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Publication numberUS3556048 A
Publication typeGrant
Publication dateJan 19, 1971
Filing dateSep 5, 1968
Priority dateSep 5, 1968
Publication numberUS 3556048 A, US 3556048A, US-A-3556048, US3556048 A, US3556048A
InventorsFrazer Robert E
Original AssigneeNasa
Export CitationBiBTeX, EndNote, RefMan
External Links: USPTO, USPTO Assignment, Espacenet
Vacuum evaporator with electromagnetic ion steering
US 3556048 A
Abstract  available in
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Claims  available in
Description  (OCR text may contain errors)

United States Patent TO GUNS I ELECTRON GUN 114 r13 12 POWER SUPPLY V P SERVO SERVO SERVO CONTROLLED CONTROLLED CONTROLLED REGULATEO REGULATED REGULATED POWER SUPPLY POWER SUPPLY POWER SUPPLY SERVO UNIT CONTROL [72] inventors T. O. Paine [56] References Cited Deputy Administrator of the National UNITED STATES PATENTS iz r g zfis gfg fi' 3,211,128 10/1965 Putter et a1. 1 17/106 7 R i F aw Canada Calif 3,205,087 9/1965 Allen 117/106 [2!] App] No 7:71:62; r 1 1 3,117,022 1/1964 Bronson et al.. 204/192 9 I Filed Sept 5,1968 3,046,936 7/1962 S1mons 117/106 Patented Jan. 19, 1971 Primary Examiner-John H. Mack Assistant Examiner-Sidney S1 Kanter Attorneys-Monte F. Mott, J. H. Warden and G. T. McCoy [54] VACUUM EVAPORATOR WITH [0N STEERING ABSTRACT: An apparatus for vaporizing material in a high alms rawmg vacuum chamber is disclosed. The apparatus includes an elec- [52] US. Cl 118/495, tromagnetic arrangement comprising a plurality of coils. The 1 204/298 coils are controllably energized to produce a rotating mag- [51 Int. Cl C23c 13/08 netic field in the path of the vaporized material or ions to con- Field 01 Search 1 17/932, trollably steer them to selected points of the chambers inner 106; 204/192; 118/49, 49.], 49.5 surface.

' PMENTE U: JAM 9 I871 v TO sums ELECTRON sun 1 T I POWER SUPPLY sERvo SERVO SERVO CONTROLLED CONTROLLED CONTROLLED -35 REGULATED REGULATED REGULATED Pw PP ERSP P UPPY 0 ER su LY POW A u PLY OWER s L INVENTOR- 1 1 ROBERT E. FRAZER SERVOv ATTORNEYS 1 VACUUM EvAroRAToR WITH ELECTROMAGNETIC [N s'rsssmc ORIGIN O l-INVENTION- The invention described herein' was "made in the performance of work under a NASA- contract and is subject to the provisions of Section 305 of theNationaI Aeronautics and Space Act of I958, Public Law-85 568 (72 Stat. ,435; 42 USC I BACKGROUND OF THE INVENTION 1. Field of the Invention I This invention generally relates to? an apparatus for evaporating substancesin high vacuum and, more particularly, to improvementstherein.v t

2. Description of the Prior Art Many devices have been designed and developed to evaporate materials, for example, metals, in high vacuum to produce films. Typically, a container, often referred to as a crucible supports the material to be evaporated in a vacuumtight housing. The material is evaporated by electron bombardment. The evaporated material, consisti'ng'of ions carrying neutral atoms, is used to coat a substrate, or simply condense over a selected surface to form a film. Generally, the area of the desired film surface is relatively small. Con sequently, a single crucible may be employed to contain the material which, after evaporation, produces the film.

However, difficult problems arise whenever the surface to be coated is quite large; In the prior art. attempts have been made to produce a largedeposited film by utilizing a plurality of crucibles (sources). Such an arrangement is satisfactory only'if the uniformity of the film is not particularly critical. However, if filmcoating has to be of highly uniform thickness or has to meet specific thickness requirements, a multicrucible arrangement has been found to be of very limited use. The need for film coatings of relatively large surface area and of a high degree of uniformity. exists in both commercial and military applications. For example, the need is present whenever it is necessary toproduce large diameter mirrors for solar simulators, solar energy converters, large antenna dishes, and the like.

OBJECTS AND SUMMARY OF rus'mvsm'ron It is a primary object of the present invention'to provide a newimproved apparatus for evaporating substances, such as metals and nonmetals, to produce a relatively large deposited film.

Another object of the present invention is to provide improvements in an evaporation apparatus in order to control deposition of evaporant onto a relatively large surface area.

