CN1264278A - 用作清洁片的三维结构 - Google Patents
用作清洁片的三维结构 Download PDFInfo
- Publication number
- CN1264278A CN1264278A CN98807385A CN98807385A CN1264278A CN 1264278 A CN1264278 A CN 1264278A CN 98807385 A CN98807385 A CN 98807385A CN 98807385 A CN98807385 A CN 98807385A CN 1264278 A CN1264278 A CN 1264278A
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- CN
- China
- Prior art keywords
- cleaning foil
- cleaning
- peak
- foil
- layer
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
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- Y10T442/668—Separate nonwoven fabric layers comprise chemically different strand or fiber material
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- Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
- Y10—TECHNICAL SUBJECTS COVERED BY FORMER USPC
- Y10T—TECHNICAL SUBJECTS COVERED BY FORMER US CLASSIFICATION
- Y10T442/00—Fabric [woven, knitted, or nonwoven textile or cloth, etc.]
- Y10T442/60—Nonwoven fabric [i.e., nonwoven strand or fiber material]
- Y10T442/689—Hydroentangled nonwoven fabric
Abstract
公开了具有大体上为宏观三维度的清洁片。可供选择地,宏观三维清洁片可包括一种可收缩的材料(例如,一种纱布材料(scrimmaterial),这种材料在加热和随后冷却时产生收缩,从而提供一种宏观三维结构。宏观三维度用“平均的峰—到—峰的距离”和“表面构形指数”以及用“平均高度差”描述。还公开了清洁工具,该工具包括一个手柄和所说的清洁片。还公开了清洁片的制作方法,该方法的益处,以及所制造的制品。
Description
发明领域
本发明涉及特别适合去除和夹带灰尘,棉绒,头发,沙,食物碎屑,草等等的清洁片。
发明背景
在已有技术中用无纺片清理干的灰尘类是众所周知的。这种片通常使用一种纤维的复合物,其中纤维是用粘合,缠结或其它强制力粘接起来的。例如,可见于美国专利第3,629,047号和美国专利第5,144,729号。为得到一种耐久的擦试片,采用了与连续的长丝或网状结构形式的人造短纤维相结合的方式的加强方法。例如,可见于美国专利第4,808,467号,美国专利第3,494,821号和美国专利第4,144,370号。同样,为提供一种能够耐受抹擦过程的酷烈,在已有的无纺片上曾使用上述的一种或多种强制力强力地粘接纤维。在得到耐用材料的同时,这种强力粘接可能不利地影响材料的拾取和留住颗粒污物的能力。在致力于这一方面的努力中,授予Shizuno等人的美国专利第5,525,397号描述了一种包括一个聚合物网状层和至少一个无纺层的清洁片,其中两层轻度地水缠结(hydroentangled)以提供一种低缠结系数的清洁片。所得片材被认为具有强度和耐久性,同时由于复合纤维是轻度水缠结的而改善了采集灰尘的性能。具有低缠结系数(即,不大于500m)的片材被认为可以提供较好的清洁效能,因为纤维在很大程度上是能够和污物相接触的。
虽然据称’397号专利所述的片材解决了已有无纺清洁片的某些问题,那些片材通常可视作均匀单位重量的,至少是在宏观的水平上;和基本上均匀的厚度,同样也是在宏观的水平上。即,作为水缠结时液体压力差异的后果,正常的和预期的单位重量和厚度的波动和变化是在随机的基础上发生的。但是,不会认为其结构含有单位重量不同的分离的区域。例如,在微观的水平上,如果测量纤维间缝隙的单位重量,将会得到明显的零单位重量,事实上,除非在无纺结构的一个孔上进行测量,这种区域的单位重量是大于零的。这种波动和变化是水缠结工艺的正常的和预期的结果。熟练的技工会理解无纺织物,包括在专利’397中描述的那些,具有这种变化,从宏观的概念上讲基本上具有均匀的单位重量和厚度。具有均匀单位重量片材意味着材料不特别适合于采集和夹带各种大小,形状,等等的污物。
因此,仍然需要提供一种能改善污物清除效能的清洁片。在这一方面,本申请人发现通过增加清洁片在宏观概念上的三维度,即可达到增强去除污物的效果。
于是,本发明的一个目的是要克服已有技术中的问题和特别是提供一种更能去除和夹带不同类型污物的结构。特别是,本发明的一个目的是要提供一种具有明显的三维度的无纺结构,下面将予详细地说明。
另一个目的是要为清洁片的消费者和使用者提供改善的清洁操作和所需的益处,特别是通过清洁片的组装,或是组装成带有用以分开清洁片的孔洞的卷形,或者带有将清洁片分成所需长度的装置,并将其包装成箱,箱上应告知消费者改善的操作和/或可获得的好处,特别是那些对消费者在直觉上不明显的好处。另一个目的是要为清洁片提供添加物,特别是对将污物粘结在基片上有所改善的那些,和特别为以下将予描述的那些清洁片提供三维结构,这些组合具有特殊的操作上的优点,同时这些组合提供了改进的益处。
发明概述
本发明涉及一种大体上具有宏观三维度的清洁片。如这里在描述三维清洁片时所使用的,术语“宏观三维度”意为在观察者的眼睛和清洁片平面之间的垂直距离约为12英寸时用肉眼可以很容易地看出的三维的式样。换句话说,本发明的三维结构为非平面的清洁片,其中清洁片的一面或两面以多面的形式存在,这些面之间的距离在距结构约12英寸处观察时可以用肉眼看出来的。与此相反,术语“平面的”指的是清洁片在一侧或两侧具有微小程度的表面像差(aberration),在观察者的眼睛和网平面之间的垂直距离约为12英寸或更大时很难用肉眼看出表面的像差。换句话说,从宏观规模来讲,观察者在清洁片的一个或两个表面看不到致使其成为三维的多面的存在。
