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Publication numberUS3795483 A
Publication typeGrant
Publication dateMar 5, 1974
Filing dateSep 21, 1972
Priority dateJul 7, 1969
Also published asDE1934363A1, DE1934363B2
Publication numberUS 3795483 A, US 3795483A, US-A-3795483, US3795483 A, US3795483A
InventorsGrafingholt A
Original AssigneeLever Brothers Ltd
Export CitationBiBTeX, EndNote, RefMan
External Links: USPTO, USPTO Assignment, Espacenet
Method and device for sterilising of containers
US 3795483 A
A method of sterilising stackable containers by the effects of a sterilising gas before they are filled and closed in which the containers to be sterilised are stacked one inside the other, are exposed to the effects of sterilising gas in a sterilisation chamber and are subjected to strong fluctuations in pressure of the gas at successive intervals, after which the containers are filled and sealed under sterile conditions.
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Description  (OCR text may contain errors)

United States Patent 1191 Grafingholt 1 1 Mar. 5, 1974 [541 METHOD AND DEVICE FOR STERILKSKNG 3,206,275 9/1965 Sair ct a1 .I ..'21 5s OF CONTAINERS 3,409,389 11/1968 Bjork 21/56 3,436,170 4/1969 Lodge i. 21/56 1 1 lnventorl Alfred Graflngholt, g, 3,494,725 2 1970 lrons ct al 21/56 Germany 3,511,022 5/1970 Finley ct al. 21/78 UX 1731 Assigneez Lever Brothers Company, New 3322??? 31133,; 322222221.$1311....5:311:31i11 York, N.Y. 7 a [22] Filed: Sept. 21, 1972 FORElGN PATENTS OR APPLlCATlONS I 542,554 1/1942 Great Britain 21/94 [21] Appl' 291151 698,972 10 1953 Great Britain 21 94 Related US. Application Data [63] iCantgnuatj-ion of Ser. No. 52,208, July 6, 1970, Primary Examiner Barry S. Richman am one Att0rney, Agen t, or F rm-Lever Brothers Company [30] Foreign Application Priority Data July 7, 1969 Germany 1934363 [57] ABSTRACT U-S. f sterilising Stackable containers the 21/78 21/91 21/92 21/93 2l/94 21/95 fects of a sterilising gas before they are filled and 51 I Cl 21/ 4 closed in which the containers to be sterilised are 'l i 1/00 13/00 A611 13/02 stacked one inside the other, are exposed to the ef- 1 0 a 2156758 D fects of sterilising gas in a sterilisation chamber and 91-98 78 are subjected to strong fluctuations in pressure of the 56 gas at successive intervals, after which the containers 1 References Clted are filled and sealed under sterile conditions.

UNITED STATES PATENTS- 7/1962 McConnell 1. 21/D 1G. 4

4 Claims, 3 Drawing Figures PATENTEDHAR 51914 3.795.483


sum 2 0F 3 Inventor ALFRED GRAFINGl lOLT PATENTED 3.795.483

sum .3 or 3 Inventor METHOD AND DEVICE FOR STERHLHSHNG 01F (IQNTAKNERS This is a continuation of application Ser. No. 52,208, filed July 6, i970, and now abandoned.

The invention relates to a method of sterilising prefabricated, stackable packaging containers before they are filled and closed, sterilisation being effected by means of a sterilising gas. The invention also relates to devices for carrying out this method.

It is known to pass flat packaging material through a sterilising bath before it is formed into a tube from which bag-like containers are formed after filling, and to keep it in a protective gas atmosphere until the packs have been scaled. It has also been proposed to sterilise cylindrical cans with high-pressure steam before they are filled, the cans being conveyed separately in a straight-like conveyor device through a processing chamber bounded by two rotating gates. in the case of containers of deep-drawn plastics film, attempts have also been made to sterilise these, for example by radiation. Due to the short duration of the treatment and because processing by means of deep-drawing moulds cannot be kept sterile, it is not, however, possible to achieve adequate sterilisation.

The known devices are not suitable for sterilising packaging containers such as tubs or trays adequately in the quantities which can be filled and closed by a fast-running packaging machine. in the case of the plastics packaging containers common today, it must also be noted that atleastin some cases they consist of material which cannot be heated excessively without undergoing undesirable deformation. It is therefore often impossible to sterilise them by means of super-heated steam.

Packaging sensitive liquids or paste-like products, such as fruit juice, oil, mayonnaise, milk, ice cream and processed cheese for example, in prefabricated containers requires sterilisation notonly of these products but also of the packing material in order to extend their storage period. Theobject of the invention is therefore to sterilise prefabricated packaging containers by treating them with a germicidal gas for an adequate time and, if necessary, repeating the treatment with this gas.

