DE69402509D1 - Verfahren zur Herstellung eines hydrophoben Aerogels - Google Patents

Verfahren zur Herstellung eines hydrophoben Aerogels

Info

Publication number
DE69402509D1
DE69402509D1 DE69402509T DE69402509T DE69402509D1 DE 69402509 D1 DE69402509 D1 DE 69402509D1 DE 69402509 T DE69402509 T DE 69402509T DE 69402509 T DE69402509 T DE 69402509T DE 69402509 D1 DE69402509 D1 DE 69402509D1
Authority
DE
Germany
Prior art keywords
production
hydrophobic airgel
airgel
hydrophobic
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Expired - Lifetime
Application number
DE69402509T
Other languages
English (en)
Other versions
DE69402509T2 (de
DE69402509T3 (de
Inventor
Hiroshi Yokogawa
Masaru Yokoyama
Koichi Takahama
Yuriko Uegaki
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Panasonic Electric Works Co Ltd
Original Assignee
Matsushita Electric Works Ltd
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Family has litigation
First worldwide family litigation filed litigation Critical https://patents.darts-ip.com/?family=17669302&utm_source=google_patent&utm_medium=platform_link&utm_campaign=public_patent_search&patent=DE69402509(D1) "Global patent litigation dataset” by Darts-ip is licensed under a Creative Commons Attribution 4.0 International License.
Application filed by Matsushita Electric Works Ltd filed Critical Matsushita Electric Works Ltd
Publication of DE69402509D1 publication Critical patent/DE69402509D1/de
Publication of DE69402509T2 publication Critical patent/DE69402509T2/de
Application granted granted Critical
Publication of DE69402509T3 publication Critical patent/DE69402509T3/de
Anticipated expiration legal-status Critical
Expired - Lifetime legal-status Critical Current

Links

Classifications

    • CCHEMISTRY; METALLURGY
    • C08ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08GMACROMOLECULAR COMPOUNDS OBTAINED OTHERWISE THAN BY REACTIONS ONLY INVOLVING UNSATURATED CARBON-TO-CARBON BONDS
    • C08G77/00Macromolecular compounds obtained by reactions forming a linkage containing silicon with or without sulfur, nitrogen, oxygen or carbon in the main chain of the macromolecule
    • C08G77/04Polysiloxanes
    • C08G77/06Preparatory processes
    • CCHEMISTRY; METALLURGY
    • C01INORGANIC CHEMISTRY
    • C01BNON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
    • C01B33/00Silicon; Compounds thereof
    • C01B33/113Silicon oxides; Hydrates thereof
    • C01B33/12Silica; Hydrates thereof, e.g. lepidoic silicic acid
    • C01B33/14Colloidal silica, e.g. dispersions, gels, sols
    • C01B33/157After-treatment of gels
    • C01B33/158Purification; Drying; Dehydrating
    • C01B33/1585Dehydration into aerogels
    • CCHEMISTRY; METALLURGY
    • C08ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08GMACROMOLECULAR COMPOUNDS OBTAINED OTHERWISE THAN BY REACTIONS ONLY INVOLVING UNSATURATED CARBON-TO-CARBON BONDS
    • C08G77/00Macromolecular compounds obtained by reactions forming a linkage containing silicon with or without sulfur, nitrogen, oxygen or carbon in the main chain of the macromolecule
    • C08G77/02Polysilicates
DE69402509T 1993-11-12 1994-04-27 Verfahren zur Herstellung eines hydrophoben Aerogels Expired - Lifetime DE69402509T3 (de)

Applications Claiming Priority (2)

Application Number Priority Date Filing Date Title
JP283726/93 1993-11-12
JP5283726A JP2725573B2 (ja) 1993-11-12 1993-11-12 疎水性エアロゲルの製法

Publications (3)

Publication Number Publication Date
DE69402509D1 true DE69402509D1 (de) 1997-05-15
DE69402509T2 DE69402509T2 (de) 1997-07-17
DE69402509T3 DE69402509T3 (de) 2005-09-15