本发明的宏观三维结构可选择地由一种纱布材料(scrimmaterial)制成,该材料在加热并随后冷却时收缩从而提供了一种宏观的三维结构。其它可提供收缩力从而产生三维度的材料将在下面予以讨论。宏观三维度在这里被表示为术语“平均高度差”,该术语在这里定义为清洁片的一个给定表面上相邻的峰和谷之间的平均距离,以及“平均的峰-到-峰的距离”,即一个给定表面的相邻的峰之间的平均距离。宏观三维度还用术语清洁片外表面的“表面构形指数”描述;表面构形指数为表面的平均高度差除以表面的平均的峰-到-峰的距离所得的比值。在一个实施例中,清洁片的两个外表面都具有所描述的平均的峰-到-峰的距离和表面构形性质。平均的峰-到-峰的距离和平均高度差的测量方法将在下面的试验方法中详细介绍。
至少一个外表面的平均的峰-到-峰的距离至少约为1mm,较优选地至少约为2mm,和更为优选地至少约为3mm。在一个实施例中,平均的峰-到-峰的距离由约1到约20mm,特别是由约3到约16mm,更特别地由约4到约12mm。至少一个外表面的表面构形指数由约0.01到约10,优选地由约0.1到约5,更为优选地由约0.2到约3,再更为优选地由约0.3到约2。而平均高度差的值不是关键性的,至少一个外表面所具有的平均高度差优选地至少约为0.5mm,更为优选地至少约1mm,和再更为优选地至少约1.5mm。至少一个外表面的平均高度差通常为由约0.5到约6mm,更为典型地由约1到约3mm。
本发明的清洁片和类似的清洁片,特别是那些如在这里所描述的在低水平上含有添加物的,和特别是其上的添加物基本上均匀地附着在至少一个连续的面积上的那些清洁片,可用于改善的清洁方法并为清洁片的消费者和使用者提供所需的益处,其中的某些益处如下面所详述的消费者在直觉上是不明显的。因此需要将清洁片包装成或是带有用以帮助分开清洁片的孔洞的卷形,或者带有将清洁片分成所需长度的装置,和/或将其包装成包,包上应告知消费者改善的方法和/或可获得的好处,特别是那些对消费者在直觉上不明显的好处。清洁片和添加物,包括那些至少在一个或更多区域上带有低水平的优选地大体上均匀地附着的添加物,组合地提供特殊的性能益处,这种组合还可提供改善的益处,特别是在清洁片具有这里提出的所需的结构的情况下。
附图简述
图1为一平面视图,示意说明本发明清洁片的一个三层的实施例,其中第二层包括一种带有沿着与清洁片侧边和端部边缘平行延伸的长丝的纱布材料,其中所示第一层的一部分被切除,同时为清晰起见略去了其中的第一层的表面特性。
图2为图1所示类型的本发明的另一个实施例的图示说明,其中第二层的长丝相对于清洁片的侧边和端部边缘倾斜一个约45度的角度。
图3为一平面图,为表示第一层宏观三维外表面的织地的照片图5的示意说明,特别是在第一层外表面上延伸的脊线。
图4为沿平行第二层的一根长丝所截取的清洁片的截面图,并示出长丝沿长丝交点中间延伸的部分,长丝的该部分并未粘结在第一层上,以及长丝沿长丝交点中间延伸的部分并未粘结在第三层上。
图5为表示第一层宏观三维表面的织地的显微照片,特别是表面的延伸的脊线。图5中的尺度为英寸。
图6为放大的图5中所示类型的显微照片,表示延伸的脊线具有沿不同方向延伸的分叉。
图7为扫描电子显微照片,提供了第一层宏观三维表面的透视图。
图8为清洁片截面的扫描电子显微照片,表示长丝沿长丝交点中间延伸的部分,长丝的该部分并未粘结在第一层上。
图9为一扫描电子显微照片,表示第一层和第三层在长丝交点处与第二层相粘结。
发明详述
I.定义
如在这里所使用的,术语“包括”意味着在实施本发明时各种部件,成分,或步骤可以共同使用。因此,术语“包括”含有更具限制性的术语“基本上由....组成”和“由....组成”。
如在这里所使用的,术语“水缠结”通常意味着一种制做一种材料的工艺,其中,一层松散的纤维材料(例如,聚酯)放在一个有孔的构图部件上并承受足够大的水压差使单独的纤维机械地缠结以形成织物。有孔的构图部件可以由,例如,织物网,穿孔的金属板,等等做成。
如在这里所使用的,术语“Z-维”指的是垂直于本发明的清洁片长和宽或其组成部分的维度。Z-维通常相应于清洁片的厚度。
如在这里所使用的,术语“X-Y维”指的是垂直于清洁片厚度或其组成部分的平面。X和Y维通常分别相应于清洁片或清洁片部件的长和宽。
如在这里所使用的,术语“层”指的是主要维度为X-Y,即沿其长和宽的清洁片的构件或部件。应该理解,术语层不必限定于材料的单一的层或片。因此,层可以包括叠层片或所需类型材料的几个片或织物的组合。于是,术语“层”包括术语“多层”和“成层的”。
为了本发明的目的,清洁片的“上”层为相对地更为远离待清洁的表面(即,就工具来讲,在使用时相对地靠近工具的把手)。术语“下”层相反地意为清洁片的相对地靠近待清洁表面的一层(即,就工具来讲,在使用时相对地更为远离工具把手)。
除特殊说明者外,这里所使用的所有百分比,比值和比例都是以重量计算的。
II.清洁片
本发明涉及适用于由各种表面上去除灰尘,棉绒,头发,草,沙,食物碎屑,和其它各种大小,形状,稠度等等物质的清洁片。优选地,这种清洁片在消费者专门小组试验中将显示出改善的清洁性能。
作为该清洁片由表面以及空气以不同的方式,包括接触和夹带,减少或消除灰尘,棉绒和其它物质的能力的结果,该清洁片在相似的清洁目的上相对于其它制品和实际操作将会对表面上和大气里的这些物质形成更高水平的减少。这一能力在清洁片含有如在这里所描述的添加物时特别明显。甚至在此前引入的美国专利第5,525,397号中的清洁片也能提供这种益处,虽然和这里的优选的结构相比其程度是较小的,因此,在包装上,或与包装一起提供这一信息是重要的,用以鼓励使用清洁片,包括’397专利中所说的那些清洁片,特别是用在非-传统的表面如墙壁,天花板,室内饰品,幕布,地毯,衣服,等等,在这些地方通常没有使用过除尘清洁片。低含量添加物的使用,即使用均匀地附着在清洁片的至少一个,优选地在其连续的区域上的有效数量的低水平的添加物,以改善对污物特别是颗粒污物和尤其是那些引起过敏反应的颗粒污物的粘结,对粘结污物的控制达到了惊人的程度。在使用清洁片时,至少在清洁片上的那些有添加物存在的区域,为此而使用的低水平是重要的,因为,和油作为流体或喷雾施加的传统的除尘操作不同,极少有形成可视的油斑的危险,特别是在那些非-传统的表面上。优选的结构通过收集较大颗粒而不是将其研磨成较小的尺寸也提供了好处。
过敏反应的消费者将由使用这里的清洁片,特别是其优选的结构,而特别地受益,因为过敏源通常以灰尘的形式存在和特别需要减少可吸入的小颗粒的水平。为了这一效果,在污物变得明显可视时,在常规的基础上使用清洁片而不是按已有技术的方式是重要的。