. a packaging machine in which they are filled and closed in a sterile atmosphere in a manner known per se. The

lids required for the closure are sterilised in the same way as the containers and conveyed to the packaging machine. According to the invention the fluctuations in pressure in the sterilisation chambers are at least 1/3 and preferably more than 9/10 of the maximum pressure. It was found preferable to allow the pressure of the processing gas to fluctuate several times between approximately 1 atm. and l to 10 mm. mercury column. Before the processing gas is first introduced the sterilisation chamber is evacuated in order to remove most of the air brought in with the containers. Before the containers are discharged to the packaging machine the sterilising gas is likewise removed by evacuation before the sterilisation chamber is filled with the sterile atmosphere used in the packaging machine.

Thanks to the method according to the invention not only is an adequate sterilisation period obtained but as a result of treating the containers and lids in stacks an economic ratio is also achieved between the effective capacity of the containers and the amount of gas required. Even greater economy can be achieved by using the gas several times.

The device provided for putting the method into effect consists of a number of tubular chambers to take the stacks of containers. These chambers can be arranged parallel to one another and mounted rotatably about a common shaft. it is also possible, however, to arrange them in the path of the feed line of the packaging containers, the chambers then being in series.

The device and the method to be carried out with it are described in detail below with the aid of the embodiments illustrated in diagram form in the attached drawings:

FIG. ll shows a cross-section through a device with chambers rotating about a shaft,

FIG. 2 shows a cross-section through chambers arranged in series, and

FIG; 3 shows the chambers arranged according to FIG. 2 in the path of the feed line of the containers to the packaging machine.

In the device according to H0. ll several tubular chambers l are arranged in a type of rotating platform 16. The cross-section of the chambers l is slightly larger than the largest diameter of the containers in the stack of containers 15. The chambers l have at their upper end an inlet opening, the cross-section of which is as large as that of the chambers. This inlet opening can be hermetically sealed by a sealing organ 2, for example in the form of a retractable slide plate. The lower end of the chambers l is constructed in the same way and is hermetically sealed by a similar sealing organ 3. Each of the chambers has at least one pipe connection 5 for vacuum and/or gas. The height of the chambers is approximately the same as the height of a stack of containers which can be filled by the packaging ma chine coupled to the outlet side in a period that depends on the number of chambers and the duration of the sterilisation treatment. The chambers ll arranged in the rotating platform to or suitable supporting arms can be rotated about the shaft 6 so that the chambers i can be connected in one position of the rotating platform M with the feed pipe 12 for the tubs and in another position with the discharge pipe 13 for the sterilised tubs. The rotating platform 16 rotates intermittently so that there is sufficient time for the tubs to be introduced and discharged. On the shaft 6 there is a distributor to provide a link between the connections 5 on the chambers l and the feed pipes ill for vacuum, sterilising gas and protective gas. This distributor consists of a perforated disc ti rotating with the rotating platform 16, from which feed pipes Ml branch off to the connections 5, and a fixed perforated disc 9 to which the pipes 11, through which the gases are introduced or discharged, lead via the control mechanisms '7.

For aprocessingperiod of approximately 15 minutes in the sterilisation device it, chambers El, say, are provided in the rotating platform, each of the chambers ll being able to take a stack of containers which can be handled by the packaging machine in approximately one minute. The individual chambers in this device are moved to the next position about once a minute. The duration of the individual processing operations may be longer or shorter than the time a chamber remains in each position. By operating the control mechanisms it is possible to carry out several operations with the chamber in a single position or to extend a processing operating over several positions of a chamber.

Thus, after a new stack of tubs has been supplied relatively quickly through the feed pipe 12, it is possible to close this chamber by means of the sealing organ 2, then substantially to remove the air by means of a vacuum pump and to introduce sterilising gas into this chamber while it is still in the same position. In another position repeated fluctuations of pressure between a maximum of one atm. and less than mm. mercury column can be induced. These fluctuations in the pressure of the sterilising gas can naturally be extended to several successive positions of the chambers. Before the sterilised tubs pass from the chamber 1 into the discharge pipe 13, which takes the tubs to the packaging machine, by the sealing organ 3 being opened, the chamber 1 is first evacuated and then filled with the protective gas under which the tubs are handled in the packaging machine. Evacuation of the chamber 1 with the sterilised tubs and filling it with protective gas can, if necessary, be repeated several times in order to remove all traces of the sterilising gas.

