inventories of industrial and chemical processes, and the like. Typically, the control system performs these functions using field devices distributed at key locations ~in the industrial process and coupled to the control circuitry in the control room by a process control loop. The term "field device" refers to any device that performs a function in a distributed control or process monitoring system, including all devices used in the measurement, control and monitoring of industrial processes.
Field devices are used by the process control .and measurement industry for a variety of purposes. Usually such devices have a field-hardened enclosure so that they can be installed outdoors in.
relatively rugged environments and are able to withstand climatalogical extremes of temperature, humidity, vibration, mechanical shock, etc. These devices also can typically operate on relatively low power. For example, field devices are currently available that~receive all of their operating power from a known 4-20 mA loop.
Some field devices include a transducer. A
transducer is understood to mean either a device that generates an output signal based on a physical input or that generates a physical output based on an input signal. Typically, a transducer transforms an input into an output having a different form. Types of transducers include various analytical equipment, pressure sensors, thermistors, thermocouples, strain gauges, flow transmitters, positioners, actuators, solenoids, indicator lights, and others.
Typically, each field device also includes communication circuitry that is used for communicating with a process control room, or other circuitry, over a process control loop. In some installations, the process control loop is also used to deliver a regulated current and/or voltage to the field device for powering the field device.
Traditionally, analog field devices have been connected to the control room by two-wire process control current loops, with each device connected to the control room by a single two-wire control loop. Typically, a voltage differential is maintained between the two wires within a range of voltages from 12-45 volts for analog mode and 9-50 volts for digital mode. Some analog field devices transmit a signal to the control room by modulating the current running through the current loop to a current proportional to the sensed process variable.
Other analog field devices can perform an action under the control of the control room by controlling the magnitude of the current through the loop. In addition to, or in the alternative,, the process control loop can carry digital signals used for communication with field devices. Digital communication allows ~a much larger degree of communication than analog communication. Moreover, digital devices also do not require separate wiring for each field device. Field devices that communicate digitally can respond to and communicate selectively with the control room and/or' other field devices.
Further, such devices can provide additional signaling such as diagnostics and/or alarms.
In some installations, wireless technologies have begun to be used to communicate with field devices. Wireless operation simplifies field device wiring and setup. Wireless installations are currently used in which the field device is manufactured to include an internal battery, potentially charged by a solar cell without any sort of wired connection. Problems exist in using an internal battery as the energy demands of wireless devices may vary greatly depending on numerous factors such as the device reporting rate, device elements, et cetera.
Difficulties also arise in installations where solar power is not reliable. For example, it becomes problematic to use solar power in areas that experience full shade twenty-four hours a day, indoors seven days a week, or in parts of the world where solar insolation numbers are very small, such as in the Arctic Circle. Accordingly, in these installations, powering a wireless process device using solar power is not reliable. Accordingly, there is an ongoing significant need for wireless process devices that can operate using an abundant renewable source of power that is not dependent upon the sun.
SUMMARY OF THE INZTENTION
A wireless field device is disclosed. The field device includes a wireless communications module and an energy conversion module.. The wireless communications module is configured to wirelessly communicate process-related information with another device. The energy conversion module is coupled to the wireless communications module. The energy conversion module is configured to couple to a thermal source, and to generate electricity from thermal potential energy in the thermal source.
A field device includes a controller, a wireless communications module, and a power generation module. The wireless communications module is coupled to the controller. The power generation module is located within the field device, and is coupled to the controller and to the wireless communications module. The power generation module is configured to interact with molecules proximate the exterior of the field device to generate electricity.
The power generation module is preferably a thermal generator that harvests energy from a temperature differential near the field device.
BRIEF DESCRIPTION OF THE DRAWINGS
FIG. 1 is a diagrammatic view of an exemplary field device with which embodiments of the present invention~is particularly useful.
FIG. 2 is a block diagram of the field device shown in FIG. 1.
FIG. 3 is a block diagram of a field device including wireless communication circuitry for communicating with a remote device.
FIG. 4 is a diagrammatic view of a wireless field device operating in accordance with an embodiment of the present invention.
FIGS. 5A and 5B are diagrammatic views of a temperature-sensing field device deriving power in accordance with embodiments of the present invention.
FIGS. 6A and 6B are diagrammatic views of a field device deriving power from a semiconductor thermoelectric generator in accordance with embodiments of the present invention.
FIG. 7 is diagrammatic view of a field device deriving power from a semiconductor thermoelectric generator in accordance with an embodiment of the present invention.
DETAINED DESCRIPTION OF THE PREFERRED EMBODIMENTS
~ FIGS. 1 and 2 are diagrammatic and block diagram views of an exemplary field device with which embodiments of the present invention are useful.
Process control or monitoring system 10 includes a control room or control system 12 that couples to one or more field devices 14 over a two-wire process control loop 16. Examples of process control loop 16 include analog 4-20 mA communication, hybrid protocols which include both analog and digital communication such. as the Highway Addressable Remote Transducer (HART~) standard, as well as all-digital protocols such as the FOUNDATIONTM Fieldbus standard.
Generally process control loop protocols can both power the field device and allow communication between the field device and other devices.
In this example, field device 14 includes circuitry 18 coupled to actuator/transducer 20 and to process control loop 16 via terminal board 21 in housing 23. Field device 14 is illustrated as a process variable (PV) generator in that it couples to a process and senses an aspect, such as temperature, pressure, pH, flow, et cetera of the process and provides an indication thereof. Other examples of field devices include valves, actuators, controllers, ~"r and displays.