本发明的清洁片可以利用纺织或无纺的方法制造,或者通过使用溶化的材料在模板上铺展的成形操作,特别是在带中,和/或通过对薄膜进行的包括机械作用/改性的成形操作。可以使用任意的数种方法制作结构,只要基本的三维的需要能够被辨别出来。无论如何,优选的结构是无纺的,特别是那些在本领域中所周知的用水缠结制作的,因为它们提供了高度理想的疏松的结构。因此,这里所使用的优选的清洁片是具有这里所描述的特性的无纺结构。特别适合于制作本发明优选的无纺清洁片的材料包括,例如,天然的纤维素以及合成纤维材料如聚烯烃类(例如,聚乙烯和聚丙烯),聚酯,聚酰胺,合成纤维素(例如,RAYON),及其掺合物。同样适用的是天然纤维,如棉花或其混合物和那些由各种纤维素源得出的纤维。用于制作本发明的水缠结纤维性清洁片的优选的原始材料为合成材料,这些材料的形式可以是梳通的,纺丝粘结的,溶喷的,气敷设的,或其它的结构形式。特别优选的是聚酯,尤其是梳通的聚酯纤维。纤维的疏水性或亲水性程度的最佳选择依赖于清洁片所期望的目的,依据待清除的污物的类型,有添加物存在时依据所提供的添加物类型,生物可降解性,可用性,等这些考虑中的一个及其综合。一般来说,比较生物可降解的材料是亲水的,但更为有效的材料往往是疏水的。
清洁片可以由一个单个的纤维层形成,但优选地为至少两个单独的层形成的复合物。优选地,清洁片为用水缠结的方法制作的无纺织物。在这方面,在用水缠结纤维的个别层之前,在用缠结联结各层之前须对每一层进行轻度地缠结。
在本发明的一个特别的优选实施例中,为增强所得清洁片的整体性,优选地包括一个和纤维性材料配置在一起的聚合物网(这里指的是一种“纱布”材料),例如,通过加热或化学的方法如粘结,水缠结,等等,构成层状结构。这里所使用的纱布材料在美国专利第4,636,419号中有详细的描述,在这里将其引入作为参考。纱布材料可以直接地由挤压模形成,或者通过原纤维形成作用或模压加工接着进行张拉和分裂由挤压膜得出。纱布可以取自聚烯烃类如聚乙烯或聚丙烯,或其共聚物,聚对苯二甲酸丁二醇酯,聚对苯二甲酸乙二醇酯,尼龙6,尼龙66,等等。纱布材料可由各种商业来源购得。适于本发明使用的优选纱布材料为聚丙烯纱布,可由Conwed Plastics(Minneapolis,MN)购得。
在本发明的另一方面,本申请人还发现在清洁片中加入纱布材料随即进行加热形成了清洁片的宏观三维特性。已经发现这种宏观的三维度极大地增强了清洁片的清洁效能,尽管清洁片的单位重量大体上是均匀的。特别是,在纱布/纤维复合物被加热然后冷却时即可获得宏观的三维度。该工艺导致纱布(沿X-Y维)收缩,由于其与纤维是相连接的,导致清洁片形成较大的三维度。附加的三维度的程度可由对纱布/纤维混合物加热的水平来控制。在结构中的纤维为无纺织物时,掺入纱布是特别有益的,尤其是在结构为水缠结的。
在这一方面,本发明涉及宏观三维的清洁片。这些清洁片与,例如,纸巾相比优选地具有相对开口的结构。在一个优选实施例中,宏观三维清洁片具有一个第一表面和一个第二表面包括纱布材料。在一个这类的优选实施例中,清洁片具有一个第一外表面和一个第二外表面并包括一个纱布材料,其中至少一个外表面的平均的峰到峰的距离至少约为1mm而该表面的表面构形指数为由约0.01到约5。
无论清洁片的形状如何,至少一个外表面的平均的峰到峰的距离至少应为约1mm,更为优选地至少约为2mm,再更为优选地至少约为3mm。在一个实施例中,平均的峰到峰的距离为由约1到约20mm,特别是由约3到约16mm,更为特别地由约4到约12mm。至少一个外表面的表面构形指数将为由约0.01到约10,优选地由约0.1到约5,更为优选地由约0.2到约3,再更为优选地由约0.3到约2。虽然不是关键的,至少一个外表面优选地具有的平均高度差为至少约0.5mm,更为优选地至少约1mm,和再更为优选地至少约1.5mm。至少一个外表面的平均高度差通常为由约0.5到约6mm,更为一般地由约1到约3mm。
关于本发明的宏观三维的清洁片,其结构将会提供增强的延伸率,特别是在CD方向,这将会改善其顺从性,无论清洁片作为单独的制品使用还是和一个清洁工具联合使用。在这一方面,宏观的三维清洁片将优选地在500g时具有至少约3%的CD延伸率,更为优选地至少约6%,更为优选地至少约10%,再更为优选地至少约15%,和再更为优选地为20%。
本发明清洁片的任何清洁效能可通过处理清洁片的纤维而进一步增强,特别是用各种添加物包括表面活性剂或润滑剂中的任一种对表面进行处理,将会增强污物在清洁片上的粘结。在使用时,这种添加物以足以提高清洁片粘结污物的能力的程度。加在清洁片上的这种添加物的添加水平以重量计至少约0.01%,更为优选地至少约0.1%,更为优选地至少约0.5%,更为优选地至少约1%,再更为优选地至少约3%,再更为优选地至少约4%。一般地,添加水平以重量计为由约0.1%到约25%,更为优选地由约0.5%到约20%,更为优选地由1%到约15%,再更为优选地由约3%到约10%,再更为优选地由约4%到约8%,和最优选地由约4%到约6%。一种优选的添加物为蜡或一种油(例如,矿物油,矿脂,等等)和蜡的混合物。适用的蜡包括各种类型的碳氢化合物,以及某些脂肪酸的酯(例如,饱和的甘油三酸脂)和脂肪醇。它们可由天然来源中提取(即,动物,植物或矿物)或人工合成。也可使用这些不同的蜡的混合物。可用于本发明的某些有代表性的动物的和植物的蜡包括蜂蜡,carnauba,鲸蜡,羊毛脂,虫胶蜡,小烛树蜡等等。可用于本发明的有代表性的矿物资源的蜡包括基于石油的蜡如石蜡,矿脂蜡和微晶蜡,和化石蜡或地蜡如白纯地蜡,黄纯地蜡,白石蜡,等等。可用于本发明的有代表性的合成的蜡包括乙烯聚合物如聚乙烯蜡,氯化萘如“卤蜡”,用Fischer-Tropsch合成法制作的碳氢化合物类型的蜡,等等。
在使用矿物油和蜡的混合物时,各种成分的混合优选地按照油与蜡的比例以重量计由约1∶99到约7∶3,更为优选地由约1∶99到约1∶1,再更为优选地由约1∶99到约3∶7。在一个特别优选的实施例中,油与蜡之比以重量计为约1∶1,而添加物的添加水平以重量计约为5%。一种优选的混合物为矿物油和石蜡的1∶1的混合物。
在一个单独的清洁片中,当提供宏观的三维度和添加物时,达到了特别增强的清洁效能。如此前所讨论的,在添加物以有效的水平和优选基本上均匀的方式添加到清洁片上的至少一个单独的连续的区域时,这种低水平是特别需要的。优选的低水平的使用,特别是使用改善污物在清洁片上的粘结的添加物,提供了意想不到好的清洁和抑制空气中灰尘的效果,优选的用户印象,特别是触感,和,另外,添加物可以为加入和附加香水,害虫控制成分,抗菌剂,包括杀菌剂,以及许多其它有益成分特别是那些可溶于或分散于添加物中的成分提供了一种方法。这些好处仅仅是作为例子。在添加物对于基片,包装,和/或待处理的表面有不利影响时,添加物的低水平是特别需要的。
