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Publication numberUS2610149 A
Publication typeGrant
Publication dateSep 9, 1952
Filing dateAug 10, 1949
Priority dateAug 10, 1949
Publication numberUS 2610149 A, US 2610149A, US-A-2610149, US2610149 A, US2610149A
InventorsDyke Orien W Van
Original AssigneeMagnet Cove Barium Corp
Export CitationBiBTeX, EndNote, RefMan
External Links: USPTO, USPTO Assignment, Espacenet
Method and means of preventing fluid loss through porous walls
US 2610149 A
Abstract  available in
Images(3)
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Claims  available in
Description  (OCR text may contain errors)

During the drillingof an oil well or Patented Sept. 9, 1952 METHOD AND FLUID Loss 'rn WALLS s 'ATENT OFFICE MEANS Ora-PREVENTI G ROUGH, POROUS Orien WJVan'D'yke, HoustomjTex assignor to Magriet'Co've Barium Crporation,Ho1iston, Tex .,a corporationof Arkansas? 9 i .1.

No Drawing; Application ugust10,1949,

v Serial N0.109,612

This invention r'elates'to a method and product which may be employed in drilling and carrying out other processes in wells for thepurpose of preventing or reducing loss of fluid from the well bore into thesurrounding formations.

the like it is not uncommon to encounter porous gravels,

culated down through the drill pipe during drill- ]ing enters the porous formati'on and does not return tothe surface. Since drilling fluid performs a number of'functions in the course of a drilling operation, one of which is to serve as a vehicle for carrying the cuttings to the surface, and another of which is to exert suflicient hydrostatic pressure against the formations drilled to balance any pressures existing in these formations, it is necessary for all or substantially all of the fluid pumped into the hole to return to the surface and for the hole to remain full of fluid. When porous formations are encountered, which allow the mud to escape from the hole, drilling operations must stop because cuttings cannot then be removed and fluid must be pumped into the bore hole at a rapid rate in order to maintain suflicient hydrostatic head to balance formation pressures, or the hole will collapse and the danger will exist that fluids or gas under pressure will blow out of the hole.

Drilling fluid is usually a water suspension of colloidal clays, weighting materials and formation solids that is stabilized by chemical treatment. Drilling fluids have viscosities that range from approximately centipoises to as much as 80 centipoises. The weight of a drilling fluid varies from 9 pounds per gallon to as heavy as 19 pounds per gallon. During the drilling operation it is usual practice to provide in some fashion for settling or removing of the cuttings from the drilling mudv The mud is then collectediin a pit from which it is picked up by pumps and pumped back into the hole. Drilling fluids such as that just described are ordinarily capable of building a relatively impervious filter cake on porous formations made up of materials such as fine sand grains, but suchfluids will readily flow through small cracks or other openings in formations, In order to prevent this loss offluid in' theporou's formations, it has been the usual practice to" add various types of materials such as fibrous materials or flake materials which can be mixed with the mud and which are capable 8 Claims. (01.252

. .12. i of circulatingthrough the reciprocating pumps ordinarily employed inpumping the mud. Materials which have been used or suggested in the past for this purposeinclude chopped up corn stalks, sugar cane, beet pulp, cottonseed hulls, sawdust, wood shavings, flake cellophane, chopped up'paper and mica flakes. i I

It is the object of this invention to provide material substantially more effective than those previously employed which willbuild an impervious mat in or over fissures; cracks and porous formations through which mat mud will not pass, and which will be of such a nature that it will not foul the valves and other working partsof the circulating pumps. It is also an. object to provide a method preventing fluid loss by employing such a product and a method of making same.

