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Publication numberUS3248046 A
Publication typeGrant
Publication dateApr 26, 1966
Filing dateJul 2, 1965
Priority dateJul 2, 1965
Publication numberUS 3248046 A, US 3248046A, US-A-3248046, US3248046 A, US3248046A
InventorsFeltman Jr John P, Piemonte William J
Original AssigneeFeltman Jr John P, Piemonte William J
Export CitationBiBTeX, EndNote, RefMan
External Links: USPTO, USPTO Assignment, Espacenet
High speed rotor used for centrifugal separation
US 3248046 A
Abstract  available in
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Claims  available in
Description  (OCR text may contain errors)

April 26, 1966 J. P. FELTMAN, JR., ETAL 3,243,046

HIGH SPEED ROTOR USED FOR CENTRIFUGAL SEPARATION Filed July 2, 1965 H l I INVENTORS H Jam r2 FELT/7AM JR.

BY WiLL/ANLLP/E/YU/VTE United States Patent l 3,248,046 HIGH SPEED ROTOR USED FOR CENTRIFUGAL Y SEPARATION John P. Feltman, JL, 1 74th St., Brooklyn, N.Y., and William J. Piemonte, 2135 80th St., Brooklyn, N.Y. Filed July 2, 1965, Ser. No. 469,242 2 Claims. (Cl. 233-26) This is a continuation-in-part of application Ser. No. 361,967, filed April 23, 1964, and now abandoned.

This invention relates to high speed rotors used in centrifuges and more specifically in the construction of a rotor built up of superposed layers of glass fibers that are bonded together to form a balanced solid rotor provided with small tube holding apertures or bores.

Rotors of aluminum, heat treated steel and titanium are well known in the-art. However, all of these rotors are limited to a degree of centrifugal force at which they break down and will disintegrate, for example, the tensile strength of the materials.

Aluminum will not exceed 85,000 lbs. per square inch.

Titanium will not exceed 170,000 lbs. per square inch.

Heat treated steel will not exceed 250,000 lbs. per square inch.

The density of the materials must be considered:

Aluminum .097 Titanium .165 Heat treated steel .285

Thus the strength to Weight ratio is approximately 880,000 lbs. per square inch.

It is also to be noted that spinning buckets are well known in the art. In spinning buckets for rayon or artificial silk, the bucket is formed as a bowl with a central open chamber. These buckets are designed for normal operating speeds of 9000 r.p.m. and according to Patent No. 2,965,220 they will, under test, rupture at 14,900 r.p.m. It is also to be noted that in all of the prior art relating to spinning buckets, the bucket or rotor is constructed as a cylindrical wall extendingfrom a supporting base in which the walls of the bowl are comparatively light or thin and in which the wall may be composed of a fibrous strip with a binder as in Patent No. 2,028,040, or a cellulosic fabric material impregnated and bonded together with a phenolic resin as in Patent No. 2,965,220, or as a fibrous material impregnated with resinoid and reinforced with a circumferentially placed wrapping of stainless steel wire as in Patent No. 2,436,716, or of glass yarn as disclosed in Patent No. 2,594,693, or as a molded bucket having fiber glass in the wall on a reinforcing medium.as disclosed in Patent- No. 2,525,469, or the combination of a glass fiber warp with a cotton fill in a molded bucket of artificial resins as disclosed in Patent No. 2,372,983, or the use of a glass fiber thread or strand as reinforcement in a molded resinous roller as in the Dutch Patent No. 87,740, or the molding of a plurality of layers of a mixture of an organic fibrous material and an acid resistant asbestos woven into a fabric as in Patent No. 2,128,097, but in all the art on spinning buckets the speeds or r.p.m. indicated is a modest 1415,000 r.p.m.

It is also to be noted that pipe is constructed by wrapping glass fibers about a mandrel and impregnating the glass fibers with a thermo setting plastic binder. In all pipe formed by this method there is a comparatively thin pipe wall formed that is exceedingly strong, but never subject to centrifugal forces.