这些添加物的施用方法优选地至少将相当数量的添加物添加在清洁片的位于清洁片结构“内部的”点上。这是三维结构的特殊的优点,即,限制了添加物与待处理的表面,和/或包装相接触的数量,从而使那些对其它表面会引起损伤或影响其功能的物质只能产生有限的不利影响或没有不利影响。添加物在结构内部的存在的好处在于粘结在结构内部的污物很少可能被随后的擦抹作用除去。
图1为根据本发明的一个多层清洁片20。清洁片20包括侧边22和端部边缘24。侧边22一般地沿平行于清洁片20的长度延伸,端部边缘24通常沿平行于清洁片的宽度延伸。可以选择地,清洁片20可以包括一个围绕清洁片周边延伸的边缘封口26。这种边缘封口26的形成可以通过加热,使用粘合剂,或采用加热和粘合剂的组合。
清洁片20包括一个第一层100和一个第二层200。优选地,清洁片还包括一个第三层300。第二层200可以放置在第一层100和第三层300之间。在图1中,第一层100的一部分被切除以显示其下的第二层200和第三层300的部分。
第一层100可以由纺织材料,无纺材料,纸网,泡沫材料,battings,和本领域中所熟知的材料制成。特别优选的材料是无纺织物,其中所具有的纤维或长丝如在“气-敷设”或某些“湿-敷设”工艺中随机分布,或如在某些“湿-敷设”和“梳通”工艺中具有一定的取向度。第一层100中的纤维或长丝可以是天然的,或来自天然的(例如,纤维素纤维如木纸浆纤维,棉花的棉绒纤维,人造纤维,和甘蔗渣纤维)或合成的(例如,聚烯烃类,聚酰胺或聚酯)。第三层300基本上与第一层100相同,或可另外具有不同的材料和/或结构。
在一个实施例中,第一层100和第三层300各自都包含有合成无纺纤维的水缠结织物,纤维具有小于每9000米长的纤维约4.0克的丹尼尔数,优选地小于约3.0,更为优选地小于约2.0克。一种适合的第一层100(以及一个合适的第三层300)为聚酯纤维的水缠结织物,纤维具有每9000米长的纤维约1.5克或略小的丹尼尔数,而织物的单位重量为约每平方米30克。一种适合的织物可按牌号PGI9936由PGINonwovens ofBenson,N.C.购得。
第二层200以不连续的形式连接在第一层100(和第三层300,如果有第三层存在的话)上,并通过第二层的收缩使第一层收拢。收缩的机制,但不作为限制地,包括第二层的热致收缩和弹性特性。如上所述,在这样的一个实施例中,第二层200包括长丝的网-状结构并具有与相邻长丝所限定的开口。另外,第二层可以为聚合物薄膜的形式,其上可选择地具有开口,以提供所需的收缩机制,这种薄膜必须具有足够的弹性以提供构成表面三维度的收拢的功能。代替或除开口外薄膜可以是模压加工的以提供表面的凹陷。作为另外一种选择,可收缩的效应可以由含有在加热和再冷却时产生收缩的纤维生成。在这一方法中,某些纤维将不产生收缩,但由于其联结在可收缩的纤维上,只要含有足够多的这种可收缩的纤维,整个清洁片将因可收缩纤维的收缩而“缩拢”。
在所述的实施例中,第二层带有一个长丝的网状结构,包括一个第一种多个长丝220和一个第二种多个长丝240。长丝220通常彼此平行地延伸,长丝240通常彼此平行地延伸并通常垂直于长丝220。长丝在长丝交点260之间延伸。相交且相邻的长丝220和240构成了第二层200中的开口250。长丝的交点和开口250的布置通常是非无规的,重复的格栅状的式样。
第二层200可包括一个聚合物网(这里指的是一种“纱布材料”)。适用的纱布材料在美国专利第4,636,419号中有详细的描述,在这里将其引入作为参考。纱布可以取自聚烯烃类如聚乙烯或聚丙烯,或其共聚物,聚(对苯二甲酸丁二醇酯),聚对苯二甲酸乙二醇酯,尼龙6,尼龙66,等等,及其混合物。
纱布材料优选地利用加热或化学方法如粘合通过层压成形连接在层100和300上。优选地,纱布材料的长丝在受热时产生相对于层100和300的收缩,第二层200的收缩使层100和300收拢,并赋予层100和300的外表面以宏观三维的结构,如以下将详细描述的。
一种特别适合用作第二层200的纱布材料为一种可由ConwedPlastics of Minneapolis,MN购得的热活化增强网,如THERMANET牌增强网,该网具有聚丙烯/EVA树脂,2侧粘结,和其长丝数量为在通过如加热收缩之前每英寸3根长丝乘以每英寸2根长丝。在加热后,第二层200可能具有每英寸约3.5到4.5根长丝之间乘以每英寸约2.5到3.5根长丝之间。
“2侧粘结”意为在长丝两侧都存在有EVA粘合剂(乙基-乙酸乙烯酯粘合剂)。EVA的活化温度通常为约85℃(约185°F)。在将层200层压到层100和300的聚酯纤维上的过程中,EVA粘合剂被活化形成层200的长丝和层100和300的纤维之间的粘结。不受理论的限制,相信在一个相对短的时间里(例如,小于约30秒)施加相对低的压力(例如,小于50psi和更为优选地小于25psi),层200的长丝不会连续地粘结在层100和300的无纺织物上。这种不连续的粘结,以及聚丙烯长丝受热引起的收缩,形成层100和300的外表面增强的质地。
在图1中,长丝220通常沿平行于侧边22和清洁片20的长度延伸。同样,长丝240通常沿平行于端部边缘24和清洁片20的宽度延伸。
另外,长丝220可以相对于清洁片20的长度和侧边22倾斜一个由约20到约70度之间的角度,更为优选地在约30度到约60度之间。长丝240可以相对于清洁片20的宽度和端部边缘24倾斜一个由约20到约70度之间的角度,更为优选地在约30度到约60度之间。
图2为本发明的一个实施例,其中长丝220相对于侧边22倾斜一个约45度的角度(图2中的角A),而其中的长丝240相对于端部边缘24倾斜一个约45度的角度(图2中的角B)。这样一种结构的优点为长丝220和240相对于清洁片20的长度和宽度形成一个角度的取向可使层200的网状结构的变形平行于边22和24。这种变形为清洁片提供了平行于清洁片长度和宽度的类似弹性的效果。
“类似弹性的行为”意为所讨论的单元在一个方向承受张力时可以沿该方向伸长,其所量得的伸长的尺寸至少为单元在该方向原始的,松弛尺寸的百分之120,在解除张力时单元恢复其松弛尺寸的百分之10以内。
本发明的一个实施例的一个重要的方面为第一层100间断地粘结在第二层200上。特别是,第一层100可以在长丝交点260处间断地粘结在第二层200上,而长丝220的部分,长丝240的部分,或长丝交点260之间的长丝220和240的部分和第一层100保持不粘结。
其结果,第一层100外表面的表面质地不受长丝的网状结构中开口的几何形状的限制,而又与开口250重复的非无规几何形状无关。同样地,第三层300可间断地粘结在第二层200上在第三层300的外表面上形成相似的表面质地。
为清晰起见在图1和2中略去了第一层100的表面质地。表面质地示于图3-8中。