Generally field devices are characterized by their ability to operate in the "field" which may expose them to environmental stresses, such as temperature, humidity and pressure. In addition to environmental stresses, field devices must often withstand exposure to corrosive, hazardous and/or even explosive atmospheres. Further, such devices must also operate in the presence of vibration and/or electromagnetic interference.
FIG. 3 is a block diagram of a wireless field device in accordance with an embodiment of the present invention. Field device 34 includes power conversion module 38, controller 35, wireless communications module 32, and actuator/transducer 20.
Conversion module 38 can be any device that is able to convert thermal potential energy from the process into electrical energy. Conversion module 38 can be any device, known or later developed, that translates thermal potential energy available from molecules proximate field device 34 into electricity. For example, module 38 .can employ known thermopile devices to generate electricity from disparate temperatures using the Pettier Effect. Other temperature-based conversion devices can be used for module . 38. Such devices include thermoelectric diodes; solid state thermogenerators; and semiconductor thermoelectric generators. Moreover, any device now known, or later developed, that converts thermal potential energy to electricity may -g_ b~e used as or in combination with module 38.
Conversion module 38 can provide power for wireless communications module 32 alone, other portions of field device 34, or even all of the components within field device 34.
Wireless communication module 32 is coupled to controller ~35 and interacts with external wireless devices via antenna 26 based upon commands and/or ' data from controller 35. Wireless communication 32 can communicate process-related information as well as device-related information. Depending upon the application, wireless communication module 32 may be adapted to communicate in accordance with arty suitable wireless communication protocol including, but not limited to: wireless networking technologies (such as IEEE 802.11b wireless access points and wireless networking devices built by Linksys of Irvine, California), cellular or digital networking technologies (such as Microburst~ by Aeris Communications Inc. of San Jose, California), ultra wide band, free space optics, Global System for Mobile Communications (GSM), General Packet Radio Service (GPRS), Code Division Multiple Access (CDMA), spread spectrum technology, infrared communications techniques, SMS (Short Messaging Service/text messaging), or any other suitable wireless technology. Further, known data collision technology can be employed such that multiple units can coexist .within wireless operating rage of one another. Such collision prevention can include using a number of different radio-frequency channels and/or spread spectrum techniques.
Wireless communication module 32 can also include transducers for a plurality of wireless communication methods. For example, primary wireless communication could be performed using relatively long distance communication methods, such as GSM or GPRS, while a secondary, or additional communication method could be provided for technicians, or operators near the unit, using for example, IEEE
802.11b or Bluetooth.
Some wireless communications modules may include circuitry that can interact with the Global Positioning System (GPS). GPS can be advantageously employed in device 34 for mobile devices to allow finding the individual device 34 in a remote location. However, location sensing based upon other techniques can be used as well. ' Memory 37 is illustrated in FIG. 3 as being separate from controller 35, but may, in fact, be part of controller 35. Memory 37 can be any suitable type of memory including volatile memory (such as Random Access Memory), non-volatile memory (such as flash memory, EEPROM memory, ' etc.) and any combination thereof. Memory 37 may contain program instructions for controller 35 as well as any suitable administrative overhead data for device 34.
Memory 37~may contain a unique identifier for device 34, such that device 34 can distinguish wireless communications meant for it among other wireless communications. Examples of such an identifier could include, a Media Access Controller (MAC) address, Electronic Serial Number, global phone number, Internet Protocol (IP) address, or any other suitable identifier. Moreover, memory 37 may include information about attached field devices, such as their unique identifiers, configurations, and abilities. Finally, controller 35, using memory 37 can cause the output of device 34 to be provided in any suitable form. For example, configuration and interaction with field device' 34 and/or one or more associated field devices could be provided as HyperText Markup Language (HTML) web pages.