It has been found that exceptionally and unexpectedly good results may be secured. through the employment of a product made from. whole ripe flax straw. However, the flax straw is not employed in the usual manner of employing straws and the likefor this purpose but is specially treated tochange it into a flufiy mass of small fibers having particles of the hard woody outside of the flax straw :interspersed therein. Such treatment consists of first cutting the straw into lengths of the order of one-inch or less, then shredding it in a hammer mill, then blowingthe' dust out of the fluffy mass thereby produced. The strong, fine, long fibers which are found-in the central portion of the flax straw provide the fillfiy mass which is'highly desirable for'the purpose indicated, and the hard, woody outside portion of the flax straw, commonly known as shives, provide relative stiff members capable of assisting the long, fine fibers-in providing a bridge over fissures and the like. This cottonlike mass can be easily mixed with mud and when strained out on a porous medium, forms a mat that is impervious to the passage of mud. It appears that the two principal constituents both play an important part in making the shredded and dotted flax straw a suitable material for plugging porous formations. The

employment of fibers of greater length than oneinch involves a tendency on the part of the fibers to ball up and not to disperse properly in the mud, and also involves the possibility of interfering with the action of the mud pumps. With the practice of cutting the material to a length,

of one-inch or less, the likelihood. of difliculty is greatly reduced. In fact, the length preferred from the stand-point of greatest effectiveness and freedom from difliculty is in the neighborhood of three-quarters of an inch.

As compared with other materials commonly used in the drilling of wells for the purpose above indicated, shredded flax straw prepared in the manner" above described, has been found to be a greatly and unexpectedly effective.

Forexample, as regards actual use in a well being drilled, one well in which loss of circulattion infthe cavernous limestone was being experienced, was treated with numerous materials includingflake cellophane, shredded sugar cane flber, wood fiber, mica flakes, and chopped hemp rope. The use of all these materials was unsuccessful in stopping the loss of fluid. Upon the addition of- 1250 pounds of shredded flax straw, the loss of fluid was stopped and returns of the mud were established. This product has been used in several hundred Wells in order to combat the loss of mud in the porous formations, and reports on such wells indicate that the shredded flax' straw product is in almost every instance -more effective than other materials which had been previously'used. In order to more carefully compare the effectiveness and action of this flax straw product with the action of other materials which have been used or suggested for this purpose, a laboratory test method has been employed which is suggested by the'American Petroleum Institute as a method of testing materials for the prevention of loss of the drilling fluids to the formation while drilling. This method of testing involves the use of a standard filter press which is modifled to accommodate an enlarged pressure filtration cell; The special cell is a cylinder approxi- 'mately IO-inches in length, and 31 inches inside diameter, having a capacity of 1000 cc. one-quarter inch brass plate perforated with thirty -inch holes is brazed into the cylinder three-eights of an inch from the lower end. The standard filter press cap and bottom plate are used to confine the ends of the cell. The filter bed is made up of a three-fourths inch layer of copperclad steel BB shot which are 0.173 inch in diameter resting on the perforated plate. .This'bed is formed by rapidly pouring 400 grams -of the BB shot into thecell so that the onequarter inch holes in the perforated plate are I bridged. This gives a filter bed having a porosity of approximately thirty-five (35%) per cent and a permeability of approximately 70,000

darcys. v In accordance with this method a suspension of -Wyoming bentonite of a strength of five (5%) per centto eight (8%) per cent of the bentonite ,is prepared and stirred thirty minutes on a highspeed mixer. seventy-two (72) hours and stirred ten minutes It is then aged a minimum of 4 after which it is adjusted to have a viscosity of 30 centipoises, plus or minus two oentipoises. Weighed portions of the sealing material under test are then added to 800 cc. of the 30-centipoise base mud and stirredten minutes. The prepared sample is then'poure'di'nto the filter cell carefully so as not to distrub the filter bed, and the filter cell is closed and air pressure in the amount of 100 pounds per square inch is applied. The object of this test is to determine the volume of mud that passes through the filter bed before the strained out additive seals sufficiently to cause normal filtration. The test is of thirty minutes duration unless no seal-off is accomplished. A record of both the volume of mud that passes through the filter bed before a sealoff is obtained and the volume obtained by dropwise filtration is made. The thickness and character of the sealing material cake built upon the BB shot filter bed isf'f measured and recorded.

The concentration .of sealing material isexpressed as pounds per barrel added. It should be noted in this connection that one grain in 350 cc. of drilling fluid is the equivalent of one pound per barrel.

