CN104529410A - Ceramic body with low expansion coefficient, and production method thereof - Google Patents

Ceramic body with low expansion coefficient, and production method thereof Download PDF

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Publication number
CN104529410A
CN104529410A CN201410731863.6A CN201410731863A CN104529410A CN 104529410 A CN104529410 A CN 104529410A CN 201410731863 A CN201410731863 A CN 201410731863A CN 104529410 A CN104529410 A CN 104529410A
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China
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parts
ceramic body
expansion coefficient
low
preparation
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CN201410731863.6A
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Chinese (zh)
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成延栓
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Individual
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Individual
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Priority to CN201410731863.6A priority Critical patent/CN104529410A/en
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Abstract

The invention relates to a ceramic body with a low expansion coefficient. The ceramic body comprises, by weight, 5-8 parts of LiO2, 8-11 parts of K2O, 25-27 parts of Al2O3, 41-49 parts of SiO2, 2-3 parts of TiO2, 2-5 parts of Na2O, 15-19 parts of ZnO, 15-18 parts of CaO, 4-5 parts of MgO, and 1-2 parts of Fe2O3. The ceramic body obtained in the invention has a low expansion coefficient, can well adapt to other products, has no cracking problem, and facilitates popularization application.

Description

Low-expansion coefficient ceramic body and preparation method thereof
Technical field
The present invention relates to ceramic technology field, more specifically, relate to a kind of low-expansion coefficient ceramic body and preparation method thereof.
Background technology
The coefficient of expansion is very important with application to the production of stupalith, as glazing on ceramic body, if the coefficient of expansion of ceramic body and glaze cannot adapt to, product just can be caused to ftracture, therefore must regulate the coefficient of expansion of ceramic body, more adapt to allow it.And the coefficient of expansion factor affecting ceramic body is a lot, as starting material composition, firing process etc.
Summary of the invention
The object of this invention is to provide a kind of low-expansion coefficient ceramic body.
Another object of the present invention is to provide a kind of preparation method of described low-expansion coefficient ceramic body.
The object of the invention is achieved by the following technical programs:
A kind of low-expansion coefficient ceramic body is provided, is made up of each component of following weight fraction: LiO 25 ~ 8 parts, K 2o 8 ~ 11 parts, Al 2o 325 ~ 27 parts, SiO 241 ~ 49 parts, TiO 22 ~ 3 parts, Na 2o 2 ~ 5 parts, ZnO 15 ~ 19 parts, CaO 15 ~ 18 parts, MgO 4 ~ 5 parts, Fe 2o 31 ~ 2 part.
Preferably, described low-expansion coefficient ceramic body is made up of each component of following weight fraction: LiO 27 parts, K 2o 9 parts, Al 2o 326 parts, SiO 245 parts, TiO 22 parts, Na 2o 4 parts, ZnO 18 parts, CaO 16 parts, MgO 5 parts, Fe 2o 32 parts.
Present invention also offers the preparation method of described low-expansion coefficient ceramic body, comprise the following steps:
S1. raw material is got by weight ratio, with ball: water: it is that 300 mesh sieves tail over 0.5 ~ 0.6% that the ratio goal barreling of material=2:0.75:1 is milled to fineness, is sieved by grinding gained slurry iron-removing, puts into suction pit old 5 days, for subsequent use;
S2. be blank by mud injection forming obtained by S1;
S3. the blank after injection forming enters kiln oxydizing flame and burns till.
Preferably, the firing temperature described in S3 is 1350 ~ 1380 DEG C.
Preferably, the firing time described in S3 is 9 ~ 12 hours.
Compared with prior art, the present invention has following beneficial effect:
The invention provides a kind of low-expansion coefficient ceramic body, its coefficient of expansion is low, can be applied to better on other products.
Embodiment
Below in conjunction with specific embodiment, the present invention is further illustrated.
Embodiment 1
Present embodiment discloses a kind of low-expansion coefficient ceramic body, be made up of each component of following weight fraction: LiO 27 parts, K 2o 9 parts, Al 2o 326 parts, SiO 245 parts, TiO 22 parts, Na 2o 4 parts, ZnO 18 parts, CaO 16 parts, MgO 5 parts, Fe 2o 32 parts.
Embodiment 2
Present embodiment discloses a kind of low-expansion coefficient ceramic body, be made up of each component of following weight fraction: LiO 25 parts, K 2o 8 parts, Al 2o 325 parts, SiO 241 parts, TiO 23 parts, Na 2o 2 parts, ZnO 15 parts, CaO 15 parts, MgO 4 parts, Fe 2o 31 part.
Embodiment 3
Present embodiment discloses a kind of low-expansion coefficient ceramic body, be made up of each component of following weight fraction: LiO 28 parts, K 2o 11 parts, Al 2o 327 parts, SiO 249 parts, TiO 22.8 parts, Na 2o 5 parts, ZnO 19 parts, CaO 18 parts, MgO 5 parts, Fe 2o 31.8 part.
Embodiment 4
Present embodiment discloses a kind of low-expansion coefficient ceramic body, be made up of each component of following weight fraction: LiO 26 parts, K 2o 10 parts, Al 2o 326 parts, SiO 247 parts, TiO 22.8 parts, Na 2o 3 parts, ZnO 16 parts, CaO 17 parts, MgO 4.5 parts, Fe 2o 31.5 part.
Embodiment 5
The components by weight percent of Example 1 ~ 4 any embodiment prepares low-expansion coefficient ceramic body, and preparation process is as follows:
S1. raw material is got by weight ratio, with ball: water: it is that 300 mesh sieves tail over 0.5% that the ratio goal barreling of material=2:0.75:1 is milled to fineness, is sieved by grinding gained slurry iron-removing, puts into suction pit old 5 days, for subsequent use;
S2. be blank by mud injection forming obtained by S1;
S3. the blank after injection forming enters kiln oxydizing flame and burns till, and firing temperature is 1350 DEG C, and firing time is 9 hours.
The coefficient of expansion of gained ceramic body is 4.5 × 10 -6/ DEG C, because the coefficient of expansion is low, better can adapt to other products, as also not easily caused cracking in its surperficial glazing.
Embodiment 6
The components by weight percent of Example 1 ~ 4 any embodiment prepares low-expansion coefficient ceramic body, and preparation process is as follows:
S1. raw material is got by weight ratio, with ball: water: it is that 300 mesh sieves tail over 0.6% that the ratio goal barreling of material=2:0.75:1 is milled to fineness, is sieved by grinding gained slurry iron-removing, puts into suction pit old 5 days, for subsequent use;
S2. be blank by mud injection forming obtained by S1;
S3. the blank after injection forming enters kiln oxydizing flame and burns till, and firing temperature is 1380 DEG C, and firing time is 12 hours.
The coefficient of expansion of gained ceramic body is 4.37 × 10 -6/ DEG C, because the coefficient of expansion is low, better can adapt to other products, as also not easily caused cracking in its surperficial glazing.
Embodiment 7
The components by weight percent of Example 1 ~ 4 any embodiment prepares low-expansion coefficient ceramic body, and preparation process is as follows:
S1. raw material is got by weight ratio, with ball: water: it is that 300 mesh sieves tail over 0.6% that the ratio goal barreling of material=2:0.75:1 is milled to fineness, is sieved by grinding gained slurry iron-removing, puts into suction pit old 5 days, for subsequent use;
S2. be blank by mud injection forming obtained by S1;
S3. the blank after injection forming enters kiln oxydizing flame and burns till, and firing temperature is 1350 DEG C, and firing time is 10 hours.
The coefficient of expansion of gained ceramic body is 4.15 × 10 -6/ DEG C, because the coefficient of expansion is low, better can adapt to other products, as also not easily caused cracking in its surperficial glazing.