FIG. 4 is a diagrammatic view of a wireless field device operably coupled to energy conversion module 38 in accordance with an embodiment of the present invention. In the embodiment illustrated in FIG. 4, module 38 is disposed external to field device 34. Additionally, transducer 20 is illustrated in FIG. 4 as being a sensor. The sensor or sensor tap 20 and wireless field device 34 are, by virtue of the process to which they are coupled, maintained at a differential temperature. For example, sensor 20 may be coupled to process fluid that is at a higher temperature than the ambient temperature to which device 34 is exposed. Conversion module 38 is thermally coupled, illustrated by phantom lines 40, 42 to sensor 20 and field device 34, respectively.
The differential temperature coupled to conversion module 38 generates electricity within conversion module 38 that is provided to wireless field device 34 via line 44. When so powered, field device 34 generates and transmits wireless information to one or more remote transceivers 46, which may, in fact, be part of control system 12.
Given that conversion module 38 generally transforms thermal potential energy in or near the process fluid to electricity, one particularly synergistic application for embodiments of the present invention is that of temperature measuring field devices. In such embodiments, sensor 20 is a temperature sensor, such as a thermocouple, thermistor, or resistance temperature device (RTD).
While embodiments of the present invention will be described with respect to a temperature-sensing field device, embodiments of the present invention are practicable with any field device.
FIGS. 5A and 5B are diagrammatic views of field devices deriving power ,from thermal energy in accordance with embodiments of the present invention.
FIG. 5A illustrates a temperature-sensing . field device 50 having an electronics compartment 52 coupled to a thermowell 54 which is shaped, or otherwise configured, to engage a process fluid.
Within thermowell 54, a temperature sensor 56 provides an indication of process fluid temperature proximate end 58 of thermowell 54. Additionally, a portion of conversion module 38 (shown in FIG 4) is disposed proximate end 58. Specifically, device 60 is disposed proximate end 58 and electrically coupled to electronics compartment 52 via power.lines 62, 64.
Device 60 is preferably any suitable device that converts thermal energy into electricity. Thus, device 60 may be a thermopile, thermodiode (thermoelectric diode), a solid state thermogenerator, a semiconductor thermoelectric generator, or any combination thereof. Temperature sensing of field device 50 is accomplished via temperature sensor 56 providing a signal on signal lines 66 and 68 to electronics compartment 52.
FIG. 5B illustrates field device 70 having an electronics compartment 52 and a thermowell 54.
In contrast to field device 50, field device 70 employs device 72 that generates electricity related to the temperature to which it is exposed. Examples o.f suitable devices for device 72 include a thermopile or a thermoelectric diode. Such devices are suitable because they do not require a heat flow through the device, but instead generate electricity based upon exposure to a specific thermal source.
Technology advancements are currently increasing the feasibility of a field device such as that illustrated in FIGS. 5A and 5B. On the power generation side, solid state thermogenerators are becoming more and more efficient. Additionally, advancements in wireless technology are also increasing the feasibility of such field devices.
Specifically, wireless transmitters need less and less power to cover the same area. Additionally, even in embodiments where the transmission distance of a specific field device may be limited, such as to a radius of approximately 20 meters, embodiments of the present invention contemplate the use of repeating or mesh networks to increase the area covered by such devices. Thus, where a plurality of wireless field devices are disposed within the wireless transmission radius from one another, a first device can have its wireless information relayed by a second device thus extending the net range of the first device by that of the second device.
FIGS. 6A and 6B illustrate field devices that employ a semiconductor thermoelectric generator for thermoenergy scavenging in accordance with embodiments of the present invention. Semiconductor thermoelectric generators produce power when a temperature difference is maintained across the device. Thus, there is a flow of heat through the device, so the cool side should be properly heat sunk for advantageous power generation.
In FIG. ~A, field device 80 includes electronics compartment 52 and thermowell 54 having a semiconductor thermoelectric generator device 82 'disposed proximate distal end 58 of thermowell 54.
