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Publication numberUS3398754 A
Publication typeGrant
Publication dateAug 27, 1968
Filing dateJun 27, 1966
Priority dateJun 27, 1966
Publication numberUS 3398754 A, US 3398754A, US-A-3398754, US3398754 A, US3398754A
InventorsDenis Tughan Victor
Original AssigneeGallaher Ltd
Export CitationBiBTeX, EndNote, RefMan
External Links: USPTO, USPTO Assignment, Espacenet
Method for producing a reconstituted tobacco web
US 3398754 A
Abstract  available in
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Claims  available in
Description  (OCR text may contain errors)

Aug. 27, 1968 v. D TUGHAN METHOD FOR PRODUCING A RECONSTITUTED TOBACCO WEB Filed June 27, 1966 United States Patent() I 3,398,754 METHOD FOR'PRODUCING A RECONSTITUTED TOBACCO WEBv i t Victor Denis Tughan, Belfast, Northern Ireland, assignor to Gallaher Limited, a British company I Filed June 27, 1966, Ser. No. 560,594 2 Claims. (Cl. 131143) of the tobacco into'web fOl'H'lJAS a result, the web has low strength. It: is not always permissible or desirable to adulterate tobacco productswith binders, fillers, gums, or other additives to increase the strength of the web. Another previous disadvantage in using a tobacco web, either as a filler or as a wrapper, has been that the reconstituted web does not have the full aroma andfiavour of original tobacco. Normal paper web production techniques have to be modified when making atobacco web because the essential constituents of the tobacco which give it its characteristic flavour and aroma are water soluble and would be lost during the preparation and concentration of a fibre slurry corresponding to a papermakers slurry. One way of overcoming this problem has been to extract the soluble constituents of the tobacco,

and these may amount to between 30% and 60% by weight, with water and to concentrate the solution to a thick viscous liquid using, for example, a climbing film evaporator. A paper web is then made out of the insoluble constituents of the original tobacco, which are usually found to be mainly cellulose, and subsequently the two faces of the web are coated with th e concentrated solution. However this is not entirely successful because excessive heating is required to concentrate the solution of the soluble constituents of tobacco'and this heating breaks down many of' the constituents, such'as protein, causes some constituents to'interact chemically so"ch ang ing' their composition, and resinifies' other constituents, such as pectin, a natural'gurn present in tobacco. The resulting flavour and aromaof'the tobacco is poor and a burnt taste is introduced. w I

In accordance with thepresent invention a method of producing a powdered tobacco extract comprises extracting the soluble constituents from tobacco with solvent, atomising the solution and evaporating the minute droplets quickly with a hot gas to form a powder of the solute. I I v II The isolation of the essential constituents off'the tobacco must be' brought about extremely quickly so that the solute'inthe' atomised solution is notat the temperature of the hot drying gas for long enough for i an appreciable degradation of the flavour-giving constituents or pectin to take place. We find that these criteria are satisfied'if the'atomisatio'n and evaporation is carried out in a'spray drier. The pressure in'the spray drier may be sub-'atmospherici in which case the evaporation will take placeat a lower temperature and even less degradation will take place. V I I I I The extraction of the soluble constituents of the original tobacco is preferably carried out with water although other solvents whichdo not're'act chemically with the tobacco may be used. The gas with which the atomised solution is evaporated may be, for example, air o'r'riitrogen, air being preferred owing to its convenience.

The powdered solute which is produced by evaporating the atomised solution forms in effect a concentrated toice bacco extract and contains substantially in their original form, all the essential constituents of the original tobacco which give it its characteristic flavour and aroma. This powdered extract itself forms an important intermediate product and it may prove to be an efficient way of transporting the essential constituents of tobacco 'in a light form. The powder must, however, be kept in an airtight container, because it is hygroscopic.

The most important use for the powdered tobacco extract is in the preparation of a tobacco web wherein a concentrated solution of the tobacco extract is applied as a coating to a paper web. I

Although the paper web may be any suitable absorbent paper, it is preferably itself prepared by conventional paper making techniques from the non-soluble residue of an extraction process in which the soluble constituents of the tobacco have been extracted with a solvent, particularly during the preparation of the powdered tobacco extract.