A further object of the present invention is to provide highly reliable means which are easily controllable to control the deposition of vaporized films onto a relatively large surface area. I

These and other objects of the invention are achieved by providing improved means in a vacuumtight housing in which a material is evaporated, in order to control the steering of the evaporated material towards a relatively large surface area to be coated therewith. Briefly, in one embodiment, theimproved steering means consists of a plurality, such as three, coils wound around an annular ring which is placed above a crucible, in which evaporant is heated by electron bombardment. Ions, carrying with them neutral atoms, which are released from the hot material surface pass throughthe field of the coils. The coils are energized by a polyphase current to produce a controlled rotating magnetic field, whose rate of rotation and amplitude arecontrolled'by controlling the phase and amplitudes of the currents, suppliedto thethree coils. It is the controlled rotatingmagnetic field which is used to steer the ions as they pass through the magnetic field so that they are controllably deposited to form the desired large surface film.

The novel features of the invention are set forth with particularity in the appended claimsrThe invention will best be understood from the following description when read in conjunction with the accompanying drawings.

BRIEF DESCRIPTION OF THE DRAWING The FIG. is a combination block and modified cross-sectional diagram of a material deposition apparatus which incorporates the present invention.

DESCRIPTION OF THE PREFERRED EMBODIMENTS 1 In the FlG., three electron beam guns l2. l3 and 14 are shown spaced approximately from each otheraround crucible 8. The electron beams, suppliedwith power from an electron gun power supply 15, are designed to produce streams of electrons or electron beams which are aimed at the center of evaporant 9 in crucible 8. In order to simplify the drawing, the connections between power supply 15 and the various guns are deleted. Various commercially available electron guns may be employed. In one embodiment actually reduced to practice, each of guns l2, l3 and 14, consisted of a 10 kilowatt gun of the 270 bent beam type, manufactured by Airco Temescal, a Division of Air Reduction Company at Berkeley, California.

As is appreciated by those familiar with the art, the function of the electron beams is to heat evaporant 9, and cause it to evaporate. The vapor, in the form of ions carrying neutral atoms, which in the FIG. are designated by dashed lines 17, leaves crucible S'andtravels toward a substrate 18, shown supported in housing 7 by a support member 19. The vapor, upon striking the surface of substrate 18, which is assumed to be of a relatively large area, condenses to form a film thereon.

In accordance with the teachings of the present invention, in order to control the uniformity of the film deposited on the surface of substrate 18, an annular ring 20 is placed above crucible 8. The ring is provided with three inwardly directed projections, which are spaced approximately l20 apart, and serve as magnetic pole pieces 21, 22 and 23. Electrically conductive coils 31, 32 and 33 are wound around the annular ring 20, intermediate the inwardly directed projections. Coils 31, 32 and 33 are connected to respective servo controlled regulated power supplies 35, 36 and 37. The leads of the various coils extend through the walls of housing 7 and are insulated therefrom by vacuumtight insulators, generally designated by reference numeral 39. Power supplies 35, 36 and 37 are shown connected to a servocontrol unit 40.

The basic function of the annular ring 20, the three coils wound thereabout and the servocontrol power assembly, consisting of power supplies 35, 3'6, 37 and servocontrol unit 40, is to control the direction of the'ions which pass through ring '20 so that when the ions strike the surface of substrate 18 a film of selected characteristics is deposited thereon. That is, the function of such means is to controllably steer the ions toward a controlled point on the surface of the substrate 18. The controlled steering is accomplished by controlling, by means of servocontrol unit 40, the amplitudes and the relative phases of the currents supplied to the three coils in order to produce a controlled rotating magnetic field about ring20. By

three power supplies to produce a magnetic field rotating at a rate of three cycles per second. Such a field was used to steer ions emanating from a single crucible to form a deposit of aluminum on a 23 foot diameter surface for use as a solar simula- It should be appreciated by those familiar with the art that various servocontrol techniques may be employed in the design of servocontrol unit 40 in order to control the amplitudes in the relative phases of current supplied by a plurality, such as 3, power supplies. Therefore, the unit 40 is not described in further detail.

There has accordingly been shown and described herein novel means for controllably steering vapor or ions towards a relatively large surface area in order to produce a film of selected controlled characteristics. The means include a plurality of windings which are energized to produce a rotating magnetic field. As the ions pass through the rotating magnetic field, their direction is affected thereby so that they strike the surface on which the film is to be formed at a controlled point.