In the presently known rotors the centrifuge that may be constructed of aluminum, titanium or heat treated steel the strength to weight ratio is low, that is while aluminum is light it has a low tensile strength and .')',Z48,046 Patented Apr. 26, 1966 where heat treated steel has a high tensile strength it is heavy. The presently known rotors using metal are operating up to 60,000 r.p.m. In one example of their use that is in the separation of viruses, the rotors operating at 60,000 r.p.m. take from 60 to 70 hours for actual separation of the virus. In the present invention the rotors will operate at 100,000 r.p.m. and the same separation of viruses will be performed in from 2 to 3 hours.

In the present invention the article or rotor is formed as a solid body as in all rotors designed for holding tubes or bottles for centrifugal separation processes. Also in the present invention the rotor must be capable of extremely high r.p.m. to produce a centrifugal force over 250,000 X gravity and up to 325,000 gs, for the separation of certain viruses in a reasonably minimum time in clinical study.

It is an object of the invention to provide a high speed rotor for holding tubes or bottles for'centrifugal separation of substances requiring a force of over 250,000 X gravity.

It is a further object of this invention to provide a high speed rotor for holding tubes or bottles in a centrifuge in which the rotor is constructed solely of glass fiber filament wound in superposed layers and impregnated with a thermosetting binder to form a solid body that is capable of withstanding a centrifugal force in excess of 250,000 'X gravity.

Other objects of this invention will be apparent by reference to the detailed description and the drawings in which FIG. 1 is a plan view of a rotor.

FIG. 2 is a side view partially in cross section, and

FIG. 3 is an elevational view illustrating the method of forming the rotor.

Referring to the drawings there is illustrated a rotor member R, FIGS. 1 and 2 which is constructed as illustrated in FIG. 3 by winding upon a mandrel 24 a narrow strip or strand of glass fiber material 10 while a plastic material such as resin is sprayed by gravity upon each convolution of the glass fiber material simultaneously with the winding of the glass fiber material. The glass fiber strand is fed through a guiding member 66 passing through a hub member 12 which is slotted lengthwise so as to exert friction upon the glass fiber thread to cause the thread to Wind over the mandrel 24 with a uniform predetermined tension. The rotation of the mandrel 24 and the simultaneous back and forth operation of the glass fiber thread 10 by means of the movement of the guiding member 66 back and forth produces a uniform coiling of the strand 10 over mandrel 24 and continues to superpose layers of strand one-upon the other to build up the rotor body R. One end of mandrel 24 as shown in FIG. 3 is supported by the point 18 fitted in the tail stock spindle of a winding machine while the opposite end of mandrel 24 is supported by the head stock of the winding machine. The head stock receiving the reduced end 15 of mandrel 24. Positioned between disc 13 and the superposed layers of strand 10 is a second disc 16 having a pin 17 extending laterally therefrom for engaging an opening in disc 13 thus keying the disc member 16 to disc 13 of the head stock. To assist in forming the rotor. R there is provided a cylindrically shaped member 19 mounted on the tail stock for rotary movement only. A hub 20 is mounted on the cylindrically shaped member 19 for sliding movement. Member 20 is formed with a disc portion 21, the disc portion having a diameter corresponding to the larger coiled diameter of the rotor to be formed, the cylindrical member 19 and the disc 21 serving to hold the glass fiber strand 10 in a plane at right angles to the axis of the mandrel during the coiling of the glass fiber thread. The sliding movement of disc 21 on the cylindrically shaped member 19 is affected manually and is set by a pin 23 engaging a groove 50 as shown in FIG. 3. Thus the disc may be set in the dotted position for winding and forming rotor R as illustrated. A sleeve 26 may be placed over the mandrel 24 to prevent the adherence of the plastic material to the mandrel and thus permit removal of the rotor after the cooling of the plastic material. Likewise a disc .25 of an appropriate material may be placed against the face of disc 21 and another disc 25 may be placed against the face of disc 16. Thus the strand 10 will not adhere to either disc or to the mandrel and the rotor R may be easily removed. To start the winding of the strand 10 upon mandrel 24', one