, In the latter case all the constituents of the original tobacco sample are used and the coated tobacco web has many valuable uses. Thus it has substantially the same smoking qualities and burning rate as natural tobacco but has a very much more even texture and colouringdoes not dry out and is not subject to fragmentation and tobacco products made from it do not have to be kept in an absolutely airtight package. The web may be shredded for use as a filler in cigars or cigarettes or as a pipe tobacco but the real advantage lies in the use of the web as a hinder or wrapper for cigars products. Indeed, we believe that strips of the coated web can be used as a wrapper in a continuous tobacco rod making machine. Not only is there the advantage that the web can be made from otherwise waste tobacco, which itself represents a big saving, but in the case of use as a cigar wrapper, the web replaces, and is in many cases superior to conventional wrapper which consists of the very finest quality and most expensive leaf.

When the coated tobacco web is to be used as an 'outer wrapper, the appearance of its surface which is to be used outermost, may subsequently be improved by spray or roller painting with a dispersion of finely divided tobacco in water. The finely divided tobacco may be produced by a jet pulverisation technique.

The process is open to infinite variation in the blending of different tobaccos both in the production of the uncoated tobacco web and in the production of the coating solution. Thus in order to vary the quality and strength of the coated tobacco web, the powder extracted from one sample of tobacco may be used to coat a tobacco web prepared from the residue of a different extraction. Also the amount of tobacco extract with which a particular tobacco web is coated may be significantly different from the amount extracted from the sample the residue of which is made up into that particular tobacco web. Typi- "cally the coating solution may have a concentration varying between 2 lbs. and 10 lbs. per gallon of water which the uncoated tobacco web will absorb. The coating gives therefore the uncoated tobacco web may in theory be prepared from the residue of a stem or lamina extraction alone, in practice it will be prepared from about 50% of each and for convenience both stem and lamina may be mixed prior to extraction. However, in some circumstances, for example in making a superior quality wrapper, it may be desirable to make up the coating solution from a greater proportion of powder extracted from lamina than from stem. In this case it is necessary to extract from the stem and lamina separately and then if necessary to blend suitable proportions of stem and lamina extracts from the same or different tobaccos prior to making up the coating solution.

One example of the preparation of a coated tobacc web using a powdered tobacco extract in accordance with the invention is illustrated in the accompanying diagram.

Two hundred gallons of water from a back water storage tank 1, which can be made up with fresh water through a line 2, are fed through a line 3 to a mixing vessel 4 containing a perforated bottom plate 5 and a paddle 6. The water is raised to a temperature of 70 C. by means of steam supplied through a line 7 to a jacket 8 around the vessel 4. 200 lbs. of Sumatra stem and 200 lbs. of assorted scrap cigar lamina are then added to the water in the vessel 4 above the plate 5. With the temperature in the vessel maintained at 70 C., the mixture is gently agitated by the paddle 6 for thirty minutes and the water is continuously extracted from the bottom of the vessel below the plate 5 by a pump 9 and recirculated back to the vessel through lines 10 and 11. After this period, during which the water extracts a large proportion of the soluble constituents of the tobacco, the solution is pumped by the pump 9 from beneath the plate 5 through the line 10 and a line 12 into a tank 13 where it is kept moving by a paddle 14. The solution pumped into the tank 13 has a concentration of extracted tobacco of about 4.5% by weight. A further 200 gallons of water are then added from the tank 1 through the line 3 to the wet tobacco in the vessel 4. With the vessel still maintained at 70 C. this second batch of water is recirculated for a further 30 minutes through the vessel 4 and around the lines 10 and 11. The solution resulting from this second percolation is then pumped from beneath the plate 5 through the lines 10 and 12 into the tank 13. The second volume of solution has a concentration of approximately 2% by weight and the total volume collected in the tank 13 from the two percolations is about 250 gallons with a concentration of about 3%. This represents the greater part of the soluble flavour-giving constituents and pectin present in the original tobacco. The lost 150 gallons of water remain absorbed in the fibrous residue of the tobacco in the vessel 4 above the plate 5.

