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Publication numberUS2812160 A
Publication typeGrant
Publication dateNov 5, 1957
Filing dateJun 30, 1953
Priority dateJun 30, 1953
Publication numberUS 2812160 A, US 2812160A, US-A-2812160, US2812160 A, US2812160A
InventorsBinder Jr George G, Freeman Jr William A, West Robert C
Original AssigneeExxon Research Engineering Co
Export CitationBiBTeX, EndNote, RefMan
External Links: USPTO, USPTO Assignment, Espacenet
Recovery of uncontaminated cores
US 2812160 A
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Description  (OCR text may contain errors)

2 Sheets-Sheet 1 R. c. wEs'r Erm.V v

RECOVERY oF UNCONTAMINATED coREs Nov. s, 1957 Fuga June so, 1953 ma()` ATTORNEYk R. C'. WEST ETAL RECOVERY 0F UNCONTAMINATED CORES Nov. 5, 1957 2 Sheets-Sheet 2 Filed June 30, 1953.

BORE I-IOLE ORE BARREL INNER BARREL OUTER BARREL OUTT INGS MOVING UF FROZEN CORE LIQUID EXPANSION VALVE AUGER TO 4CARRY OUTTINGB TO .CUTTING BASKET |NvENToRs BINDERJR AN .JR

ATTO RN E Y United `States Patent O 2,812,160 Y RECOVERY F UNCONTAMINATED CORES Robert C. West, George G. Binder, Jr., and William A. Freeman, Jr., Tulsa, Okla., assignors to Esso Research and Engineering Company, a corporation of Delaware Application June 30, 1953, Serial No. 365,206

2 Claims. (Cl. Z55-1.4)

The present invention is concerned broadly with the production of oil. The invention is more specically concerned with the recovery of uncontaminated cores during a coring operation. In oil well drilling practice, a sample of subsurface rock penetrated in the course of drilling operations isreferred-to as a core. The operation by which such a sample is obtained in order to ascertain the properties of a given formation is known in the art as coring. The devices employed to collect these cores are known as core barrels and are usually so constructed as to be attached to the lower end of a drill pipe. In accordance with the present invention, an uncontaminated core is secured by freezing the core as it is being recovered from the earths substrata.

The cores obtained by all types of core barrels known at present are essentially similar in the respect that these cores are exposed to a constantly diminishing pressure from the moment the core begins its upward movement until it arrives at the surface. Mineral oil and gas found in subsurface foundations are generally under a high pressure which is commonly referred to as the formation pressure. The extent of this pressure depends upon the depth of the formation and in general is proportional to the hydrostatic pressure exerted on the formation in which oil or gas is found. It is a well known fact that when oil or gas-bearing formations are exposed to a pressure lower than the formation pressure, the oil or gas contained in them has a tendency to expand and leave the formation. Consequently, the reduction in pressure on a core obtained by present methods of coring during its travel to the surface brings about a considerable change in theoil and gas content of the core, thereby rendering the core unreliable.

Thus, one diiculty has been to secure a core accurately representing the exact nature of the earths substrata'from which it was removed. This is particularly critical in view of a growing interest in water flooding and other secondary recovery methods, since it is essential that a direct and accurate measurement of residual oil and water saturations be determined prior to employing a selected secondary recovery operation.

At the present time estimates of residual oil saturation in the reservoir can be obtained from past production records, data on crude oil, interstitial water content, porosity, pay sand, and the like. However, lack of knowledge of some of the above factors, together with such features and oil migration and water influx, make estimat ing residual oil saturation in the depleted reservoir prior to secondary recovery operations uncertain. In accordance with the present invention, a core is frozen or cooled in situ as it is being cored, thus preventing or substantially reducing the migration of oil and water from the core, or the adsorption of oil and other contaminants from sources foreign to the core.

The process of the present invention may be more fully understood by reference to the drawings illustrating one apparatus which is satisfactory for freezing or chilling the core in situ as it is being recovered.

Fig. 1 is a sectional view in elevation showing a portionl of the drill string of the apparatus.

ice

Fig. 1a is a vertical sectional view of a portion of the outer barrel and core barrel members of the apparatus.

Fig. lb is a vertical sectional view of another portion of the core barrel and outer barrel members of the apparatus and also the coring bit.