Family

ID=17669302

Family Applications (1)

Application Number Title Priority Date Filing Date
DE69402509T Expired - Lifetime DE69402509T3 (de) 1993-11-12 1994-04-27 Verfahren zur Herstellung eines hydrophoben Aerogels

Country Status (4)

Country Link
US (1) US5496527A (de)
EP (1) EP0653377B2 (de)
JP (1) JP2725573B2 (de)
DE (1) DE69402509T3 (de)

Families Citing this family (61)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US5504042A (en) * 1994-06-23 1996-04-02 Texas Instruments Incorporated Porous dielectric material with improved pore surface properties for electronics applications
FR2736342B1 (fr) * 1995-07-07 1999-01-29 Univ Claude Bernard Lyon Procede pour la fabrication d'aerogels de silice monolithiques et aerogels de silice ainsi obtenus
US6177505B1 (en) 1995-08-31 2001-01-23 The Yokohama Rubber Co., Ltd. Polysiloxane-containing rubber composition
DE19533851A1 (de) * 1995-09-13 1997-03-20 Hoechst Ag Organofunktionalisierte Aerogele
DE19541279A1 (de) * 1995-11-06 1997-05-07 Hoechst Ag Verfahren zur Herstellung von organisch modifizierten Aerogelen unter Verwendung von Alkoholen
US6037277A (en) * 1995-11-16 2000-03-14 Texas Instruments Incorporated Limited-volume apparatus and method for forming thin film aerogels on semiconductor substrates
US5753305A (en) * 1995-11-16 1998-05-19 Texas Instruments Incorporated Rapid aging technique for aerogel thin films
US6319852B1 (en) 1995-11-16 2001-11-20 Texas Instruments Incorporated Nanoporous dielectric thin film formation using a post-deposition catalyst
US6130152A (en) * 1995-11-16 2000-10-10 Texas Instruments Incorporated Aerogel thin film formation from multi-solvent systems
US6380105B1 (en) 1996-11-14 2002-04-30 Texas Instruments Incorporated Low volatility solvent-based method for forming thin film nanoporous aerogels on semiconductor substrates
US5955140A (en) * 1995-11-16 1999-09-21 Texas Instruments Incorporated Low volatility solvent-based method for forming thin film nanoporous aerogels on semiconductor substrates
US5807607A (en) * 1995-11-16 1998-09-15 Texas Instruments Incorporated Polyol-based method for forming thin film aerogels on semiconductor substrates
US5736425A (en) * 1995-11-16 1998-04-07 Texas Instruments Incorporated Glycol-based method for forming a thin-film nanoporous dielectric
US5790742A (en) * 1995-12-12 1998-08-04 Matsushita Electric Works, Ltd. Optical fiber
DE19622500C2 (de) * 1996-06-05 1998-09-17 Fraunhofer Ges Forschung Verfahren zur Herstellung poröser Keramik der Zusammensetzung Pb(Zr¶x¶Ti¶1¶-¶x¶)0¶3¶
DE19648798C2 (de) * 1996-11-26 1998-11-19 Hoechst Ag Verfahren zur Herstellung von organisch modifizierten Aerogelen durch Oberflächenmodifikation des wäßrigen Gels (ohne vorherigen Lösungsmitteltausch) und anschließender Trocknung
US6197270B1 (en) 1996-12-20 2001-03-06 Matsushita Electric Works, Ltd. Process for producing aerogel
DE19718741A1 (de) 1997-05-02 1998-11-05 Hoechst Ag Verfahren zur Kompaktierung von Aerogelen
DE19718740A1 (de) 1997-05-02 1998-11-05 Hoechst Ag Verfahren zur Granulierung von Aerogelen
DE19726330C2 (de) * 1997-06-20 1999-07-29 Joerg Ortjohann Vakuum-Isolationspaneel, Verfahren zur Herstellung eines solchen Paneels und ein Verfahren zur Regelung der Wärmeströme
US6154595A (en) * 1997-07-14 2000-11-28 Matsushita Electric Works, Ltd. Side-face illuminating optical fiber
DE19752456A1 (de) * 1997-11-26 1999-05-27 Hoechst Ag Verfahren zur Herstellung von organisch modifizierten Aerogelen auf Basis von Siliciumtetrachlorid
DE19756633A1 (de) 1997-12-19 1999-06-24 Hoechst Ag Verfahren zur unterkritischen Trocknung von Lyogelen zu Aerogelen
DE19801004A1 (de) * 1998-01-14 1999-07-15 Cabot Corp Verfahren zur Herstellung von im wesentlichen kugelförmigen Lyogelen in wasserunlöslichen Silylierungsmitteln