The homogeneous solution in the tank 13 is then pumped by a pump 15 through a line 16 into a header tank 17 in which the head is kept constant by an overflow line 18 leading back to the tank 13. The solution in the tank 17, which has now cooled to below 60 C. is allowed to flow under gravity through a line 19 at a flow rate of 50 gallons per hour into a centrifugal atomising head 20 of a spray drier 21. The spray drier is fed through a line 22 with air at between 200 and 250 C. and a flow rate of 2000 cubic feet per minute. The extracted tobacco solution thrown outwards from the head 20 atomises and is almost instantaneously evaporated by the air into a fine powder with a particle size of slightly larger than ten microns. The powder is carried by the air flow, as shown by the arrows in the drawing, through the bottom outlet of the spray drier 21 through a line 22 into a twin cyclone 23 where the air is exhausted through a line 24 and the powder settles into a container 25. The outlet air temperatures from the spray drier is between 105 and 110 C. The container 25 is sealed when full to prevent moisture reaching the hygroscopic tobacco extract powder which is stored for subsequent use.

A paper web is then made from the fibrous residue in the vessel 4 as follows.

940 gallons of fresh water from the tank 1 are added to the residue in the vessel 4 through the line 3 and the mixture is agitated by the paddle 6 for an hour to break up the fibre whilst the temperature is maintained at C. The fibre water suspension is then continuously recirculated from abovethe plate 5 by a pump 26 through a line 27, a cone refiner28, and lines 29 and 30 back to the vessel 1. A bypass line 31 enables the refiner 28 to be bypassed for a short period if desired. The recirculation is carried out with the temperature of the vessel 4 maintained at 90 C. and a motor load of amps on the refiner 28. The required degree of refining, which controls the fibrillation and hence the strength of the web to be made is reached after between 1 and 2 hours, usually about 1 hours. The suspension is then diluted to 2 /z% by weight and pumped through a line 32 into tanks 33 and 34 where the suspension is agitated by paddles 35 in the tanks 33 and 34. If any outsized particles remain, they may be eliminated by passing the suspension through a deflaker 36 in a line 37 in parallel with the line 29 as the suspension is pumped over into the tanks 33 and 34.

The agitated suspension is then pumped over from the tanks 33 and 34 by a pump 38 through a line 39 into a header tank 40 in which a constant head is maintained by an overflow line 41 returning to the tanks 33 and 34. A line 42 is provided for pumping the suspension from the tanks'33 and 34 back to the vessel 4 should further refining in the refiner 28 be found to be necessary.

The fibre suspension is allowed to fiow from the header tank 40 under gravity through a feed line 43 into a mixing box 44 in which it flows over a weir 45 and out through a feed line 43 into a mixing box 44 in which it flows over a weir 45 and out through a line 46 into a trough 47 at the end of a conventional paper making machine 48. The suspension is distributed by the trough 47 over the upper surface of a moving wire bed 49 with a concentration of between 25 and 75, but preferably about 45, gms. per sq. metre dry weight. The backwater drains through the bed 49 onto a table 50 and into a backwater tank 51. The backwater is pumped by a pump 52 through a line 53 into the mixing box 44, so that tobacco particles draining through the bed 49 are recovered, and in order to maintain the concentration in the mixing box 44 at approximately by weight tobacco fibre. If the tank 51 becomes too full the water pours over a weir 54 and is pumped by a pump 55 through a line 56 back into the back water storage tank 1. The fibres on the moving table 49 matt together and form a tobacco web 57 which is picked up and squeezed by felt rollers 58, and passes over a hot drum 59, heated by steam through a line 60, before the web is wound on a reel 61 with a moisture content of 25% to 35% by weight.

