CN101318843B - Glazing process for isostatic compaction of ceramic base substrate - Google Patents
Glazing process for isostatic compaction of ceramic base substrate Download PDFInfo
- Publication number
- CN101318843B CN101318843B CN2008101071085A CN200810107108A CN101318843B CN 101318843 B CN101318843 B CN 101318843B CN 2008101071085 A CN2008101071085 A CN 2008101071085A CN 200810107108 A CN200810107108 A CN 200810107108A CN 101318843 B CN101318843 B CN 101318843B
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- ceramic
- coat enamel
- glaze
- rough body
- isostatic compaction
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Abstract
The invention proposes a glazing process method for an isostatic compaction ceramic rough body. The method comprises the following steps that: firstly a high polymer solution layer is formed on the ceramic rough body having undergone bisque firing at a temperature of between 900 and 1000 DEG C through impregnation, and a multi-orifice high polymer micropore film formed on the surface of the dried rough body can serve as a screen to prevent solid particles in a slurry from entering the pores of the rough body without impacting the slurry absorption performance of the rough body; then a layer of base coat and overglaze is applied to the rough body to obtain a smooth and flat glaze after high-temperature burning. The method solves the problem of easy production of a glaze hole defect lying in isostatic compaction ceramic products.
Description
Technical field
The invention belongs to the traditional ceramics manufacturing technology, be specifically related to a kind of glazing process that is used for isostatic compaction of ceramic base substrate
Background technology
When adopting isostatic pressing method to prepare ceramic product, in order to improve the flowability of powder, blank must pass through mist projection granulating, and final resulting blank is the spheric coacervate, and its particle size is bigger.This blank is through behind the isostatic pressing, and compacting fully between the spheroidal particle causes the coarse injustice of base substrate of moulding, and there is a large amount of pits in the surface.During glazing, glaze slip is easy to penetrate in the pit that forms between spheroidal particle, very easily makes glaze a lot of small holes occur on this base substrate.Though these glaze small holes size in sintering process reduces to some extent, can not make up fully, cause ceramic product still to be covered with a large amount of pin holes burning till the back glaze, glaze glossiness variation has a strong impact on the quality and the class of ceramic product.Adopt traditional glazing process,,, still can't fundamentally solve the difficult problem of the ceramic product glaze quality difference of isostatic pressing though glaze quality is made moderate progress by improving glaze formula.
Summary of the invention
The objective of the invention is to propose a kind of new glazing process that is used for isostatic compaction of ceramic base substrate, can solve the difficult problem that the isostatic pressing ceramic product very easily produces the glaze needle pore defect effectively.
A kind of glazing process that is used for isostatic compaction of ceramic base substrate that the present invention proposes is characterized in that: earlier through 900 ℃~1000 ℃ unglazed ceramic body surface impregnation high molecular polymer aqueous solution, execute ground-coat enamel after the drying, execute cover-coat enamel after the drying again.Described high molecular polymer is so long as can get final product at the high molecular polymer that billet surface forms one deck micropore organic film.
Above-mentioned high molecular polymer preferably carboxymethyl cellulose sodium (CMC) or polyvinyl alcohol (PVA), the preferred 0.1wt%~2.0wt% of base substrate impregnation concentration; The fineness requirement of described ground-coat enamel and cover-coat enamel is preferably: ground-coat enamel was 100 mesh sieve screen over-size 0.2wt%~0.5wt%, and cover-coat enamel was 250 mesh sieve screen over-size 0.02wt%~0.05wt%.
Key problem in technology of the present invention and innovation are at first at dipping one deck macromolecule polymer solution on 900 ℃~1000 ℃ unglazed ceramic bodies, dry back billet surface just forms one deck high molecular polymer microporous membrane, it plays the effect of screen cloth, can stop the solid particulate in the glaze slip to enter into the base substrate hole, thereby effectively avoid glaze to produce small holes.Can form the glaze layer of even compact when making glazing, burn till the back and just can obtain the smooth smooth ceramic product of glaze.Because the high molecular polymer film is a microporous membrane, it can be permeable, so it can not influence the suction slurry performance of base substrate again.
Another innovation part of the present invention is the thicker ground-coat enamel of first last layer particle before the glaze in the above, can prevent better that like this glaze slip fine particle from infiltrating in the base substrate hole, guarantee cover-coat enamel surface even compact and small holes can not occur, help burning the back and form smooth smooth glaze.
Embodiment
Embodiment one
Compound concentration is the CMC aqueous solution of 0.1wt%, will through 920 ℃ of biscuitings 6 " ceramic disc immerses and wherein to take out after 8 seconds; in 70 ℃ baking oven dry 20 minutes; again this ceramic disc being immersed concentration is 50wt%; fineness was that 100 mesh sieve screen over-sizes are about 5 seconds in the ceramic bottom glaze slip of 0.2wt%; take out the back in 60 ℃ baking oven dry 30 minutes; again this dish being immersed concentration afterwards is 40wt%, fineness was that 250 mesh sieve screen over-sizes are about 2 seconds in the ceramic plane glaze slip of 0.02wt%, after the taking-up, firing process routinely burns till again, and the ceramic disc glaze of acquisition is smooth smooth, no pin-hole defect.