图3为示于图5照片中的第一层100表面质地的示意说明。图4为第一层100和第三层300表面质地的截面图解说明。图5表示第一层100宏观三维表面质地的显微照片。图6为放大的第一层100宏观三维表面的显微照片。图7为说明第一层100三维表面的透视图的扫描电子显微照片。图8为清洁片截面的扫描电子显微照片。
参照图3-8,由于第二层相对于第一层100的收缩使第一层100的一些部分被收拢。这种收拢形成第一层100的宏观三维表面如图3-8所示。同样,第三层300由于第二层200的收缩而收拢,形成第三层300的宏观三维表面。
第一层100的三维表面具有相对升起的峰105和相对凹陷的谷107。第三层具有峰305和谷307。在图4中第一层100的峰用参考号105A和105B表示,而第一层100的谷用参考号107A和107B表示。同样地,层300的峰标以305A和305B,谷标以307A和307B。峰105在第一层100的外表面上形成伸长的脊线120,而峰305在第三层300的外表面上形成伸长的脊线320。
第一层100的宏观三维外表面可以用一个峰和一个相邻的谷的“平均高度差”,以及相邻的峰之间的“平均的峰-到-峰的距离”来描述。一对峰105A/谷107A的高度差为图4中的距离H。相邻的一对峰105A和105B之间的峰-到-峰的距离在图4中用距离D表示。清洁片的“平均高度差”和“平均的峰-到-峰的距离”按下面所述的“试验方法”进行测量。外表面的“表面构形指数”为用表面平均的峰-到-峰的距离除表面平均高度差所得的比值。
熟悉此项技术的人很清楚峰和谷相对较小的范围不能足够明显地被认为是宏观的三维度。例如,这个区域可能在单元中出现,它是由,例如,一种弹性材料偶然的收缩所形成的三维度。再有,这种波动和变形是制造工艺正常和预期的结果并不是在测量表面构形指数时所考虑的。
不受理论的限制,可以相信表面构形指数是在表面的谷中接受和容纳物质方面对宏观三维表面有效性的一个度量。对于一个给定的平均的峰-到-峰的距离,一个相对高的平均高度差的值提供了可以收集和容纳物质的深而窄的谷。于是,可以确信一个相对较高的表面构形指数的值表明在擦抹时对物质的有效捕捉。
本发明的清洁片具有第二层200的长丝220的一些部分,长丝240的一些部分,或长丝220和240二者的一些部分并未和第一层100相联结的特点。参照图4,长丝220在长丝交点260A和260B之间延伸的一个部分没有联结在第一层100上。长丝220没有和第一层100相联结的部分用参考号220U表示。长丝220和第一层100之间的缝隙在第一层100和长丝220中间提供了一个空隙空间180。同样,在长丝交点260之间延伸的长丝220的一些部分没有联结在第三层300上,在长丝220和第三层300之间提供了一个空隙空间380。
图7和8表明了清洁片20的这一特性。在图7中,分别在第一和第三层100,300的外表面上可以看到细长的脊线120和320。在图8中,可见一个长丝220在两个长丝交点260中间延伸。长丝在两个长丝交点中间延伸的部分与第一层是隔开和没有联结的。
在图3和图5中以平面图示出了脊线120。至少某些脊线120穿过了第二层200的至少一根长丝。在图4中,相应于峰105A的脊线120穿过了至少一根长丝220。
因为脊线穿过一根或更多的长丝,脊线可以具有大于相邻长丝交点260之间的最大距离(在第二层200收缩并收拢层100和300之后相邻长丝交点之间的距离)的长度。特别是,脊线120的长度可能大于图1所示开口250的最大尺寸(即,大于跨越矩形开口250对角线的长度)。在图3中脊线120的长度用字母L表示。长度L为一根脊线120的两端之间的直线距离,脊线120的端部为脊线120在一个谷107终了的点。
L的值为至少约1.0厘米,特别是某些脊线120至少约1.5厘米。在一个实施例中,至少某些脊线120的长度L为至少约2.0厘米。长度L可至少两倍于相邻的长丝交点之间的距离。
例如,为了确定脊线120相对于相邻的长丝交点之间距离的长度,可以浸湿清洁片20并放在一个透亮的桌子上或其它适合的后部光照的光源上。这样的后部光照以及清洁片的被浸湿,可用以透过层100看到层200的长丝交点,因而脊线120相对于长丝交点之间的距离的长度可以用同一标准测量。
伸长的脊线为增强由待清洁的表面去除物质提供了柔软的,可变形的擦抹元件。相反,如果第二层的长丝连续地粘结在第一和第二层上,则第一和第三层的任何质地特性将被限定于第二层200中的开口250的面积。
至少某些伸长的脊线延伸的方向不同于至少某些其它脊线。参看图3,脊线120A,120B,和120C每根沿不同的方向延伸。于是,在清洁片用于沿不同方向擦抹时清洁片可有效地拣起物质。
图3和6还表示一根脊线120可以有沿不同方向延伸的分支。在图3中,所示脊线120具有三个沿不同方向延伸的分支123A,123B,和123C。同样,图6表示一根脊线120具有至少三个标号为123A,123B,和123C的分支。
第一层100和第三层300在长丝交点260处牢牢地粘结在第二层200上。图9表明层100和300二者的纤维在长丝交点260处和第二层相粘接。
参看图4,7和8,第一层100的峰105通常在清洁片20的平面内偏离第三层的峰305。例如,在图4中第三层的峰305A并非直接在峰105A之下,但通常代替的是对准毗邻峰105A的谷107A。于是,第一层的峰105通常对准第三层的谷307,第三层的峰305通常对准第一层的谷107。
本发明还包括制作多层清洁片的方法。设置了一个第一无纺层,一个包括一个长丝的网状结构的第二层,和一个第三无纺层。第一层与第二层面对面地被放置在靠近第二层的上表面上。第三层与第二层面对面地被放置在靠近第二层的下表面上。
随后第一层和第三层间断地粘结在第二层的分散的,间隔开的部分,从而使在长丝交点之间延伸的长丝部分与第一层保持不粘结,同时使在长丝交点之间延伸的长丝部分与第三层保持不粘结。第二层相对于第一层和第三层收缩从而为第一层提供一个收拢的,宏观三维的外表面,和一个收拢的第三层的宏观三维外表面。粘结和收缩的步骤可以同时进行,或顺序进行。
将第二层间断地粘结在第一层和第三层上的步骤可包括在一个相对短的时间段内以相对较低的压力热压第一层,第二层,和第三层的步骤,以避免第二层相对连续地粘结在第一和第三层上。
在一个实施例中,三层之间可以使用由HIX Corp.Pittsburg,Kansas制作的BASIX B400手压机连结。在约330°F的温度下用手压机约13秒以压力对三层进行粘结。手压机具有改变间隙的调节装置从而对施压所提供的压力进行调整。调整可以按照需要改变以在层100和300中提供所需的质地。
