DE69507502D1 - Synthese von porösen, kristallinen feststoffen in ammoniak - Google Patents

Synthese von porösen, kristallinen feststoffen in ammoniak

Info

Publication number
DE69507502D1
DE69507502D1 DE69507502T DE69507502T DE69507502D1 DE 69507502 D1 DE69507502 D1 DE 69507502D1 DE 69507502 T DE69507502 T DE 69507502T DE 69507502 T DE69507502 T DE 69507502T DE 69507502 D1 DE69507502 D1 DE 69507502D1
Authority
DE
Germany
Prior art keywords
ammonia
porous
synthesis
crystalline solids
solids
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Expired - Fee Related
Application number
DE69507502T
Other languages
English (en)
Other versions
DE69507502T2 (de
Inventor
Juan Garces
Dean Millar
Kevin Howard
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Dow Chemical Co
Original Assignee
Dow Chemical Co
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Dow Chemical Co filed Critical Dow Chemical Co
Publication of DE69507502D1 publication Critical patent/DE69507502D1/de
Application granted granted Critical
Publication of DE69507502T2 publication Critical patent/DE69507502T2/de
Anticipated expiration legal-status Critical
Expired - Fee Related legal-status Critical Current

Links

Classifications

    • CCHEMISTRY; METALLURGY
    • C01INORGANIC CHEMISTRY
    • C01BNON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
    • C01B39/00Compounds having molecular sieve and base-exchange properties, e.g. crystalline zeolites; Their preparation; After-treatment, e.g. ion-exchange or dealumination
    • C01B39/02Crystalline aluminosilicate zeolites; Isomorphous compounds thereof; Direct preparation thereof; Preparation thereof starting from a reaction mixture containing a crystalline zeolite of another type, or from preformed reactants; After-treatment thereof
    • C01B39/46Other types characterised by their X-ray diffraction pattern and their defined composition
    • C01B39/48Other types characterised by their X-ray diffraction pattern and their defined composition using at least one organic template directing agent
    • CCHEMISTRY; METALLURGY
    • C01INORGANIC CHEMISTRY
    • C01BNON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
    • C01B33/00Silicon; Compounds thereof
    • C01B33/113Silicon oxides; Hydrates thereof
    • C01B33/12Silica; Hydrates thereof, e.g. lepidoic silicic acid
    • C01B33/18Preparation of finely divided silica neither in sol nor in gel form; After-treatment thereof
    • C01B33/181Preparation of finely divided silica neither in sol nor in gel form; After-treatment thereof by a dry process
    • C01B33/185Preparation of finely divided silica neither in sol nor in gel form; After-treatment thereof by a dry process of crystalline silica-polymorphs having molecular sieve properties, e.g. silicalites
    • CCHEMISTRY; METALLURGY
    • C01INORGANIC CHEMISTRY
    • C01BNON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
    • C01B37/00Compounds having molecular sieve properties but not having base-exchange properties
    • C01B37/02Crystalline silica-polymorphs, e.g. silicalites dealuminated aluminosilicate zeolites
    • YGENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y10TECHNICAL SUBJECTS COVERED BY FORMER USPC
    • Y10STECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y10S423/00Chemistry of inorganic compounds
    • Y10S423/27Beta, e.g. NU-2
DE69507502T 1994-11-03 1995-10-31 Synthese von porösen, kristallinen feststoffen in ammoniak Expired - Fee Related DE69507502T2 (de)

Applications Claiming Priority (2)

Application Number Priority Date Filing Date Title
US08/333,670 US5599520A (en) 1994-11-03 1994-11-03 Synthesis of crystalline porous solids in ammonia
PCT/US1995/014235 WO1996014269A1 (en) 1994-11-03 1995-10-31 Synthesis of crystalline porous solids in ammonia

Publications (2)

Publication Number Publication Date
DE69507502D1 true DE69507502D1 (de) 1999-03-04
DE69507502T2 DE69507502T2 (de) 1999-05-27

Family

ID=23303769

Family Applications (1)

Application Number Title Priority Date Filing Date
DE69507502T Expired - Fee Related DE69507502T2 (de) 1994-11-03 1995-10-31 Synthese von porösen, kristallinen feststoffen in ammoniak