Referring specifically to the drawings, a drill stem or string 1 is shown disposed within the borehole 2 penetrating from the earths surface to substrata. A refrigerant pipe 3 lis shown concentrically disposed within the string I1. A packing element 4 closes off the area below the packing from the area above the packing without the refrigerant pipe 3, and within the drill stem. In operation one method is to use a selected refrigerant such as sulfur dioxide, ammonia, freon, and the like, which is pumped down within the drill stem from the earths surface. This refrigerant ows down passageway 23 in refrigerant pipe 3 into a coil 8, positioned in area 5 which is a hollow annular space disposed within the wall portion of the outer barrel 7 of the coring element. The refrigerant flows through this wound coil element 8 in area S and is discharged from the core element through liquid expansion valve 9 into area 5. The refrigerant is vaporized and flows upwardly in area 5, thus chilling the inner barrel 6. The refrigerant flows upwardly through gas return port 10 and passes via annular passageway 21 between refrigerant pipe 3 and the drill string 1 and thence through ports 11 into the area between the drill string and the borehole. A swivel element 12 permits the inner barrel 6 to remain stationary while the outer barrel 7 rotates in the coring operation. Coring bit 13 is positioned at the lower end of the bit element. An auger element 14 is positioned around the outer barrel which causes the cut- Y tings to llow upwardly in the borehole and to be discharged into cutting basket 15.

The process of the present invention is concerned with an operation wherein the core is frozen in situ as it is being recovered. This prevents contamination of the core and also prevents loss of valuable fluids from the core as it is being raised to the earths surface.

What is claimed is:

1. An improved coring apparatus for obtaining an uncontaminated core sample from the earth substrata which comprises in combination a string of drill pipe, an outer barrel member attached to the lower end of the drill string and provided with a coring bit, an inner core receiving barrel concentrically disposed within said outer barrel, means permiting rotation of said outer barrel relative to said inner barrel, a cooling chamber disposed within said outer barrel, a spiral coil conduit Within said cooling chamber and surrounding said inner barrel, irst conduit means arranged to transmit a vaporizable liquid refrigerant from the drill string to one end of said coil, expansion valve means at the opposite end of said coil arranged to vaporize said refrigerant and to discharge the vapors into said cooling chamber, second conduit means for conveying said vapors from said cooling chamber to the annular space between the drill string and the surrounding earth strata, an auger attached to the outer periphery of the outer barrel and arranged to transport drill cuttings upward from the coring bit.