In order to allow device 52 to have heat flow therethrough, a'thermal conductor 84, such as a heat conducting member, is coupled to cold side 86 of device 82 and conveys heat in the direction of arrow 88 to one or more optional cooling fins 90 that, in some embodiments, may be disposed within electronics compartment 52. Conductor 84 may be any arrangement that conveys heat efficiently. For example, conductor 84 could be a copper rod.
FIG. 6B illustrates an alternate arrangement for generating electricity from thermoenergy. Field device 91 includes electronics compartment 52 and thermowell 54. However, semiconductor thermoelectric generator device 92 is disposed above thermowell 54 proximate electronics compartment 52. This allows device 92 to be relatively larger in comparison to device 82. In order to maintain advantageous heat flow across device 92, thermal conductor 84 is still coupled thermally to distal end 58 and conveys heat in the direction of arrow 88 to hot side 94 of device 92.
The cold side 96 of device 92 is coupled to one or more optional cooling fins 90 that may or may not be disposed within housing 52.
As illustrated in FIGS. 6A and 6B, there are different ways to conceptually achieve' thermal flow across a semiconductor thermoelectric element.
While FIGS. 6A and 6B illustrate a pair of examples, other possibilities may be practiced in accordance with embodiments of the present invention. In fact, the thermoelectric power generation element. need not be disposed proximate the field device itself.
FIG. 7 illustrates a diagrammatic view of field device 100 having an electronics compartment 52 coupled to a thermowell 54 for sensing a process temperature. A thermoelectric power-generating device 102 is disposed remote from field device 100 and coupled thereto via power conductors 104, 106. An elevated process temperature is coupled to hot side 108 of semiconductor thermoelectric generator device 110, which has one or more optional fins 90 coupled to its cold side 112. Since device 102 is mounted remote from field device 100, the physical size of device 102 is not constrained at all by the design of field device 100. This is advantageous because typically only small thermoelectric generating devices will fit within thermowell 54. Commercially available thermoelectric generating devices having a size on the order of 2 mm by 4 mm by 2 mm thick are believed to be able to fit within the thermowell, and to generate approximately 48 milivolts and 80 miliamps with a 50° C temperature different across hot and cold sides. This generated voltage is generally low and preferably is stepped up with a step up voltage conversion circuit known in the art of field devices. Accordingly, approximately 0.22 watts of heat flow through the thermoelectric generator device under such conditions. Although the operating efficiency is relatively low (approximately 20) the approximately. 4 milliwatts of generated power is believed to be sufficient for wireless field device operation.
However, if the thermoelectric generating device is disposed remote from the field device, it is reasonable that the thermoelectric generating device could be sized much larger than the example given above. Specifically, thermoelectric generating devices having a size of approximately 15 mm by 15 mm by 2 mm thick can be used. Such devices are commercially available and believed to generate 375 millivolts and 300 milliamps for the same 50° C
difference. While a step up voltage conversion circuit is still useful, the approximate 112 milliwatts of generated power makes the design of such a circuit much simpler and lower cost.
Approximately 6 watts of heat flow through the thermoelectric generating device under such conditions.
The conversion module can include, or be coupled to, additional power circuitry to provide additional functions related to power generation and/or storage. For example, a storage device, such as a capacitor or rechargeable cell can be operably coupled to the conversion module to maintain power levels when the amount of power available from the ' conversion module (via the thermal source) drops below that which could minimally operate the field device, or portions thereof., Additionally, any known power conditioning circuitry can be used to step up the voltage, remove noise from the power signal, isolate the power signal, smooth and/or otherwise shape the power signal. However, those skilled in the art will recognize that any desired functions can be accommodated with power conditioning circuitry as desired.
Although the present invention has been described with reference to preferred embodiments, workers skilled in the art will recognize that changes may be made in form and detail without departing from the spirit and scope of the invention.