The datagiven below shows the results of a series of tests employing the above method in which the materials being tested were various fibrous materials which have been used orsuggested for the purpose'of preventingfluid loss in drilling wells, as indicated below. The data'given Dropwise 0011mm 1111 ha] M at A tration Surge Thwk a ii it cc. ness U MIHS.

f /bbl. inches .Newspaper l0 No mat Bagasse 10 2 Cottonseed hulls 1o 1 Shredded prairie hay... 10 600 2 l Shredded wheat strawv 10 500 2% 0) Ground asbestos 10 700 l Shredded rice straw 10 600 1% Bagasse and paper i p p in 230 1/ a Shredded balsa wood 10 530 f; 90%, fiax Jfisiilraw 10% ases os er 10. 125 Shredded flax straw 5 350 i; 11 Do 10 105 is 8.2 1 No seal cfl.

1 Unconsolidated mass.

- In the foregoing it will be seen that by far the bestiproduct tested is the shredded flax straw of this invention, and that of all the other'products tested, the best results were indicated by the combination of shredded flax straw and 10% Such straw is considered unfit for use in producing fibers for use in fabrics but is highly suitable for the use in accordance with this invention because the woody portion of the straw will have become dry and brittle, and though still relatively rigid as compared with thefine inner fibers of the straw, will readily break up and become interspersed with the fluffy mass of fine fibers so as to produce the product of this invention.

From the foregoing it will be seen that there has been provided a product for use in a drilling fluid for the purpose of preventing a loss thereoi into porous formations, which product is both economical and highly effective, and makes possible a method which is capable of accomplishing the desired results to a degree better than heretofore obtained. Furthermore, there has been produced a new method of making such a product which differs distinctly from methods employed in preparing previously used materials for this purpose and which is highly advantageous in producing a vastly improved material.

All the objects and advantages sought by this invention are thus attained by the method and means set forth, although it is to be understood that the foregoing specific disclosure is by way of illustration and example only and is not to be taken by way of limitation. This invention is to be limited only by the prior art and by the terms of the appended claims.

The invention having been described, what is claimed as:

1. An article of manufacture comprising a dry fiuffy mass of fine flax fibers having shives interspersed therethrough and derived from ripened flax straw, the lengths of the fibers and shives being of the order of one-inch and less and at least some of the shives being elongated to provide relatively stiff bridging members to give body tothe fibers.

2. The method of preventing drilling fluid loss in earth bore holes which comprises introducing into the bore hole a quantity of shredded ripened flax straw comprising a fluffy mass of fine fibers having shives interspersed therethrough.

3. The method of preventing drilling fluid loss in earth bore holes which comprises introducin into the bore hole a quantity of shredded ripened flax straw comprising a fluffy mass of fine fibers having shives interspersed therethrough, the shives and fibers being of lengths of the order of one-inch and less.

4. The method of preventing drilling fluid loss in earth bore holes which comprises introducing ripened flax straw comprising a fiuffy mass of 6 fine fibers having shives interspersed therethrough.

5. The method of making an additive for drilling fiuid for preventing loss thereof in drilling earth bore holes which comprises chopping whole ripe fiax straw into lengths of the order of one-.

inch and less, shredding and fiufiing the cut straw in a dry state, and blowing the dust therefrom.

6. The method of making an additive for drilling fiuid for preventing loss thereof in drilling earth bore holes which comprises chopping whole ripe fiax straw into short lengths in a dry state, shredding and fiufiing the cut straw, and blowing the dust therefrom.

7. A drilling mud which comprises, in combination, suflicient liquid to maintain the mud as a fiuid,.sufficient clayey material to form a filter cake on the wall of a well and a lost circulation reducing material comprising a quantity of shredded ripe flax straw made up of a mass of fine fibers adapted to mat and form a membrane and relatively stifi shives interspersed therethrough to provide a bridging for support of said membrane, the quantity of said straw being sufiicient to reduce mud loss to porous formations contacted by said mud.

'8. The drilling mud of claim 7 wherein said fibers and said shives are of lengths of the order of one inch and less.

ORIEN W. VAN DYKE.

REFERENCES CITED The following references are of record in the file of this patent:

UNITED STATES PATENTS Number Name Date 1,168,285 Coyne Jan. 18, 1916 2,119,829 Parsons a June 7', 1938 2,298,994 Wells Oct. 19, 1942 2,351,434 Jessen et al June 131, 1944 2,477,219 Van Dyke July 26, 1949 OTHER REFERENCES Hertel 82 Edson, Drilling Mud Practice in the Venture. Avenue, pps. 387-388, Petroleum Development 8; Technology, 1930.