JP2002517585A (ja) 1998-06-05 2002-06-18 カボット・コーポレーション ナノ多孔質相互浸透有機−無機網目構造
DE69935236T2 (de) * 1998-08-12 2007-11-08 Rofin Australia Pty. Ltd., Dingley Flüssigkeitslichtleiter
JP4107732B2 (ja) 1998-10-20 2008-06-25 松下電器産業株式会社 有機多孔体の製造方法
US6586501B1 (en) 1999-01-20 2003-07-01 Cabot Corporation Aggregates having attached polymer groups and polymer foams
BR0014797A (pt) * 1999-10-21 2002-06-11 Aspen Systems Inc Método rápido aperfeiçoado para a preparação de um produto aerogel
US6762553B1 (en) 1999-11-10 2004-07-13 Matsushita Electric Works, Ltd. Substrate for light emitting device, light emitting device and process for production of light emitting device
EP1153739B1 (de) 1999-11-10 2008-06-04 Matsushita Electric Works, Ltd. Aerogelsubstrat und seine herstellung
US6764667B1 (en) 2001-03-09 2004-07-20 Steiner, Iii Stephen A. Method for the formation of aerogel precursor using rapid gelation two-step catalysis
US20030032681A1 (en) * 2001-05-18 2003-02-13 The Regents Of The University Of Clifornia Super-hydrophobic fluorine containing aerogels
EP2226365B1 (de) 2001-10-25 2016-08-10 Panasonic Intellectual Property Management Co., Ltd. Tafellichtemittierender Körper
US20050119360A1 (en) * 2003-11-28 2005-06-02 Kabushiki Kaisha Kobe Seiko Sho Method for producing porous material
CN1950414B (zh) 2004-12-01 2010-05-05 三洋电机株式会社 有机金属聚合物材料
TWI401161B (zh) 2005-06-21 2013-07-11 Zeon Corp 偏光板用保護膜(二)
US7998563B2 (en) 2005-06-21 2011-08-16 Zeon Corporation Protective film for polarizing plate
US8367793B2 (en) * 2005-09-30 2013-02-05 Abs Materials, Inc. Swellable materials and methods of use
US8021610B2 (en) * 2006-09-07 2011-09-20 Biolargo Life Technologies, Inc. Systems providing antimicrobial activity to an environment
JP2008193291A (ja) * 2007-02-02 2008-08-21 Matsushita Electric Ind Co Ltd 乾燥ゲルを含む音響整合層とその製造方法
CN101357766B (zh) * 2007-07-30 2012-04-18 成都思摩纳米技术有限公司 二氧化硅疏水粉末超临界制取技术
JP4575978B2 (ja) * 2008-10-31 2010-11-04 日東電工株式会社 液晶表示装置
GB0905205D0 (en) * 2009-03-26 2009-05-13 Dow Corning Preparation of organosiloxane polymer
JP5377252B2 (ja) * 2009-11-27 2013-12-25 日東電工株式会社 画像表示装置
WO2012148522A1 (en) 2011-04-26 2012-11-01 Keller Compainies, Inc. Aerogel with reduced dust, static charge, and having reduced fluidity when in granular form
JP5803468B2 (ja) * 2011-09-14 2015-11-04 富士ゼロックス株式会社 疎水性シリカ粒子の製造方法
JP6099029B2 (ja) * 2011-11-08 2017-03-22 オゾンセーブ株式会社 断熱用塗料、該塗料を用いた断熱方法、及び該塗料を塗布したシート材
KR101409884B1 (ko) 2012-05-04 2014-06-27 한국과학기술연구원 소수성 모노리스형 실리카 에어로젤의 제조방법
KR101501015B1 (ko) * 2012-12-13 2015-03-10 한국생산기술연구원 이산화탄소 용매를 이용한 폴리실세스퀴옥산의 제조방법 및 이를 이용하여 제조된 폴리실세스퀴옥산.
US9399632B2 (en) 2013-02-05 2016-07-26 Basf Se Process for producing a solid oxidic material
KR20150115939A (ko) * 2013-02-05 2015-10-14 바스프 에스이 고체 산화물 물질의 제조 방법
JP2016507624A (ja) * 2013-02-05 2016-03-10 ビーエーエスエフ ソシエタス・ヨーロピアBasf Se 多孔性または微細な固体無機材料の製造方法
US9249075B2 (en) 2013-02-05 2016-02-02 Basf Se Process for producing porous or finely divided solid inorganic materials
WO2015129736A1 (ja) 2014-02-26 2015-09-03 日立化成株式会社 エアロゲル
WO2016047740A1 (ja) * 2014-09-25 2016-03-31 日立化成株式会社 エアロゲル複合体、エアロゲル複合体付き支持部材及び断熱材
RU2576311C1 (ru) * 2014-11-25 2016-02-27 Федеральное государственное бюджетное учреждение науки Институт элементоорганических соединений им. А.Н. Несмеянова Российской академии наук (ИНЭОС РАН) Способ получения полиорганосилоксанов
US10821705B2 (en) 2015-09-02 2020-11-03 Hitachi Chemical Company, Ltd. Aerogel laminated composite and thermal insulation material
ES2818298B2 (es) 2019-10-07 2021-11-08 Consejo Superior Investigacion Procedimiento para la preparación de aerogeles hidrofóbicos
CN112875711B (zh) * 2021-01-26 2022-06-21 西南科技大学 一种梯度密度疏水氧化硅气凝胶的制备方法
CN115093241B (zh) * 2022-06-07 2023-10-13 航天特种材料及工艺技术研究所 一种疏水型耐高温气凝胶材料及其制备方法