Country Status (8)

Country Link
US (2) US5599520A (de)
EP (1) EP0789668B1 (de)
JP (1) JPH10508570A (de)
KR (1) KR970707041A (de)
AU (1) AU4142996A (de)
DE (1) DE69507502T2 (de)
ES (1) ES2126954T3 (de)
WO (1) WO1996014269A1 (de)

Families Citing this family (42)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
AU5382796A (en) * 1995-04-03 1996-10-23 Massachusetts Institute Of Technology Composition and method for producing hexagonally-packed meso porous metal oxide
US6187283B1 (en) 1995-11-15 2001-02-13 California Institute Of Technology Hydrothermal conversion of Y-zeolite using alkaline earth cations
US5935551A (en) * 1995-11-15 1999-08-10 California Institute Of Technology Synthesis of zeolites by hydrothermal reaction of zeolite P1
US6217840B1 (en) 1995-12-08 2001-04-17 Goldendale Aluminum Company Production of fumed silica
US6193944B1 (en) 1995-12-08 2001-02-27 Goldendale Aluminum Company Method of recovering fumed silica from spent potliner
US5840271A (en) * 1996-02-09 1998-11-24 Intevep, S.A. Synthetic material with high void volume associated with mesoporous tortuous channels having a narrow size distribution
US5849258A (en) * 1996-06-06 1998-12-15 Intevep, S.A. Material with microporous crystalline walls defining a narrow size distribution of mesopores, and process for preparing same
US5919430A (en) * 1996-06-19 1999-07-06 Degussa Aktiengesellschaft Preparation of crystalline microporous and mesoporous metal silicates, products produced thereby and use thereof
US5688484A (en) * 1996-07-29 1997-11-18 Arco Chemical Technology, L.P. Non-hydrothermal method of making a titanium-containing zeolite
WO1998015500A1 (en) * 1996-10-10 1998-04-16 Massachusetts Institute Of Technology Compositions and methods for preparing porous metal oxides
JPH10139419A (ja) * 1996-11-11 1998-05-26 Yukong Ltd 非結晶性中間細孔モレキュラーシーブの製造方法及びそのモレキュラーシーブ
IT1290846B1 (it) * 1996-12-12 1998-12-14 Enichem Spa Composizione catalitica e processo per l'alchilazione e/o la transalchilazione di composti aromatici
DE19701080C1 (de) * 1997-01-15 1998-07-02 Bk Giulini Chem Gmbh & Co Ohg Verfahren zum Färben von Keramikoberflächen
US6190639B1 (en) * 1997-03-17 2001-02-20 Shell Oil Company Process for the preparation of mesoporous molecular sieves and porous crystalline materials
US5942208A (en) * 1997-06-20 1999-08-24 Yu Kong Limited Mesoporous molecular sieve substance and method for preparing the same
US6071614A (en) * 1997-07-14 2000-06-06 3M Innovative Properties Company Microporous fluorinated silica agglomerate and method of preparing and using same
ES2137885B1 (es) * 1997-12-19 2000-08-16 Univ Valencia Politecnica Zeolita itq-5.
EP1123581A4 (de) * 1998-10-21 2005-08-10 American Calcar Inc Positionkamera und gps datenaustauchsverfahren
US6248302B1 (en) 2000-02-04 2001-06-19 Goldendale Aluminum Company Process for treating red mud to recover metal values therefrom
US6223563B1 (en) * 2000-03-17 2001-05-01 Lucent Technologies Inc. Process for fabricating fluorine-doped sol-gel article