Claims (5)

1. a low-expansion coefficient ceramic body, is characterized in that, is made up of: LiO each component of following weight fraction 25 ~ 8 parts, K 2o 8 ~ 11 parts, Al 2o 325 ~ 27 parts, SiO 241 ~ 49 parts, TiO 22 ~ 3 parts, Na 2o 2 ~ 5 parts, ZnO 15 ~ 19 parts, CaO 15 ~ 18 parts, MgO 4 ~ 5 parts, Fe 2o 31 ~ 2 part.
2. low-expansion coefficient ceramic body according to claim 1, is characterized in that, is made up of: LiO each component of following weight fraction 27 parts, K 2o 9 parts, Al 2o 326 parts, SiO 245 parts, TiO 22 parts, Na 2o 4 parts, ZnO 18 parts, CaO 16 parts, MgO 5 parts, Fe 2o 32 parts.
3. the preparation method of low-expansion coefficient ceramic body according to claim 1 or 2, is characterized in that, comprise the following steps:
S1. raw material is got by weight ratio, with ball: water: it is that 300 mesh sieves tail over 0.5 ~ 0.6% that the ratio goal barreling of material=2:0.75:1 is milled to fineness, is sieved by grinding gained slurry iron-removing, puts into suction pit old 5 days, for subsequent use;
S2. be blank by mud injection forming obtained by S1;
S3. the blank after injection forming enters kiln oxydizing flame and burns till.
4. preparation method according to claim 3, is characterized in that, the firing temperature described in S3 is 1350 ~ 1380 DEG C.
5. preparation method according to claim 3, is characterized in that, the firing time described in S3 is 9 ~ 12 hours.
CN201410731863.6A 2014-12-06 2014-12-06 Ceramic body with low expansion coefficient, and production method thereof Pending CN104529410A (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
CN201410731863.6A CN104529410A (en) 2014-12-06 2014-12-06 Ceramic body with low expansion coefficient, and production method thereof

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
CN201410731863.6A CN104529410A (en) 2014-12-06 2014-12-06 Ceramic body with low expansion coefficient, and production method thereof

Publications (1)

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CN104529410A true CN104529410A (en) 2015-04-22

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Citations (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN1094269A (en) * 1993-04-26 1994-11-02 张文池 A kind of cooking white sand pot of tool high thermal stability
US5614330A (en) * 1995-08-18 1997-03-25 American Thermocraft Corporation Porcelain coating compositions for low expansion porcelain cores and the resulting all-ceramic dental restorations
CN1253125A (en) * 1999-11-08 2000-05-17 苏君道 Non-expansion lithium ceramics and process for preparing its crucible
JP2013155100A (en) * 2012-01-31 2013-08-15 Sumitomo Chemical Co Ltd Green honeycomb formed body, production method of green honeycomb formed body, and production method of honeycomb fired body

Patent Citations (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN1094269A (en) * 1993-04-26 1994-11-02 张文池 A kind of cooking white sand pot of tool high thermal stability
US5614330A (en) * 1995-08-18 1997-03-25 American Thermocraft Corporation Porcelain coating compositions for low expansion porcelain cores and the resulting all-ceramic dental restorations
CN1253125A (en) * 1999-11-08 2000-05-17 苏君道 Non-expansion lithium ceramics and process for preparing its crucible
JP2013155100A (en) * 2012-01-31 2013-08-15 Sumitomo Chemical Co Ltd Green honeycomb formed body, production method of green honeycomb formed body, and production method of honeycomb fired body

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Application publication date: 20150422