end of strand is hooked to the discs 13 and 16 and coiled over the sleeve 26 at a pitch corresponding to the size of the fiber glass thread used and the winding is continued with the strand 10 being fed through hub member 12 and by movement of guide member 66, the actual'desired contour of rotor R may be formed as shown in FIG. 3. The rotor R is removed from mandrel 24 and then cured forming an integral body from the wound strand 10. The rotor R may then be treated as a solid body for machining its outer periphery to provide a perfect balance or any variation in shape as desired. It may also be drilled to provide a plurality of cylindrical bores L1, L2, L3, L4, L5, etc., of a size to permit the insertion of laboratory tubes as illustrated in FIG. 2 thus completing the rotor R for use in a centrifuge. The glass fiber material or strand 10 approximates .075 lb. per cubic inch. The tensile strength of this strand is approximately 200,000 plus lbs. per square inch. Thus the strength to weight ratio equals 4.75 which is a strength to weight ratio of 2,700,- 000 inches approximately. Thus the tensile strength of the rotor R, because of the relatively low density and high strength of the glass fiber as bonded together, possesses a weight to strength ratio of approximately 240% above that of any other material heretofore used for rotors and due to its build up of superposed layers into a solid or integrally formed rotor, the rotor R does trifugal separation of materials, it is to be understood that the bores may be varied in their shape to retain any desired type of tube or bottle and the number of bores may be varied according to the particular type of rotor utilized and the size of the rotor may be varied, that is, a small rotor will be utilized for the extremely high rpm. while a larger rotor may be utilized for a lesser rpm. and desired centrifugal force for separation.

strength strand, namely, glass fiber bonded together to provide the strongest possible rotor for extremely. high r.p.m. operation'and extremely high centrifugal force for separation :as a centrifuge. Changes in the glass fiber as to its contour whether round, square, etc., may be made as long as the fiber retains its lightweight and high tensile strength. without departing from the spirit of this inlationship, said bores extending radially into said rotor so that the base of the bores are positioned in a greater;

diametrical relation than the upper portion of said bores.

2. A solid rotor for a centrifuge which may be sub-.

jected to a stress of'250,000 X gravity during its oper ation, comprising a generally cylindrical form having its 1 lower portion with a greater diameter than -its upper. portion and formed of superposed layers of binder treated glass fiber with the turns of one layer being overlapped by the turns of the next layer whereby the glass fiber filaments of all layers are interlocked into an internal balanced rotor having uniform density, the external layers of said rotor provided with atv least two small bottle holding bores that are radially spaced in equal and dynamically balanced relationship, said bores extending radially into said rotor.

References Cited by the Examiner UNITED STATES PATENTS 2,028,040 1/1936 Benge 57--76 2,128,097 8/1938 Mains 5776 X 2,372,983 4/ 1945 Richardson 5776 2,436,726 2/ 1948 Moyer 57-76 2,525,469 10/195'0 Anderson 57-76 2,594,693 4/ 1952 Smith 5776 X 2,965,220 12/1960 Naul 5776X FOREIGN PATENTS 87,740 3/ 1958 Netherlands.

M. CARY NELSON, Primary Examiner;

It is also to be understood that the rotor R is solely constructed of the lightest weight toughest tensile 1