US6521198B2 (en) 2000-05-17 2003-02-18 The Regents Of The University Of California Metal surfaces coated with molecular sieve for corrosion resistance
AU2002328130B2 (en) * 2001-06-06 2008-05-29 Ammono Sp. Z O.O. Process and apparatus for obtaining bulk monocrystalline gallium-containing nitride
PL207400B1 (pl) * 2001-06-06 2010-12-31 Ammono Społka Z Ograniczoną Odpowiedzialnością Sposób i urządzenie do otrzymywania objętościowego monokryształu azotku zawierającego gal
KR100679387B1 (ko) 2001-10-26 2007-02-05 암모노 에스피. 제트오. 오. 질화물 반도체 레이저 소자 및 이의 제조방법
AU2002354467A1 (en) 2002-05-17 2003-12-02 Ammono Sp.Zo.O. Light emitting element structure having nitride bulk single crystal layer
US20060138431A1 (en) * 2002-05-17 2006-06-29 Robert Dwilinski Light emitting device structure having nitride bulk single crystal layer
EP1514958B1 (de) * 2002-05-17 2014-05-14 Ammono S.A. Vorrichtung zur herstellung von volumeneinkristallen unter einsatz von überkritischem ammoniak
TWI334890B (en) 2002-12-11 2010-12-21 Ammono Sp Zoo Process for obtaining bulk mono-crystalline gallium-containing nitride, eliminating impurities from the obtained crystal and manufacturing substrates made of bulk mono-crystalline gallium-containing nitride
EP1576210B1 (de) * 2002-12-11 2010-02-10 AMMONO Sp. z o.o. Substrat für epitaxie und verfahren zu seiner herstellung
US20050100494A1 (en) * 2003-11-06 2005-05-12 George Yaluris Ferrierite compositions for reducing NOx emissions during fluid catalytic cracking
US20050100493A1 (en) * 2003-11-06 2005-05-12 George Yaluris Ferrierite compositions for reducing NOx emissions during fluid catalytic cracking
US7304011B2 (en) * 2004-04-15 2007-12-04 W.R. Grace & Co. -Conn. Compositions and processes for reducing NOx emissions during fluid catalytic cracking
US20050232839A1 (en) 2004-04-15 2005-10-20 George Yaluris Compositions and processes for reducing NOx emissions during fluid catalytic cracking
WO2005121415A1 (en) * 2004-06-11 2005-12-22 Ammono Sp. Z O.O. Bulk mono-crystalline gallium-containing nitride and its application
JP4719835B2 (ja) * 2004-09-13 2011-07-06 島根県 シリカ多孔体結晶の製造方法
PL371405A1 (pl) * 2004-11-26 2006-05-29 Ammono Sp.Z O.O. Sposób wytwarzania objętościowych monokryształów metodą wzrostu na zarodku
SG169976A1 (en) 2005-04-27 2011-04-29 Grace W R & Co Compositions and processes for reducing nox emissions during fluid catalytic cracking
FR2895275B1 (fr) * 2005-12-22 2008-07-25 Framatome Sa Membranes de separation de gaz contenant une couche de silice microporeuse a base de silice dopee par un element trivalent
JP5600870B2 (ja) * 2008-12-19 2014-10-08 東ソー株式会社 ソーダライト粉末及びその製造方法
ES2343234B2 (es) * 2009-01-23 2011-03-24 Fmc Foret, S.A. Mezcla fotocatalitica para la degradacion de oxidos de nitrogeno.
EP2463410B1 (de) 2010-12-13 2018-07-04 Rohm and Haas Electronic Materials LLC Elektrochemisches Ätzen von Halbleitern
US9802182B2 (en) 2013-03-13 2017-10-31 Basf Corporation Stabilized metal-exchanged SAPO material