Embodiment two
Compound concentration is the CMC aqueous solution of 0.8wt%, will through 960 ℃ of biscuitings 6 " ceramic disc immerses and wherein to take out after 4 seconds; in 70 ℃ baking oven dry 25 minutes; again this ceramic disc being immersed concentration is 50wt%; fineness was that 100 mesh sieve screen over-sizes are about 5 seconds in the ceramic bottom glaze slip of 0.5wt%; take out the back in 60 ℃ baking oven dry 30 minutes; again this dish being immersed concentration afterwards is 40wt%, fineness was that 250 mesh sieve screen over-sizes are about 2 seconds in the ceramic plane glaze slip of 0.05wt%, after the taking-up, firing process routinely burns till again, and the ceramic disc glaze of acquisition is smooth smooth, no pin-hole defect.
Embodiment three
Compound concentration is the PVA aqueous solution of 2.0wt%, will through 1000 ℃ of biscuitings 6 " ceramic disc immerses and wherein to take out after 8 seconds; in 70 ℃ baking oven dry 20 minutes; again this ceramic disc being immersed concentration is 50wt%; fineness was that 100 mesh sieve screen over-sizes are about 5 seconds in the ceramic bottom glaze slip of 0.4wt%; take out the back in 60 ℃ baking oven dry 30 minutes; again this dish being immersed concentration afterwards is 40wt%, fineness was that 250 mesh sieve screen over-sizes are about 2 seconds in the ceramic plane glaze slip of 0.03wt%, after the taking-up, firing process routinely burns till again, and the ceramic disc glaze of acquisition is smooth smooth, no pin-hole defect.
Claims (2)
1. a glazing process that is used for isostatic compaction of ceramic base substrate is characterized in that: earlier through 900 ℃~1000 ℃ unglazed ceramic body surface impregnation high molecular polymer aqueous solution, execute ground-coat enamel after the drying, execute cover-coat enamel after the drying again; Can form one deck micropore organic film in billet surface behind the wherein said high molecular polymer aqueous solution dipping; Described high molecular polymer is Xylo-Mucine or polyvinyl alcohol, and macromolecule polymer solution concentration is 0.1wt%~2.0wt%.
2. glazing process according to claim 1 is characterized in that the fineness requirement of described ground-coat enamel and cover-coat enamel is respectively: ground-coat enamel was that 100 mesh sieve screen over-sizes are 0.2wt%~0.5wt%, and cover-coat enamel was that 250 mesh sieve screen over-sizes are 0.02wt%~0.05wt%.
Priority Applications (1)
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CN2008101071085A CN101318843B (en) | 2008-07-11 | 2008-07-11 | Glazing process for isostatic compaction of ceramic base substrate |
Applications Claiming Priority (1)
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CN2008101071085A CN101318843B (en) | 2008-07-11 | 2008-07-11 | Glazing process for isostatic compaction of ceramic base substrate |
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CN101318843A CN101318843A (en) | 2008-12-10 |
CN101318843B true CN101318843B (en) | 2011-10-05 |
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CN2008101071085A Expired - Fee Related CN101318843B (en) | 2008-07-11 | 2008-07-11 | Glazing process for isostatic compaction of ceramic base substrate |
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Families Citing this family (3)
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CN111995367A (en) * | 2020-08-24 | 2020-11-27 | 德化东华陶瓷有限公司 | Wear-resistant weather-resistant household ceramic product prepared from waste ceramic material and preparation method thereof |
CN114621001A (en) * | 2022-03-31 | 2022-06-14 | 江西省康舒陶瓷股份有限公司 | Far infrared fine ceramic cooking device |
CN115488337B (en) * | 2022-09-27 | 2023-04-18 | 株洲东亚工具有限公司 | Isostatic pressing processing assembly for preparing sand-making wear-resistant strips |
Citations (5)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN87106477A (en) * | 1987-09-18 | 1988-07-27 | 北流县第二瓷厂 | Glazing method of facing brick |
US5458943A (en) * | 1990-11-05 | 1995-10-17 | Taylor; Donald M. | Spiral spacer |
CN1187476A (en) * | 1997-01-10 | 1998-07-15 | 淄博常鑫建筑陶瓷有限公司 | Fast-firing technique for coal gangue wall bricks and floor tiles |
CN1693273A (en) * | 2005-04-01 | 2005-11-09 | 邢宪生 | Process for improving glaze effect and function of ceramics products |
CN101182244A (en) * | 2007-11-25 | 2008-05-21 | 宜兴金帆陶瓷有限公司 | Method for preparing glaze ceramic wine bottle with body-hidden bottom |
-
2008
- 2008-07-11 CN CN2008101071085A patent/CN101318843B/en not_active Expired - Fee Related
Patent Citations (5)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN87106477A (en) * | 1987-09-18 | 1988-07-27 | 北流县第二瓷厂 | Glazing method of facing brick |
US5458943A (en) * | 1990-11-05 | 1995-10-17 | Taylor; Donald M. | Spiral spacer |
CN1187476A (en) * | 1997-01-10 | 1998-07-15 | 淄博常鑫建筑陶瓷有限公司 | Fast-firing technique for coal gangue wall bricks and floor tiles |
CN1693273A (en) * | 2005-04-01 | 2005-11-09 | 邢宪生 | Process for improving glaze effect and function of ceramics products |
CN101182244A (en) * | 2007-11-25 | 2008-05-21 | 宜兴金帆陶瓷有限公司 | Method for preparing glaze ceramic wine bottle with body-hidden bottom |
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Address after: 333001 Jiangxi province Jingdezhen City Tao Yang Road, Jingdezhen Ceramic Institute Patentee after: JINGDEZHEN CERAMIC INSTITUTE Address before: 333001 Jiangxi province Jingdezhen City Tao Yang Road, Jingdezhen Ceramic Institute Patentee before: Jingdezhen College of Ceramic Industry |
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