CN100392381C - Method for detecting combustion characteristic of coal by use of oxygen bomb method - Google Patents
Method for detecting combustion characteristic of coal by use of oxygen bomb method Download PDFInfo
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- CN100392381C CN100392381C CNB021385394A CN02138539A CN100392381C CN 100392381 C CN100392381 C CN 100392381C CN B021385394 A CNB021385394 A CN B021385394A CN 02138539 A CN02138539 A CN 02138539A CN 100392381 C CN100392381 C CN 100392381C
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- temperature rise
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- oxygen bomb
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Abstract
The present invention discloses a method for measuring coal burning characteristics by an oxygen bomb method. The heat productivity of coal is measured by the oxygen bomb method, and the heat productivity is fixed. The igniting characteristic and the burning-out rate are judged by the temperature rise condition. The present invention has the advantages of simple device, high speed, saving of power consumption, and simple operation.
Description
Described technical field
The invention belongs to coal analysis test, Thermal Power Engineering, be specifically related to a kind of assay method of coal burning characteristic.
Background technology
The coal burning characteristic generally is meant ignition propensity, burnout rate, and it is the important indicator whether certain coal of decision is fit to particular burner.In general, burner, as boiler, kiln, design is in case determine to have only and use the coal competence exertion high-level efficiency with corresponding combustion characteristics.
Coal combustion character is judged by thermogravimetric analysis in the laboratory, but thermogravimetric analyzer costs an arm and a leg, complicated operation, has only high-caliber university, research institute just to equip; The common vast combustion characteristics of judging coal with coal unit by the coal fugitive constituent indirectly, but fugitive constituent is a coal burning characteristic major influence factors, rather than unique influence factor, so the situation that do not conform to the actual conditions and close often appears in the conclusion that this determination methods draws.
Summary of the invention
The present invention is directed to the deficiency of above-mentioned combustion characteristics assay method, propose to utilize the bomb method principle to measure the method for combustion characteristics, have the advantages that equipment is simple, speed is fast, power consumption is little, simple to operate.
Concrete technical scheme of the present invention is: determine heating value of coal by the GB bomb method earlier, change again and claim that sample maintenance single test heating total amount is a steady state value, oxygenation pressure is 0.6~2.5MPa, press heat output determining method survey record igniting back temperature rise process again, judge the coal fire behaviour according to the early stage situation of temperature rise curve at last, judge the coal burnout rate according to back segment heating curve or residual ash, thus the combustion characteristics of drawing.
This method compared with the prior art, it is simple to have a test unit, test speed is fast, advantages such as little power consumption.
Description of drawings
Below in conjunction with drawings and Examples the present invention is described in further detail.
Fig. 1 is the temperature rise time plot of embodiment 1.
Embodiment
Embodiment 1
Get one group of coal, unified oven dry, pulverizing, sample preparation obtain≤coal dust of 0.2mm granularity; Place oxygen bomb heat instrument to measure its thermal value Qb each coal dust by standard conditions; At 4000 * 4.18KJ, calculate the various kinds quality of pc by the thermal value total amount; Reduce oxygenation pressure to 0.8MPa, place oxygen bomb heat instrument, determine Qb ' and temperature rise curve; The ignitability of this coal is judged in temperature rise during according to 1.5 minutes, according to φ
Q(=Qb '/Qb) judge the burning property of this coal.
Can judge burning property 5>4>3>2>1 according to last table φ, this is with identical according to the fugitive constituent inferred results; And according to Δ t
1.5Ignition propensity 5>3>4>2>1 can be judged, 3,4 order be paid special attention to, though No. 4 coal fugitive constituents are higher, its ash content height, so its ignition propensity descends, this and thermogravimetric analysis result coincide.
Embodiment 2
Get one group of coal, unified oven dry, pulverizing, sample preparation obtain≤coal dust of 0.2mm granularity; Place oxygen bomb heat instrument to measure its thermal value Qb each coal dust by standard conditions; At 4000 * 4.18KJ, calculate the various kinds quality of pc by the thermal value total amount; Reduce oxygenation pressure to 0.8MPa, place oxygen bomb heat instrument, determine temperature rise curve and do not fire ash content Aad ' entirely; The ignitability of this coal is judged in temperature rise during according to 1.5 minutes, according to φ
A{=(100-Aad ')/(100-A) } judge the burning property of this coal, A is for firing ash content fully.