Family Cites Families (42)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US2958578A (en) * 1958-03-12 1960-11-01 Chester L Baker Manufacture of finely divided metal silicate products
US3308069A (en) * 1964-05-01 1967-03-07 Mobil Oil Corp Catalytic composition of a crystalline zeolite
USRE28341E (en) * 1964-05-01 1975-02-18 Marshall dann
US3758539A (en) * 1971-03-09 1973-09-11 Air Prod & Chem Offretite synthesis from minerals
US3965042A (en) * 1973-12-07 1976-06-22 W. R. Grace & Co. Formation of alumina-containing particles with aluminum hydroxide binder
US4061724A (en) * 1975-09-22 1977-12-06 Union Carbide Corporation Crystalline silica
US4039479A (en) * 1976-09-10 1977-08-02 Uop Inc. Method of catalyst manufacture
EP0002899B1 (de) * 1977-12-23 1983-03-16 The British Petroleum Company p.l.c. Verfahren zur Herstellung von Aluminosilikaten und deren Verwendung als Katalysatorträger und Katalysatoren
NL7803662A (nl) * 1978-04-06 1979-10-09 Shell Int Research Werkwijze voor de bereiding van zeolieten.
CA1128914A (en) * 1979-09-04 1982-08-03 Clive D. Telford Method of preparing improved catalysts and use thereof in hydrocarbon conversion reactions
DE3066649D1 (en) * 1979-12-07 1984-03-22 British Petroleum Co Plc Process for the production of crystalline aluminosilicates and their use as catalysts and catalyst supports
US4300012A (en) * 1980-01-17 1981-11-10 Uop Inc. Process for transalkylation of alkylaromatic hydrocarbons
US4264473A (en) * 1980-01-17 1981-04-28 Uop Inc. Method of catalyst manufacture, and catalyst made by said method
NZ201207A (en) * 1981-07-23 1984-11-09 British Petroleum Co Plc Zeolite-based catalyst production and use
US4419220A (en) * 1982-05-18 1983-12-06 Mobil Oil Corporation Catalytic dewaxing process
NZ205457A (en) * 1982-09-07 1986-03-14 British Petroleum Co Plc The production of crystalline aluminosilicates of the type designated theta-1 and uses thereof
US4665255A (en) * 1983-05-10 1987-05-12 Mobil Oil Corporation Catalytic conversion of aromatic compounds
DE3402842A1 (de) * 1984-01-27 1985-08-08 Süd-Chemie AG, 8000 München Verfahren zur herstellung von kristallinen zeolithischen alumosilicaten
US4642226A (en) * 1984-04-16 1987-02-10 Mobil Oil Corporation Process for the preparation of zeolite Beta using dibenzyldimethylammonium ions and the product produced
US4923690A (en) * 1984-06-11 1990-05-08 Mobil Oil Corporation Method for producing highly siliceous zeolites
US4717560A (en) * 1985-02-04 1988-01-05 Exxon Research And Engineering Company Crystalline zeolite composition (ECR-5) having a cancrinite-like structure and process for its preparation
JPS6287409A (ja) * 1985-09-09 1987-04-21 Tama Kagaku Kogyo Kk 合成シリカの製造方法
FR2607128B1 (fr) * 1986-11-21 1989-04-28 Inst Francais Du Petrole Nouvelles ferrierites, leur procede de preparation et leur utilisation
DE3880369T2 (de) * 1987-05-22 1993-08-05 Rhone Poulenc Chimie Zeolithe mit mfi-struktur auf der basis von kieselsaeure und titanoxid und verfahren zu deren synthese.
US4840929A (en) * 1987-07-02 1989-06-20 Mobil Oil Corporation Zeolite beta with improved regeneration characteristics
DE3728451A1 (de) * 1987-08-26 1989-03-09 Basf Ag Alkalifreie herstellung von grossen pentasil-kristallen als schalen- und vollkatalysatoren
GB8721202D0 (en) * 1987-09-09 1987-10-14 Shell Int Research Preparation of crystalline(metallo)silicates
US4828812A (en) * 1987-12-29 1989-05-09 Mobil Oil Corporation Titanosilicates of enhanced ion exchange capacity and their preparation
DE3838710A1 (de) * 1988-11-15 1990-05-17 Sued Chemie Ag Katalysator auf der basis von kristallinen alumosilikaten
NL9000637A (nl) * 1989-04-28 1990-11-16 Seikosha Kk Papiertoevoerinrichting.
US5171556A (en) * 1989-09-22 1992-12-15 Institut Francais Du Petrole Beta type zeolite and its preparation process
FR2669618B1 (fr) * 1990-11-26 1993-05-07 Elf Aquitaine Procede de desalumination des zeolithes synthetiques a larges pores, catalyseurs et adsorbants organophiles selectifs renfermant les zeolithes desaluminees obtenues selon le procede et zeolithe beta essentiellement silicique.
US5164170A (en) * 1991-06-14 1992-11-17 Mobil Oil Corporation Synthesis of zeolite Beta
JPH0517122A (ja) * 1991-07-12 1993-01-26 Shin Etsu Chem Co Ltd 合成シリカ粉の製造方法
DE4131448A1 (de) * 1991-09-21 1993-03-25 Basf Ag Verfahren zur herstellung von im wesentlichen alkalifreien borsilikat-kristallen mit zeolithstruktur
JPH07503693A (ja) * 1991-11-20 1995-04-20 ザ・ダウ・ケミカル・カンパニー フッ化物を含有した実質的に非水の成長媒体中で結晶質微孔質固体を成長させる方法
DE4138155A1 (de) * 1991-11-21 1993-05-27 Basf Ag Verfahren zur herstellung von im wesentlichen alkalifreien titansilikat-kristallen mit zeolithstruktur
US5200168A (en) * 1992-01-31 1993-04-06 Mobil Oil Corp. Process for the dealumination of zeolite Beta
DE4206553A1 (de) * 1992-03-02 1993-09-09 Merck Patent Gmbh Clathrasil vom strukturtypen dodekasil 1 h mit kleiner mittlerer kristallgroesse
US5318766A (en) * 1992-09-25 1994-06-07 Exxon Research And Engineering Company Process for preparing LTL nano-crystalline zeolite compositions
US5374747A (en) * 1993-12-23 1994-12-20 Arco Chemical Technology, L.P. Epoxidation process and catalyst therefore
US5508019A (en) * 1994-06-30 1996-04-16 Arco Chemical Technology, L.P. Dealumination of aluminosilicates