本发明还包括盛装清洁片的包装,包装带有利用文字和/或图画告知消费者使用清洁片将会提供清洁的效益的信息,包括污物(例如,灰尘,棉绒,等等)的清除和/或夹带,以及该信息可包括优于其它清洁制品的声明。一个高度期望的改变,在于包装提供了告知消费者的信息,即清洁片的使用提供了降低灰尘和大气中空气携带的物质的能力。告知消费者在非-传统的表面,包括在织物,宠物等等上使用清洁片的效力,以保证清洁片的全部效能均可实现是很重要的。于是,使用包装连同利用文字和/或图画提供的信息重要的是要告知消费者,如在这里所讨论的,使用组合物将会提供诸如改善清洁,降低空气中颗粒污物的效果,等等。信息可以包括,例如,在所有惯用媒体上的广告,以及在包装上的,或在清洁片本身上的说明和插图,用以告知消费者。
不包括这里所述的优选结构的已有制品,可用以提供较低程度的效果,就这些效果此前未被认同来说,所有这些都应包括在所提供的信息之内。否则,消费者将会得不到相对于传统的制品或实践的改善性能的全部价值。
III.清洁工具
另一方面,本发明涉及一种包含上述清洁片的清洁工具。在这方面,清洁工具包括:
a.一个手柄;和
b.一个具有第一表面和第二表面的可拆卸的清洁片,其中平均的峰到峰的距离为至少约1.0mm和表面构形指数为由约0.01到约5。
本发明的工具和,独立地,清洁片的设计适合于所有的硬表面基质,包括木,乙烯树脂,漆布,无蜡地板,陶器,FORMICA,瓷器,等等。
清洁工具的手柄包括任意细长的耐用材料,该材料可提供在人类工程学上实用的清洁处理。手柄的长度取决于工具的最终用途。
手柄优选地在其一端具有一个清洁片可拆卸地连接在其上的支撑头。为便于使用,可利用已知的联结设备将支撑头可旋转地连接在手柄上。可以使用任何适用的装置将清洁片连接在支撑头上,只要清洁片在清洁过程中能够保持固定。适合的紧固装置的例子包括夹子,搭扣(例如,VELCRO),等等。在一个优选实施例中,支撑头带有用以将清洁片夹紧在其上表面的装置,使清洁片在严峻的清洁过程中保持机械地连接在支撑头上。但是,夹紧装置应便于将清洁片卸下以便去除和丢掉。
适用于本发明的清洁工具中的清洁片如上所述。
IV.试验方法
A.平均高度差
平均高度差可利用配备有Z-向测量设备(例如,由Boeckeler,Instruments出售的Microcode II)的光学显微镜(例如,Zeiss Axioplan,Zeiss Company,Germany)测定。该方法包括定位清洁片的一个峰或谷区域,将显微镜聚焦并将Z-向测量设备置零。随后将显微镜分别移至相邻的谷或峰区域,再对显微镜进行调焦。仪器显示出这一对峰/谷或谷/峰的高度差。这种测量至少在清洁片的随机位置上重复10次,平均高度差为这些测量结果的平均值。
B.峰-到-峰的距离
可以使用简单的光学显微镜测量峰-到-峰的距离。所使用的放大倍数应能足以容易地测量两个相邻的峰之间的距离。这种测量应在清洁片上随机的位置上重复至少10次,平均的峰-到-峰的距离为这些测量结果的平均值。
C.500g下的CD延伸率
CD延伸率为一个试验样本在500g的荷载下所量得的百分比延伸率。CD延伸率可以利用Sintech Renew Instron 7310(包括Testworks软件包)以一个100N测力传感器进行测量。利用这一仪器,即可生成荷载对%应变的曲线。其试验参数如下:
样本宽度=30mm
测量长度(Gauge Length)=100mm
十字头速度=300mm/min
由所生成的曲线,软件得出500g荷载下的%应变(%延伸率)。这被报告为在500g下的CD延伸率。
V.代表性实施例
以下为本发明清洁片的说明性实施例。增强的三维度示于表I中。
实施例1
本实施例说明结合梳通的织物和纱布(即,一个聚丙烯长丝的网)制作一个本发明的清洁片。准备好两个聚酯纤维织物及其中间的纱布。这两个梳通的织物和纱布的组合随后被放在一个有孔的成形带(N 50flat square)上并进行水缠结和干燥。水缠结的过程使纤维变成相互缠绕并同纱布相缠绕,同时使一些纤维离开从而形成两个不同的单位重量区。在干燥的过程中,作为聚丙烯纱布相对于聚酯无纺织物收缩的结果,水缠结清洁片变得被“缝拢(quilted)”(即,达到了较大的三维度)。作为可供选择的优选的步骤,无纺织物清洁片表面被涂敷(通过,例如,印刷,喷雾,等等)以5重量%的矿物油和石蜡1∶1的混合物。对缠结的无纺清洁片进一步加热,例如,在180℃下按压10秒钟,以提供较大程度的三维度。该清洁片被标示为表1中的实施例1。(这种加热可以在进行可供选择的表面处理之前或之后,但优选地在施加添加物之前进行)。这种附加的加热进一步增强了三维度。
实施例2
根据本发明的清洁片包括一个第一层100,一个第二层200,和一个第三层300。第一层100和第三层300每一层都包括一个聚酯纤维的水缠结织物,所述纤维具有单位重量约每平方米30克。第二层包括上述的THERMANET牌增强网,该网具有聚丙烯/EVA树脂,两侧粘结,和在第二层收缩之前长丝数为每英寸3根长丝乘以每英寸2根长丝。用BASIX B400手压机将第二层200放置在第一层100和第三层300之间。这三层通过在温度设为约330°F的情况下用手压机压约13秒钟进行联结。
擦抹制品所具有的平均的峰到峰的距离,平均高度差,和表面构形指数的测量值示于表I。
对比实施例A
对比实施例A说明了一个具有均匀单位重量并基本为平面的无纺清洁片。该清洁片可按牌号QUICKLE由Kao Corporation,Tokyo,Japan购得。
表I
实施例# | 平均高度差(mm) | 平均的峰到峰的距离(mm) | 表面构形指数 |
1 | 0.74 | 1.5 | 0.5 |
2 | 1.8 | 3 | 0.6 |
对比实施例A | 0.14 | 0.85 | 0.16 |
Claims (20)
1.一种宏观三维清洁片,清洁片具有一个第一外表面和一个第二外表面,其特征在于至少一个外表面的平均的峰到峰的距离为至少1mm和表面构形指数为0.01到10。
2.权利要求1中所说的清洁片,其特征在于至少一个外表面的平均高度差至少为0.5mm,优选地至少1mm,更为优选地至少1.5mm。
3.权利要求1或2中所说的清洁片,其特征在于至少一个外表面的平均的峰到峰的距离为至少2mm,优选地至少3mm。
4.权利要求1或2中所说的清洁片,其特征在于至少一个外表面的平均的峰到峰的距离为1到20mm,优选地4到12mm。
5.权利要求1-4中任一个所说的清洁片,其特征在于至少一个外表面的表面构形指数为0.1到5,优选地0.2到3,更为优选地0.3到2。
6.权利要求1-5中任一个所说的清洁片,清洁片上具有以低有效水平添加的添加物用以增进污物在清洁片上的粘结,优选地按清洁片的重量计算的添加水平为至少0.01%,优选地按清洁片的重量计算的添加水平为至少1%,优选地按清洁片的重量计算的添加水平为1到15%,优选地按清洁片的重量计算的添加水平为3到10%。
7.权利要求6中所说的清洁片,其特征在于添加物为矿物油和一种蜡的混合物。