Can judge ignition propensity 6<7<8 by last table; Easily burning property 6<7<8.
It is worthy of note that No. 8 φ appears in sample
A>1 situation no wonder is that ash content splashes and causes.
Claims (2)
1. method of utilizing bomb method to measure the coal burning characteristic, it is characterized in that: this method is carried out according to the following procedure:
(1) gets one group of coal, determine heating value of coal by the GB bomb method earlier;
(2) change the title sample, keeping single experiment heating total amount is steady state value;
(3) reduce oxygenation pressure and press heat output determining method survey record igniting back temperature rise process;
(4) judge the coal fire behaviour according to the early stage situation of temperature rise curve, according to back segment temperature rise curve or residual ash disconnected declare the coal burnout rate, thereby the combustion characteristics of drawing.
2. bomb method according to claim 1 is measured the method for coal burning characteristic, and the oxygenation pressure after it is characterized in that reducing in the step (3) is 0.6-2.5MPa.
Priority Applications (1)
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CNB021385394A CN100392381C (en) | 2002-11-06 | 2002-11-06 | Method for detecting combustion characteristic of coal by use of oxygen bomb method |
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CNB021385394A CN100392381C (en) | 2002-11-06 | 2002-11-06 | Method for detecting combustion characteristic of coal by use of oxygen bomb method |
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CN1415955A CN1415955A (en) | 2003-05-07 |
CN100392381C true CN100392381C (en) | 2008-06-04 |
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CNB021385394A Withdrawn - After Issue CN100392381C (en) | 2002-11-06 | 2002-11-06 | Method for detecting combustion characteristic of coal by use of oxygen bomb method |
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Families Citing this family (4)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN101762341B (en) * | 2009-12-28 | 2011-10-26 | 清华大学 | Method for measuring ignition temperature of solid fuel |
CN102207478A (en) * | 2011-03-11 | 2011-10-05 | 中国计量科学研究院 | Gas combustion heat measuring device and combustion heat measuring method utilizing the same |
CN104458805B (en) * | 2014-12-18 | 2017-01-18 | 广西大学 | Pulverized coal suspension combustion characteristic trial furnace for cement kiln |
CN105784767A (en) * | 2016-05-12 | 2016-07-20 | 本钢板材股份有限公司 | Method for measuring calorific value of high volatile coal |
Citations (3)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
US4616938A (en) * | 1983-01-10 | 1986-10-14 | Leco Corporation | Apparatus for measuring thermal and other quantities of substances |
US4720196A (en) * | 1985-06-18 | 1988-01-19 | Societe Nationale Elf Aquitaine (Production) | Method and apparatus for measuring the heating power of combustible gases |
JPH11295283A (en) * | 1998-03-04 | 1999-10-29 | Thermoquest Italia Spa | Method and device for analyzing element by instantaneous combustion in oxygen |
-
2002
- 2002-11-06 CN CNB021385394A patent/CN100392381C/en not_active Withdrawn - After Issue
Patent Citations (3)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
US4616938A (en) * | 1983-01-10 | 1986-10-14 | Leco Corporation | Apparatus for measuring thermal and other quantities of substances |
US4720196A (en) * | 1985-06-18 | 1988-01-19 | Societe Nationale Elf Aquitaine (Production) | Method and apparatus for measuring the heating power of combustible gases |
JPH11295283A (en) * | 1998-03-04 | 1999-10-29 | Thermoquest Italia Spa | Method and device for analyzing element by instantaneous combustion in oxygen |
Non-Patent Citations (2)
Title |
---|
混煤的着火特性分析. 周光华.浙江电力,第5期. 1995 * |
矿物组分对煤炭发热量的影响. 张洪等人.中国矿业大学学报,第27卷第3期. 1998 * |
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