Also Published As

Publication number Publication date
ES2126954T3 (es) 1999-04-01
EP0789668B1 (de) 1999-01-20
KR970707041A (ko) 1997-12-01
EP0789668A1 (de) 1997-08-20
JPH10508570A (ja) 1998-08-25
AU4142996A (en) 1996-05-31
US5599520A (en) 1997-02-04
DE69507502T2 (de) 1999-05-27
US5589153A (en) 1996-12-31
WO1996014269A1 (en) 1996-05-17

Similar Documents

Publication Publication Date Title
DE69507502D1 (de) Synthese von porösen, kristallinen feststoffen in ammoniak
DE69421288D1 (de) Poröses synthetisches kristallines material mcm-58, dessen synthese und verwendung
DE69807691D1 (de) Schlammkohlenwasserstoffsynthese mit externer produktfiltrierung
DE69501534D1 (de) Synthese von 1,1,1,3,3-Pentafluorpropan
DE69613769D1 (de) Integriertes Harnstoff-/Ammoniak-Verfahren
DK0763379T3 (da) Katalysator på basis af Fe(1-x)O til syntese af ammoniak
DE59902179D1 (de) Elektrochemische synthese von perfluoralkylfluorophosphoranen
ATE231507T1 (de) Synthese von azyklischen nukleosiden
DE69517011T2 (de) Polymergestützte lösungs-synthese von oligosacchariden
ATE66387T1 (de) Ammoniaksynthesekonverter.
DE68908440T2 (de) Synthese von Trichostatin.
DE3586161T2 (de) Verfahren zur synthese von ammoniak.
DE3771893D1 (de) Ammoniak-synthese.
DE3586114D1 (de) Synthese von ammoniak.
DE69111820D1 (de) Ammoniaksynthese mit hohem umwandlungsgrad.
DE3863249D1 (de) Ammoniumaktivierung von zeolithen in anwesenkeit von gasfoermigem ammoniak.
DK0853593T3 (da) Syntetisk, porøst, krystallinsk MCM-61, dets syntese og anvendelse
DE69915809D1 (de) Katalysator zur synthese von ammoniak aus wasserstoff und stickstoff
DE69707656T2 (de) Synthese von cycloalkyldiarylphosphin
DE69024900D1 (de) Katalytische Oxidation von Ammoniak
DE69708273T2 (de) Synthese von cycloalkyldiarylphosphin
DK0553072T3 (da) Syntetisk, porøst, krystallinsk materiale samt fremstilling og syntese af samme
DE69907115T2 (de) Katalytische Umsetzung von Ammoniak
NO974303L (no) Poröst ammoniumnitrat
DE69530024T2 (de) Verwendung von Katalysatoren zur Zersetzung von Ammoniak

Legal Events

Date Code Title Description
8364 No opposition during term of opposition
8339 Ceased/non-payment of the annual fee