8.权利要求1-7中任一个所说的清洁片,其特征在于该清洁片在消费者专门小组试验中相对于基本上为平面的清洁片显示出改进的清洁性能。
9.一种一次应用的宏观三维清洁片,与传统的去除灰尘的方法相比可以降低大气中空气携带的物质的含量。
10.一种一次应用的宏观三维清洁片,与传统的去除灰尘的方法相比可以降低表面上颗粒污物的含量。
11.权利要求1-10中任一个所说的清洁片,清洁片在一种包装中,该包装带有说明书,说明与传统的灰尘去除方法相比在具有颗粒物质的至少一个表面上使用清洁片可降低空气中颗粒物质的含量。
12.权利要求1-10中任一个所说的清洁片,清洁片在一种包装中,该包装带有说明书,说明在具有颗粒物质的至少一个表面上使用清洁片可降低表面上颗粒物质的含量。
13.一种包括宏观三维清洁片的制品,其中清洁片在一个带有使用该清洁片以降低空气携带的颗粒物质的说明书的包装内。
14.权利要求13中所说的制品,其特征在于所说的说明书包括在被颗粒物质污染的表面上使用清洁片的说明。
15.权利要求14中所说的制品,其特征在于所说的颗粒物质是不可见的和/或所说的表面不是那种传统地用清洁片可以去除颗粒物质的表面。
16.一种清洁工具,包括:
a.一个手柄;和
b.一个可拆卸的清洁片,其特征在于清洁片为权利要求1-12任一个中的清洁片。
17.权利要求16中所说的清洁工具,其带有说明书,说明书中说明使用该清洁工具与传统的清除灰尘的方法相比可降低分散在大气中灰尘的含量。
18.权利要求17中所说的清洁工具,其特征在于所说的灰尘包括过敏原。
19.权利要求16中所说的清洁工具,其带有说明书,说明书中说明使用该清洁工具与传统的清除灰尘的方法相比可降低表面上颗粒污物的含量。
20.一种清洁表面的方法,包括用一个具有第一外表面和第二外表面的宏观三维清洁片与该表面相接触,其特征在于至少一个外表面的平均的峰到峰的距离至少为1mm和表面构形指数为0.01到10。
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1998
- 1998-05-20 CN CN98807385A patent/CN1264278A/zh active Pending
- 1998-05-20 TR TR1999/02876T patent/TR199902876T2/xx unknown
- 1998-05-20 EP EP98923592A patent/EP0986322B1/en not_active Expired - Lifetime
- 1998-05-20 KR KR1019997010874A patent/KR20010012907A/ko not_active Application Discontinuation
- 1998-05-20 AT AT98923591T patent/ATE256415T1/de not_active IP Right Cessation
- 1998-05-20 AT AT01203013T patent/ATE249164T1/de not_active IP Right Cessation
- 1998-05-20 RU RU99127458A patent/RU2176143C2/ru active
- 1998-05-20 IL IL13301698A patent/IL133016A0/xx unknown
- 1998-05-20 DE DE69820611T patent/DE69820611T2/de not_active Revoked
- 1998-05-20 DE DE69802798T patent/DE69802798T2/de not_active Expired - Lifetime
- 1998-05-20 ID ID991437A patent/ID27460A/id unknown
- 1998-05-20 WO PCT/US1998/010363 patent/WO1998052459A1/en not_active Application Discontinuation
- 1998-05-20 AU AU75847/98A patent/AU740795B2/en not_active Ceased
- 1998-05-20 HU HU0003717A patent/HUP0003717A2/hu unknown
- 1998-05-20 ES ES98923592T patent/ES2167077T3/es not_active Expired - Lifetime
- 1998-05-20 CA CA002293362A patent/CA2293362C/en not_active Expired - Lifetime
- 1998-05-20 US US09/082,396 patent/US6561354B1/en not_active Expired - Lifetime
- 1998-05-20 TR TR200000246T patent/TR200000246T2/xx unknown
- 1998-05-20 BR BR9809155-7A patent/BR9809155A/pt not_active Application Discontinuation
- 1998-05-20 US US09/082,349 patent/US6645604B1/en not_active Expired - Lifetime
- 1998-05-20 CA CA002291124A patent/CA2291124C/en not_active Expired - Lifetime
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- 1998-05-20 DE DE1998618112 patent/DE69818112T2/de not_active Expired - Lifetime
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- 1998-05-20 AU AU75848/98A patent/AU7584898A/en not_active Abandoned
- 1998-05-20 JP JP55060798A patent/JP2001527455A/ja active Pending
- 1998-05-20 ES ES01203013T patent/ES2202256T3/es not_active Expired - Lifetime
- 1998-05-20 CN CN98807386A patent/CN1264279A/zh active Pending