Family Cites Families (16)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US4402927A (en) * 1980-04-22 1983-09-06 Dardel Guy Von Silica aerogel
FR2507171A1 (fr) * 1981-06-04 1982-12-10 Zarzycki Jerzy Aerogels de silice monolithiques, leur preparation et leur utilisation pour la preparation d'articles en verre de silice et de materiaux thermiquement isolants
DE3429671A1 (de) 1984-08-11 1986-02-20 Basf Ag, 6700 Ludwigshafen Verfahren zur herstellung von aerogelen
US4619908A (en) * 1984-12-24 1986-10-28 Stauffer Chemical Company Non-aged inorganic oxide-containing aerogels and their preparation
US4610863A (en) * 1985-09-04 1986-09-09 The United States Of America As Represented By The United States Department Of Energy Process for forming transparent aerogel insulating arrays
DE3616133A1 (de) * 1985-09-25 1987-11-19 Merck Patent Gmbh Kugelfoermige sio(pfeil abwaerts)2(pfeil abwaerts)-partikel
DE3814968A1 (de) 1988-05-03 1989-11-16 Basf Ag Daemmstoff der dichte 0,1 bis 0,4 g/cm(pfeil hoch)3(pfeil hoch)
US4954327A (en) * 1988-08-12 1990-09-04 Blount David H Production of silica aerogels
IT1230709B (it) * 1989-02-10 1991-10-29 Enichem Spa Procedimento per la preparazione di monoliti di aerogel di ossidi di metalli.
DE3914850A1 (de) * 1989-05-05 1990-11-08 Basf Ag Thermisches isoliermaterial auf der basis von pigmenthaltigen kieselsaeureaerogelen
WO1992003378A1 (en) * 1990-08-23 1992-03-05 United States Department Of Energy A METHOD FOR PRODUCING METAL OXIDE AEROGELS HAVING DENSITIES LESS THAN 0.02 g/cm?3¿
JP2756366B2 (ja) * 1990-11-27 1998-05-25 松下電工株式会社 疎水性エアロゲルの製造方法
JP2659155B2 (ja) * 1992-02-03 1997-09-30 松下電工株式会社 疎水性エアロゲルの製造方法
WO1993016125A1 (en) * 1992-02-18 1993-08-19 Matsushita Electric Works, Ltd. Process for producing hydrophobic aerogel
EP0585456B1 (de) * 1992-02-18 1997-05-07 Matsushita Electric Works Ltd Verfahren zur herstellung eines hydrophoben aerogels
DK0716641T3 (da) 1993-08-31 1998-02-09 Basf Ag Hydrofobe kiselsyreaerogeler