Wallace A. Sawdon, Lost Circulation in Rotary Holes A Problem Requiring Specific Treatment, pps. 27-30, The Petroleum Engineer, February 1936.

Rogers, Composition and Properties of Oil Well Drilling Fluids, 1948, pps. 455-461.

Patent Citations
Cited PatentFiling datePublication dateApplicantTitle
US1168285 *Jan 4, 1915Jan 18, 1916Gen Fiber CompanyPaper.
US2119829 *May 12, 1936Jun 7, 1938Phillips Petroleum CoMethod of and composition for preventing the loss of drilling fluid in well drilling operations
US2298994 *Jun 25, 1941Oct 13, 1942Paper Chemistry InstManufacture of papermaking fiber
US2351434 *Jan 5, 1943Jun 13, 1944Standard Oil Dev CoUse of pecan hulls for treating muds
US2477219 *Mar 21, 1947Jul 26, 1949Magnet Cove Barium CorpMethod and means of preventing fluid loss through porous walls
Referenced by
Citing PatentFiling datePublication dateApplicantTitle
US2749308 *Jun 21, 1952Jun 5, 1956Weyerhaeuser Timber CoMaterial for treating oil well drilling fluids
US2756209 *Apr 29, 1953Jul 24, 1956 Preventing lost circulation of mud in
US2830948 *Jan 30, 1956Apr 15, 1958Continental Oil CoWell working composition
US3788405 *Aug 23, 1971Jan 29, 1974Trans Canada Resources LtdProcess for plugging formations
US5118664 *Mar 28, 1991Jun 2, 1992Bottom Line Industries, Inc.Lost circulation material with rice fraction
US5332724 *May 29, 1992Jul 26, 1994Bottom Line Industries, Inc.Lost circulation material with corn cob outers
US6016869 *Oct 31, 1997Jan 25, 2000Burts, Jr.; Boyce D.Well kill additive, well kill treatment fluid made therefrom, and method of killing a well
US6016871 *Oct 31, 1997Jan 25, 2000Burts, Jr.; Boyce D.Hydraulic fracturing additive, hydraulic fracturing treatment fluid made therefrom, and method of hydraulically fracturing a subterranean formation
US6016879 *Oct 31, 1997Jan 25, 2000Burts, Jr.; Boyce D.Lost circulation additive, lost circulation treatment fluid made therefrom, and method of minimizing lost circulation in a subterranean formation
US6098712 *Oct 31, 1997Aug 8, 2000Bottom Line Industries, Inc.Method of plugging a well
US6102121 *Oct 31, 1997Aug 15, 2000BottomLine Industries, Inc.Conformance improvement additive, conformance treatment fluid made therefrom, method of improving conformance in a subterranean formation
US6218343Oct 31, 1997Apr 17, 2001Bottom Line Industries, Inc.Additive for, treatment fluid for, and method of plugging a tubing/casing annulus in a well bore
US6716798Apr 22, 1999Apr 6, 2004Burts Jr Boyce DConformance improvement additive, conformance treatment fluid made therefrom, method of improving conformance in a subterranean formation
US8002049 *Dec 3, 2007Aug 23, 2011Schlumberger Technology CorporationWell treating method to prevent or cure lost-circulation
US8371381May 19, 2010Feb 12, 2013Schlumberger Technology CorporationEngineered fibers for well treatments
US8776882Jan 6, 2013Jul 15, 2014Schlumberger Technology CorporationEngineered fibers for well treatments
US20100152070 *Dec 7, 2009Jun 17, 2010Jaleh GhassemzadehDrilling lost circulation material
EP2196516A1Dec 11, 2008Jun 16, 2010Services Pétroliers SchlumbergerLost circulation material for drilling fluids
Classifications
U.S. Classification507/104, 241/19, 241/28, 19/5.00R, 241/14
International ClassificationC09K8/50, C09K8/514
Cooperative ClassificationC09K8/514
European ClassificationC09K8/514