The tobacco web 57 from the reel 61 is then coated with a concentrated solution ofthe powder tobacco extract, or blend of such extracts, from the, or similar, containers 25. The solution is made up in a header tank 62 which is surrounded by an electrical heating mantle. The powder is placed in the tank 62 and water from the tank 1 is added through a line 63 until the concentration of tobacco powder in Water is at a desired figure of between 2 lbs. and 10 lbs. per gallon. The mixture is stirred with a paddle 64 until all the powder has dissolved and the solution is preheated up to 50 C. The coating can then begin. The tobacco web 57 on the reel 61 is trained over an idler roller 65 and down between a pair of nip rollers 66. The solution from the tank 62 passes down under gravity through a line 67 and forms a pool on top of the nip on both sides of the web 57. As the web 57 passes down through the nip, it absorbs through both its faces the solution of tobacco powder before passing through a first tunnel dryer 68 which reduces its moisture content from between 40 and 45% by weight down to approximately 30% by weight. The excess coating solution from the pool on top of the nip drops into a tank 69 and is recirculated back through a line 70 to the tank 62 by a pump 71.

The upper surface of the coated web is then spray painted, to give it a desired even colour and finish, through a spray head 72. The paint is a suspension of finely comminuted tobacco which has a concentration of one part of comminuted tobacco to three and a half parts of water and is prepared in a tank 73 containing a paddle 74. The comminuted tobacco has a particle size of between 1 and 6 microns, preferably about 3 microns and is produced in a fluid energy mill. The painted coated tobacco web then passes through a second tunnel dryer 75 which reduces its moisture content down to between 20% and 30% by weight after which it is wound on a reel 76.

The web on the reel 76 is then ready for use as a binder or wrapper, after slitting; or for use as a filler, after shredding. The spray painting step would normally be omitted if the web was to be used other than as a wrapper.

The equilibrium moisture content of the web is 15% at 60% relative humidity and 17% at 70% relative humidity. These high values ensure that the web is strong and yet flexible.

The reeling and unreeling of the web 57 on the reel 61 could be eliminated in which case the web would pass directly from the drying drum 59 to the nip between the rollers 66.

I claim:

1. A method of producing a reconstituted tobacco web, said method comprising extracting from a sample of tobacco its water soluble components with water to form a solution, immediately feeding said solution to a spray drier whereby said solution is atomised and evaporated with hot air in said spray drier to form a powder tobacco extract, breaking up and refining the nonsoluble residue of said water extraction to form a fibrous mass, preparing a paper web from a suspension of said fibrous mass and coating at least one surface of said paper web with a concentrated solution of said powdered tobacco extract in water.

2. A method according to claim 1, wherein said paper web is coated with said solution as said paper web passes downwards through a pair of nip rolls.

References Cited UNITED STATES PATENTS 3,120,233 2/1964 Battista et a1 131-143 X 3,255,760 6/1966 Selke 131-143 X 3,298,378 1/1967 Stevens et a1 131-143 3,316,919 5/1967 Green et a1 131-143 MELVIN D. REIN, Acting Primary Examiner.