Patent Citations
Cited PatentFiling datePublication dateApplicantTitle
US2028040 *Mar 14, 1933Jan 14, 1936Continental Diamond Fibre CoSpinning bucket
US2128097 *Mar 15, 1934Aug 23, 1938Westinghouse Electric & Mfg CoAcid resisting laminated product
US2372983 *Mar 29, 1944Apr 3, 1945Gen ElectricSpinning bucket
US2436726 *Aug 10, 1945Feb 24, 1948Westinghouse Electric CorpCentrifuge bucket
US2525469 *Jul 26, 1947Oct 10, 1950Westinghouse Electric CorpSpinning bucket and method of making it
US2594693 *Dec 7, 1948Apr 29, 1952Sharples CorpHollow circular article and method of making same
US2965220 *Feb 13, 1958Dec 20, 1960Westinghouse Electric CorpSpinning bucket
NL87740C * Title not available
Referenced by
Citing PatentFiling datePublication dateApplicantTitle
US3794241 *Jun 19, 1972Feb 26, 1974Szentesi PRotor for high speed centrifuges
US4102490 *Jun 6, 1977Jul 25, 1978Beckman Instruments, Inc.Data ring for vertical tube rotor
US4360149 *Nov 10, 1980Nov 23, 1982Hein Jr George NCentrifuge rotor with liquid supported swinging tubes
US4639320 *Feb 19, 1986Jan 27, 1987United Coal CompanyCentrifuging, minimized vibration
US4640770 *Feb 19, 1986Feb 3, 1987United Coal CompanyApparatus for extracting water from solid fines or the like
US4701157 *Aug 19, 1986Oct 20, 1987E. I. Du Pont De Nemours And CompanyLaminated arm composite centrifuge rotor
US4817453 *Jan 22, 1988Apr 4, 1989E. I. Dupont De Nemours And CompanyFiber reinforced centrifuge rotor
US4860610 *Jan 27, 1988Aug 29, 1989E. I. Du Pont De Nemours And CompanyWound rotor element and centrifuge fabricated therefrom
US5057071 *Aug 21, 1989Oct 15, 1991Beckman Instruments, Inc.Hybrid centrifuge rotor
US5362301 *Jun 21, 1993Nov 8, 1994Composite Rotors, Inc.Fixed-angle composite centrifuge rotor
US5382219 *Feb 25, 1994Jan 17, 1995Composite Rotor, Inc.Ultra-light composite centrifuge rotor
US5562582 *Jan 17, 1995Oct 8, 1996Composite Rotor, Inc.Ultra-light composite centrifuge rotor
US5643168 *May 1, 1995Jul 1, 1997Piramoon Technologies, Inc.Compression molded composite material fixed angle rotor
US5776400 *Dec 2, 1996Jul 7, 1998Piramoon Technologies, Inc.Method for compression molding a composite material fixed angle rotor
US5876322 *Feb 3, 1997Mar 2, 1999Piramoon; AlirezaHelically woven composite rotor
US6056910 *May 27, 1997May 2, 2000Piramoon Technologies, Inc.Process for making a net shaped composite material fixed angle centrifuge rotor
US6635007Jul 17, 2001Oct 21, 2003Thermo Iec, Inc.Method and apparatus for detecting and controlling imbalance conditions in a centrifuge system
US7938627Nov 11, 2005May 10, 2011Board Of Trustees Of Michigan State UniversityWoven turbomachine impeller
US8147392 *Feb 24, 2009Apr 3, 2012Fiberlite Centrifuge, LlcFixed angle centrifuge rotor with helically wound reinforcement
US8273202Mar 27, 2012Sep 25, 2012Fiberlite Centrifuge, LlcMethod of making a fixed angle centrifuge rotor with helically wound reinforcement
US8323169 *Nov 11, 2009Dec 4, 2012Fiberlite Centrifuge, LlcFixed angle centrifuge rotor with tubular cavities and related methods
US8449258Apr 18, 2011May 28, 2013Board Of Trustees Of Michigan State UniversityTurbomachine impeller
US8506254Apr 18, 2011Aug 13, 2013Board Of Trustees Of Michigan State UniversityElectromagnetic machine with a fiber rotor
US20100216622 *Feb 24, 2009Aug 26, 2010Fiberlite Centrifuge, LlcFixed Angle Centrifuge Rotor With Helically Wound Reinforcement
US20110111942 *Nov 11, 2009May 12, 2011Fiberlite Centrifuge, LlcFixed angle centrifuge rotor with tubular cavities and related methods
EP0283098A2 *Mar 17, 1988Sep 21, 1988Ultra-Centrifuge Nederland N.V.A centrifuge for separating liquids
EP0290686A1 *May 11, 1987Nov 17, 1988Beckman Instruments, Inc.Composite material rotor
WO1993025315A1 *Jun 9, 1993Dec 23, 1993William J CassinghamFixed-angle composite centrifuge rotor
WO1994015714A1 *Jan 14, 1994Jul 21, 1994Composite Rotors IncUltra-light composite centrifuge rotor
WO1996035156A1 *Apr 30, 1996Nov 7, 1996Piramoon Technologies IncCompression molded composite material fixed angle rotor
Classifications
U.S. Classification494/16, 494/81
International ClassificationB04B5/00, B04B5/04
Cooperative ClassificationB04B5/0414
European ClassificationB04B5/04B2