- 1998-05-20 ES ES98923591T patent/ES2213280T3/es not_active Expired - Lifetime
- 1998-05-20 WO PCT/US1998/010362 patent/WO1998052458A1/en not_active Application Discontinuation
- 1998-05-20 EP EP98923591A patent/EP0983014B1/en not_active Revoked
- 1998-05-20 JP JP55060698A patent/JP2001527454A/ja active Pending
- 1998-05-22 AR ARP980102383 patent/AR012855A1/es not_active Application Discontinuation
- 1998-05-22 AR ARP980102387 patent/AR016753A1/es not_active Application Discontinuation
- 1998-05-26 CO CO98029440A patent/CO5050376A1/es unknown
- 1998-05-26 CO CO98029446A patent/CO5040098A1/es unknown
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1999
- 1999-11-22 NO NO995728A patent/NO995728L/no not_active Application Discontinuation
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2000
- 2000-03-07 NO NO20001156A patent/NO20001156D0/no not_active Application Discontinuation
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2001
- 2001-04-12 US US09/833,869 patent/US6790794B2/en not_active Expired - Lifetime
- 2001-06-14 US US09/881,473 patent/US6797357B2/en not_active Expired - Lifetime
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2004
- 2004-06-24 JP JP2004186979A patent/JP2004337621A/ja active Pending
- 2004-07-29 US US10/902,213 patent/US6936330B2/en not_active Expired - Lifetime
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2005
- 2005-03-24 US US11/089,411 patent/US20060029774A1/en not_active Abandoned
- 2005-03-28 US US11/091,223 patent/US20050166347A1/en not_active Abandoned
- 2005-03-29 JP JP2005095161A patent/JP4369387B2/ja not_active Expired - Lifetime
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2007
- 2007-06-19 JP JP2007161618A patent/JP4814845B2/ja not_active Expired - Lifetime
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2011
- 2011-08-17 US US13/211,931 patent/US8536074B2/en not_active Expired - Fee Related
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2013
- 2013-09-16 US US14/027,414 patent/US20140026341A1/en not_active Abandoned
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2014
- 2014-01-17 US US14/157,936 patent/US9005734B2/en not_active Expired - Fee Related
- 2014-01-17 US US14/157,863 patent/US9040146B2/en not_active Expired - Fee Related
- 2014-01-17 US US14/157,911 patent/US9005733B2/en not_active Expired - Fee Related
- 2014-01-17 US US14/157,845 patent/US8999489B2/en not_active Expired - Fee Related
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2015
- 2015-03-27 US US14/670,768 patent/US20150196186A1/en not_active Abandoned
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CN105492216B (zh) * | 2013-08-22 | 2017-06-27 | 李美先 | 具有注气鼓起表面的电子装置外壳、日记本及其制造方法 |
CN105960189A (zh) * | 2014-02-07 | 2016-09-21 | 宝洁公司 | 清洁片及其层合体 |
CN105960189B (zh) * | 2014-02-07 | 2020-03-24 | 宝洁公司 | 清洁片及其层合体 |
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