2. An apparatus as defined in claim 1 including a cutting basket arranged to receive said cuttings.

References Cited in the tile of this patent UNITED STATES PATENTSv

Patent Citations
Cited PatentFiling datePublication dateApplicantTitle
US1870696 *Jul 16, 1929Aug 9, 1932Thomas G TaylorSelf cooling, drilling, and coring bit
US2040889 *May 23, 1933May 19, 1936Sullivan Machinery CoCore drill
US2617296 *Dec 20, 1946Nov 11, 1952Core Lab IncProcess for treating core samples
DE329896C *May 24, 1914Dec 1, 1920Charbonnages De Beeringen Sa DVerfahren und Vorrichtung zum Abteufen von Schaechten, insbesondere durch wasserfuehrende Schichten
Referenced by
Citing PatentFiling datePublication dateApplicantTitle
US2905444 *Jul 26, 1957Sep 22, 1959Evalyn ShepardCore barrel
US2915285 *May 23, 1956Dec 1, 1959Jersey Prod Res CoCoring subterranean formations
US3447615 *Mar 11, 1966Jun 3, 1969Schick Clifford LCore sample retrieving apparatus
US3612192 *Apr 14, 1969Oct 12, 1971Maguire James C JrCryogenic drilling method
US3650337 *Jul 31, 1969Mar 21, 1972Aerojet General CoCryogenically cooled drill
US4371045 *Apr 1, 1981Feb 1, 1983The United States Of America As Represented By The United States Department Of EnergyMethod and apparatus for recovering unstable cores
US4809790 *Sep 4, 1987Mar 7, 1989Manchak FrankDevice for sampling soils and retaining volatiles therein and method of using same
US6216804 *Jul 29, 1998Apr 17, 2001James T. AumannApparatus for recovering core samples under pressure
US6230825Jun 30, 2000May 15, 2001James T. AumannApparatus for recovering core samples under pressure
US6305482Jun 30, 2000Oct 23, 2001James T. AumannMethod and apparatus for transferring core sample from core retrieval chamber under pressure for transport
US6378631Jun 30, 2000Apr 30, 2002James T. AumannApparatus for recovering core samples at in situ conditions
US6659204Feb 8, 2001Dec 9, 2003Japan National Oil CorporationMethod and apparatus for recovering core samples under pressure
US7000711Feb 9, 2004Feb 21, 2006Ch2M Hill, Inc.Horizontal bore cryogenic drilling method
US7516785Oct 10, 2007Apr 14, 2009Exxonmobil Upstream Research CompanyMethod of developing subsurface freeze zone
US7516787Oct 10, 2007Apr 14, 2009Exxonmobil Upstream Research CompanyMethod of developing a subsurface freeze zone using formation fractures
US7631691Jan 25, 2008Dec 15, 2009Exxonmobil Upstream Research CompanyMethods of treating a subterranean formation to convert organic matter into producible hydrocarbons
US7647971Dec 23, 2008Jan 19, 2010Exxonmobil Upstream Research CompanyMethod of developing subsurface freeze zone
US7647972Dec 23, 2008Jan 19, 2010Exxonmobil Upstream Research CompanyFracturing fluid is injected into well to form fracture at depth of subsurface formation, providing fluid communication between first and second depths in well; cooling fluid is circulated under pressure through well into fracture to cause fluid to flow into subsurface formations, lowering temperature
US7669657Oct 10, 2007Mar 2, 2010Exxonmobil Upstream Research CompanyEnhanced shale oil production by in situ heating using hydraulically fractured producing wells
US8074739 *Mar 12, 2009Dec 13, 2011Jilin UniversitySampling method and sampler for gas hydrates by hole bottom freezing
US8082995Nov 14, 2008Dec 27, 2011Exxonmobil Upstream Research CompanyOptimization of untreated oil shale geometry to control subsidence
US8087460Mar 7, 2008Jan 3, 2012Exxonmobil Upstream Research CompanyGranular electrical connections for in situ formation heating
US8104537Dec 15, 2009Jan 31, 2012Exxonmobil Upstream Research CompanyMethod of developing subsurface freeze zone
US8122955Apr 18, 2008Feb 28, 2012Exxonmobil Upstream Research CompanyDownhole burners for in situ conversion of organic-rich rock formations
US8146664May 21, 2008Apr 3, 2012Exxonmobil Upstream Research CompanyUtilization of low BTU gas generated during in situ heating of organic-rich rock
US8151877Apr 18, 2008Apr 10, 2012Exxonmobil Upstream Research CompanyDownhole burner wells for in situ conversion of organic-rich rock formations
US8151884Oct 10, 2007Apr 10, 2012Exxonmobil Upstream Research CompanyCombined development of oil shale by in situ heating with a deeper hydrocarbon resource
US8230929Mar 17, 2009Jul 31, 2012Exxonmobil Upstream Research CompanyMethods of producing hydrocarbons for substantially constant composition gas generation
US8540020Apr 21, 2010Sep 24, 2013Exxonmobil Upstream Research CompanyConverting organic matter from a subterranean formation into producible hydrocarbons by controlling production operations based on availability of one or more production resources
US8596355Dec 10, 2010Dec 3, 2013Exxonmobil Upstream Research CompanyOptimized well spacing for in situ shale oil development
US8616279Jan 7, 2010Dec 31, 2013Exxonmobil Upstream Research CompanyWater treatment following shale oil production by in situ heating
US8616280Jun 17, 2011Dec 31, 2013Exxonmobil Upstream Research CompanyWellbore mechanical integrity for in situ pyrolysis
US8622127Jun 17, 2011Jan 7, 2014Exxonmobil Upstream Research CompanyOlefin reduction for in situ pyrolysis oil generation
US8622133Mar 7, 2008Jan 7, 2014Exxonmobil Upstream Research CompanyResistive heater for in situ formation heating
US8641150Dec 11, 2009Feb 4, 2014Exxonmobil Upstream Research CompanyIn situ co-development of oil shale with mineral recovery
US8770284Apr 19, 2013Jul 8, 2014Exxonmobil Upstream Research CompanySystems and methods of detecting an intersection between a wellbore and a subterranean structure that includes a marker material
DE10131973A1 *Jul 2, 2001Jan 30, 2003Keller Grundbau GmbhSample obtaining method for a ground treated with hardenable bonding agents or mortar involves insertion of a double-walled pipe into the ground before hardening takes place
DE10131973C2 *Jul 2, 2001Dec 4, 2003Keller Grundbau GmbhVerfahren zur Entnahme von Probekernen
Classifications
U.S. Classification175/17, 175/244, 175/394, 175/310
International ClassificationE21B36/00, E21B25/08, E21B25/00
Cooperative ClassificationE21B25/08, E21B36/001
European ClassificationE21B25/08, E21B36/00B