Claims (22)

1. A field device comprising:
a wireless communications module configured to wirelessly communicate process-related information with another device; and an energy conversion module coupled to the wireless communications module, the energy conversion module configured to couple to a thermal source, and to convert thermal potential energy into electricity to power circuitry within the field device.
2. The field device of claim 1, wherein the energy conversion module includes a thermopile.
3. The field device of claim 1, wherein the energy conversion module includes a thermoelectric diode.
4. The field device of claim 1, wherein the energy conversion module includes a semiconductor thermoelectric generator.
5. The field device of claim 1, wherein the energy conversion module is disposed proximate the field device.
6. The field device of claim 1, wherein the energy conversion device is disposed remote from the field device.
7. The field device of claim 1, and further comprising:

a controller coupled to the energy conversion module and to the wireless communication module; and a transducer coupled to the process and the controller.
8. The field device of claim 7, wherein the transducer is a sensor.
9. The field device of claim 8, wherein the sensor is a temperature sensor.
10. The field device of claim 9, wherein the temperature sensor generates electricity and is a component of the energy conversion module.
11. The field device of claim 9, and further comprising:
a thermowell configured to couple to a process fluid.
12. The field device of claim 11, and further comprising a heat conducting member disposed within the thermowell and configured to convey heat away from the process fluid.
13. The field device of claim 12, wherein the energy conversion module includes a semiconductor thermoelectric generator operably coupled to the heat conducting member.
14. The field device of claim 13, wherein the semiconductor thermoelectric generator has a hot side thermally coupled to the process fluid, and a cold side thermally coupled to the heat conducting member.
15. The field device, of claim 14, wherein the heat conducting member has a first end coupled to the thermoelectric generator, and a second end coupled to at least one cooling fin.
16. The field device of claim 13, wherein the semiconductor thermoelectric generator has a hot side coupled to a first end of the heat conducting member, and a cold side coupled to at least one cooling fin, and wherein a second end of the heat conducting member is thermally coupled to the. process fluid.
17. The field device of claim 1, wherein the amount of electricity converted by the conversion module is used to provide a temperature indication related to the thermal source.
18. The field device of claim 1, wherein the thermal source is a process thermal source.
19. The field device of claim 1, and further comprising a power storage device coupled to the conversion module.
20. A method of providing electricity to a wireless field device, the method comprising:
thermally coupling a thermoelectric device to a source of thermal potential energy; and electrically coupling the thermoelectric device to a wireless communication module of the field device.
21. The method of claim 20, wherein thermally coupling the thermoelectric device includes conveying heat through the thermoelectric device.
22. A field device comprising:
a wireless communications module configured to wirelessly communicate process-related information with another device; and means for converting thermal potential energy in a process thermal source to electricity to power the field device.
CA2552615A 2004-03-02 2005-03-02 Process device with improved power generation Active CA2552615C (en)

Applications Claiming Priority (3)

Application Number Priority Date Filing Date Title
US54963704P 2004-03-02 2004-03-02
US60/549,637 2004-03-02
PCT/US2005/006596 WO2005086331A2 (en) 2004-03-02 2005-03-02 Process device with improved power generation

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CA2552615A1 true CA2552615A1 (en) 2005-09-15
CA2552615C CA2552615C (en) 2014-08-26

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EP (1) EP1721067B1 (en)
JP (1) JP5058785B2 (en)
CN (1) CN1954138B (en)
CA (1) CA2552615C (en)
DE (1) DE602005018749D1 (en)
RU (1) RU2347921C2 (en)
WO (1) WO2005086331A2 (en)

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