Also Published As

Publication number Publication date
EP0653377A1 (de) 1995-05-17
DE69402509T2 (de) 1997-07-17
EP0653377B1 (de) 1997-04-09
EP0653377B2 (de) 2004-11-24
JP2725573B2 (ja) 1998-03-11
US5496527A (en) 1996-03-05
DE69402509T3 (de) 2005-09-15
JPH07138375A (ja) 1995-05-30

Similar Documents

Publication Publication Date Title
DE69402509D1 (de) Verfahren zur Herstellung eines hydrophoben Aerogels
DE4419591B4 (de) Verfahren zur Herstellung eines plastisch geformten Produkts
DE69528216D1 (de) Verfahren zur Herstellung eines Dauerstents
DE69732758D1 (de) Verfahren zur Herstellung eines Aerogels
DE69503400T2 (de) Verfahren zur Herstellung falznahtloser Dosen
DE69617797T2 (de) Verfahren zur Herstellung eines nahtlosen Rohres
DE69614609D1 (de) Verfahren zur Herstellung eines Einkristalles
DE69615265D1 (de) Verfahren zur Herstellung von anorganischen Formen
DE59604197D1 (de) Verfahren zur unterkritischen herstellung von anorganischen aerogelen
DE69707566D1 (de) Verfahren zur Herstellung eines Formkörpers
DE69319469T2 (de) Verfahren zur Herstellung eines Gitterrostes
DE59602361D1 (de) Verfahren zur Herstellung eines Bleiakkumulators
DE59306861D1 (de) Verfahren zur Herstellung eines Rohrgelenks
DE69616673T2 (de) Verfahren zur Herstellung eines selbstklebenden Verschlusses
DE69219599D1 (de) Verfahren zur herstellung eines hydrophoben aerogels
DE69424045D1 (de) Verfahren zur abbau komplexer kohlenwasserstoffe zur herstellung einfacherer kohlenwasserstoffe
DE59608440D1 (de) Verfahren zur Herstellung von gewellten Metallrohren
DE69703265D1 (de) Verfahren zur Herstellung eines Rohres
DE69404357T2 (de) Verfahren zur Herstellung eines diamantverstärktes Verbundmaterials
DE69422198D1 (de) Verfahren zur Herstellung eines Weichschaumstoffs
DE59303002D1 (de) Vorrichtung zur Herstellung eines Betonrohres
DE69400494D1 (de) Verfahren zur Herstellung eines Bodenbelages
DE69817489D1 (de) Verfahren zur Herstellung eines Betonproduktes
DE69420654T2 (de) Verfahren zur Herstellung eines Hydrofluorokohlenwasserstoffs
DE69307056D1 (de) Verfahren zur Herstellung eines laminierten Schlauches

Legal Events

Date Code Title Description
8363 Opposition against the patent
8320 Willingness to grant licences declared (paragraph 23)
8366 Restricted maintained after opposition proceedings