Patent Citations
Cited PatentFiling datePublication dateApplicantTitle
US3120233 *Sep 25, 1961Feb 4, 1964Fmc CorpMethod for manufacturing recon-stituted tobacco products
US3255760 *Aug 3, 1962Jun 14, 1966Kimberly Clark CoTobacco product which produces less tars
US3298378 *Jan 30, 1964Jan 17, 1967Kimberly Clark CoMethod of making a tobacco product
US3316919 *Apr 21, 1964May 2, 1967Brown & Williamson TobaccoProcessing of smoking tobacco
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US4068671 *Jul 25, 1975Jan 17, 1978Amf IncorporatedNicotine removal process
US4109664 *Mar 1, 1977Aug 29, 1978Brown & Williamson Tobacco CorporationSmoking materials
US4131117 *Dec 21, 1976Dec 26, 1978Philip Morris IncorporatedMethod for removal of potassium nitrate from tobacco extracts
US4768527 *Jan 23, 1987Sep 6, 1988R. J. Reynolds Tobacco CompanyTobacco material processing
US4848373 *Apr 13, 1987Jul 18, 1989Helme Tobacco CompanyMixing with alkaline agent in aerobic environment
US4962774 *Nov 16, 1988Oct 16, 1990R. J. Reynolds Tobacco CompanyTobacco reconstitution process
US4986286 *May 2, 1989Jan 22, 1991R. J. Reynolds Tobacco CompanySpray-dried aqueous extract in glycerol on alumina beads as cigarette replacements
US4987906 *Sep 13, 1989Jan 29, 1991R. J. Reynolds Tobacco CompanySolvent extraction, separation, shaping, contacting with phosphate
US4989620 *Sep 19, 1988Feb 5, 1991Philip Morris IncorporatedSurface treatment with flavors, adjuvants
US5005593 *Oct 26, 1988Apr 9, 1991R. J. Reynolds Tobacco CompanyProcess for providing tobacco extracts
US5056537 *Sep 29, 1989Oct 15, 1991R. J. Reynolds Tobacco CompanyCigarette
US5060669 *Dec 18, 1989Oct 29, 1991R. J. Reynolds Tobacco CompanyTobacco treatment process
US5131415 *Apr 4, 1991Jul 21, 1992R. J. Reynolds Tobacco CompanyTobacco extraction process
US5143097 *Jan 28, 1991Sep 1, 1992R. J. Reynolds Tobacco CompanyTobacco reconstitution process
US5159942 *Jun 4, 1991Nov 3, 1992R. J. Reynolds Tobacco CompanyProcess for providing smokable material for a cigarette
US5197494 *Jun 4, 1991Mar 30, 1993R.J. Reynolds Tobacco CompanyTobacco extraction process
US5318050 *Dec 18, 1992Jun 7, 1994R. J. Reynolds Tobacco CompanyTobacco treatment process
US5325877 *Jul 23, 1993Jul 5, 1994R. J. Reynolds Tobacco CompanyTobacco reconstitution process
US5327917 *Aug 17, 1992Jul 12, 1994R. J. Reynolds Tobacco CompanyHumectants, binders, tobacco pectins
US5339838 *Aug 17, 1992Aug 23, 1994R. J. Reynolds Tobacco CompanyContacting an aqueous slurry with a pectin release agent; crosslinking
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US5499636 *Apr 20, 1995Mar 19, 1996Philip Morris IncorporatedCigarette for electrical smoking system
US5501237 *Sep 30, 1991Mar 26, 1996R. J. Reynolds Tobacco CompanyInsoluble water extract formed into sheet, contacted with pect pectin release agent, crosslinking
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US5715844 *Dec 21, 1995Feb 10, 1998R. J. Reynolds Tobacco CompanyTobacco reconstitution process
US5908034 *Dec 8, 1997Jun 1, 1999Brown & Williamson Tobacco CorporationMethod for making a band cast reconstituted tobacco sheet using steam exploded tobacco
US5947128 *Dec 8, 1997Sep 7, 1999Brown & Williamson Tobacco CorporationMethod for making a reconstituted tobacco sheet using steam exploded tobacco
US6026820 *Sep 12, 1997Feb 22, 2000Philip Morris IncorporatedCigarette for electrical smoking system
US7900639Jan 17, 2007Mar 8, 2011R. J. Reynolds Tobacco CompanyReconstituted tobaccos containing additive materials
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Classifications
U.S. Classification131/374
International ClassificationA24B15/12, A24B15/00
Cooperative ClassificationA24B15/12
European ClassificationA24B15/12
Legal Events
DateCodeEventDescription
May 19, 1981AS02Assignment of assignor's interest
Owner name: GALLAHER LIMITED
Owner name: HERGALL (1981) LIMITED
Effective date: 19810306
May 19, 1981ASAssignment
Owner name: GALLAHER LIMITED
Free format text: CHANGE OF NAME;ASSIGNOR:WATLING FIFTY-ONE LIMITED;REEL/FRAME:003858/0227
Effective date: 19810220
Free format text: ASSIGNMENT OF ASSIGNORS INTEREST.;ASSIGNOR:HERGALL (1981) LIMITED;REEL/FRAME:003858/0222
Effective date: 19810306
Owner name: GALLAHER LIMITED, STATELESS
Free format text: ASSIGNMENT OF ASSIGNORS INTEREST;ASSIGNOR:HERGALL (1981) LIMITED;REEL/FRAME:003858/0222