It is appreciated that those familiar with the art may make modifications and/or substitute equivalents in the arrangements as shown. For example the coils 31, 32 and 33 need not be positioned in a single plane as shown in the FIG. Rather they may be positioned in any desired configuration or relative positions with respect to one another. The only requirement is that the magnetic fields produced by the currents in the coils. when combined, result in a controllable magnetic field with which the ions passing therethrough are steerable towards the desired surface. Therefore, all such modifications and/or equivalents are deemed to fall within the scope of the invention as defined in the appended claims.

lclaim:

1. Apparatus for producing a film of a vaporizable substance comprising:

a vacuumtight housing;

an open-topped crucible for holding a substance to be evaporated;

means for vaporizing said substance to convert at least a part thereof; and i electromagnetic means positioned in a plane above said crucible for providing a rotating magnetic field to control the direction of said vaporized substance toward a selected surface in said housing.

2. The apparatus as recited in claim 1 wherein said electromagnetic means for providing a rotating magnetic field surrounds an area through which flows said vaporized substance.

3. The apparatus as recited in claim 2 wherein said means for vaporizing include a plurality of electron guns, and means providing power to said guns to direct streams of electrons to heat and vaporize said substance by electron bombardment.

4. The apparatus as recited in claim 3 wherein said electromagnetic means include a plurality of coils disposed above said crucible, and servo controlled power supply means for controlling the amplitudes and relative phases of electrical current supplied to said coils to produce a magnetic field rotating at a preselected rate.

5. The apparatus as recited in claim 4 wherein said electromagnetic means include a ring disposed in said plane and said plurality of coils being wound and equidistantly spaced on said ring.

6. In a vacuum deposition apparatus for vaporizing a vaporizable material. means for vaporizing said material to form ions. the improvement comprising; electromagnetic means surrounding a portion of the path of said ions to provide a rotating magnetic field for controlling the directions thereof.

7. The apparatus as recited in claim 6 wherein said electromagnetic means comprise a plurality of windings surrounding an area in the path of said ions and means for energizing said windings to produce an electromagnetic field of selected characteristics which extends across said path to control the direction of flow of the ions pas sin therethrough.

8. The apparatus as recited in c arm 7 wherein the number of windings is at least three, equidistantly spaced from one another.

9. The apparatus as recited in claim 8 wherein said means for energizing provide said three windings with a polyphase current to produce said rotating magnetic field.

Patent Citations
Cited PatentFiling datePublication dateApplicantTitle
US3046936 *Jun 4, 1958Jul 31, 1962Nat Res CorpImprovement in vacuum coating apparatus comprising an ion trap for the electron gun thereof
US3117022 *Sep 6, 1960Jan 7, 1964Space Technhology Lab IncDeposition arrangement
US3205087 *Dec 15, 1961Sep 7, 1965Martin Marietta CorpSelective vacuum deposition of thin film
US3211128 *May 31, 1962Oct 12, 1965Kretschmar George GVacuum evaporator apparatus
Referenced by
Citing PatentFiling datePublication dateApplicantTitle
US3669860 *Apr 1, 1970Jun 13, 1972Zenith Radio CorpMethod and apparatus for applying a film to a substrate surface by diode sputtering
US3693582 *Feb 10, 1970Sep 26, 1972CockerillApparatus for applying a metal coating to an elongated metal article
US3974059 *Oct 3, 1974Aug 10, 1976Yoichi MurayamaHigh vacuum ion plating device
US4153005 *Jul 6, 1977May 8, 1979United Technologies CorporationMultiple electron beam vacuum vapor deposition apparatus
US5354445 *Jul 22, 1993Oct 11, 1994Mitsubishi Denki Kabushiki KaishaThin film-forming apparatus
US5458754 *Apr 15, 1994Oct 17, 1995Multi-Arc Scientific CoatingsPlasma enhancement apparatus and method for physical vapor deposition
US6139964 *Jun 6, 1995Oct 31, 2000Multi-Arc Inc.Plasma enhancement apparatus and method for physical vapor deposition
US20040173160 *Mar 18, 2004Sep 9, 2004Carlo MisianoApparatus for thin film deposition, especially under reactive conditions
EP0271682A1 *Oct 29, 1987Jun 22, 1988Leybold AktiengesellschaftVacuum vapour deposition assembly with a rectangular vaporizer crucible and several elektron beam guns
EP0411482A2 *Jul 27, 1990Feb 6, 1991Anelva CorporationElectron gun arrangement for use in the electron beam evaporation process
Classifications
U.S. Classification118/723.0EB, 118/726, 204/298.5, 118/723.0VE
International ClassificationC23C14/24, C23C14/32, H01J37/305, H01J37/317
Cooperative ClassificationC23C14/32, H01J37/3053, C23C14/24, H01J37/3178
European ClassificationC23C14/24, H01J37/317C, C23C14/32, H01J37/305B