The device according to the invention and the method to be carried out with it enable the tubs or similar packaging containers to be treated for a sufficient length of time. At the same time the device only requires a relatively small amount of space, as the containers are treated in stacks. The fluctuations of pressure according to the invention enable the stack of containers to be adequately sterilised. Surprisingly they ensure that even the parts of the containers in the interior of the stack are sufficiently exposed to the'sterilising gas.

In the embodiments illustrated in FIGS. 2 and 3 the chambers 1 are in a line. In this case the chambers can be arranged horizontally, vertically or obliquely. There is a sealing organ 4 between every two chambers. By opening this sealing organ 4 a connection is provided between two consecutive chambers. If at the same time a difference in pressure ora flow of gas is produced between these chambers, the stack of tubs can be conveyed from one chamber to the next, even when they are arranged horizontally.

It is nowadays customery to unpack packing materials in a separate room at a higher level and to convey them to the packing machine by exploiting the force of gravity. In this way the sterilisation chambers according to the invention can be arranged in a particularly advantageous way, as shown in FIG. 3. The stacks of tubs pass from a magazine 14, into which the prefabricated tubs are inserted in stacks and from which they are pushed into the first of the chambers I in a known way, through further chambers I, in which they are down in them. The internal cross-section of the chambers l is only slightly larger than the largest crosssection of the stack of containers. The quantity of gas required for sterilisation is kept small by this means.

The chambers to be arranged in series in a line according to FIGS. 2 and 3 make it possible to sterilise the prefabricated containers without additional space being needed for this process if the container feed pipes previously used are replaced by the chambers. The chambers also provide a bufferspace for the packaging material.

Sterilisation canbe carried out at a normal temperature without heating the containers which preferably consist of thermoplastics, by means of gases or mixtures of gases, for example HCl, ethylene oxide, formalin and the like; however, the device is naturally also suitable for treating containers with steam if the material of the containers with steam if the material of the containers permits of such treatment.

What is claimed is:

I. A method of sterilizingrigid preformed stackable containers by the effects of a sterilizing gas before they are filled and closed in which the containers to be sterilized are stacked one inside the other in a nested relationship comprising the steps of a. introducing the containers in a stacked nested configuration to a sterilization chamber, the chamber having a substantially cylindrical interior with an internal diameter slightly larger than the external diameter of the container and a height approximately that of the height of the stack of containers;

chloride, ethylene oxide, steam and formalin.

3. A method as in claim 1 wherein the sterilization gas is hydrogen chloride.

4. A method as in claim 11 wherein the pressure in the steriiization chamber is fluctuated between a maximum of 1 atmosphere and a minimum of 1 mm. mercury column when the sterilization gas is in the sterilization chamber.

Patent Citations
Cited PatentFiling datePublication dateApplicantTitle
US3042533 *Dec 6, 1955Jul 3, 1962Collier Charles PMethod of sterilization
US3206275 *Dec 15, 1961Sep 14, 1965Griffith LaboratoriesPulsation process of gas treatment for fumigation and the like
US3409389 *Sep 16, 1964Nov 5, 1968Getinge Mek Verkst S AktiebolaMethod of removing air from goods in preparation for autoclave sterilization
US3436170 *Jan 5, 1965Apr 1, 1969American Sterilizer CoMethod of sterilizing utilizing steam
US3458275 *Aug 17, 1966Jul 29, 1969Sybron CorpMaterial handling container and method for using the same
US3494725 *Jun 20, 1968Feb 10, 1970American Sterilizer CoPulsing process of sterilization
US3511022 *May 29, 1969May 12, 1970Pet IncAseptic filling apparatus
US3576594 *Jul 24, 1968Apr 27, 1971Lever Brothers LtdProcess for the sterilization of solid surfaces
GB542554A * Title not available
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Referenced by
Citing PatentFiling datePublication dateApplicantTitle
US4164538 *Nov 11, 1977Aug 14, 1979American Sterilizer CompanyLoad conditioning control method for steam sterilization
US4203943 *Nov 11, 1977May 20, 1980American Sterilizer CompanyMethod of biocidal sterilization using cyclic subatmospheric pressure conditioning
US4203947 *Feb 2, 1979May 20, 1980American Sterilizer CompanyLoad conditioning control apparatus for steam sterilization
US4239731 *Nov 21, 1979Dec 16, 1980American Sterilizer CompanyApparatus for biocidal sterilization using cyclic subatmospheric pressure conditioning
US4241010 *Feb 6, 1979Dec 23, 1980American Sterilizer CompanyPressure responsive conditioning control gas sterilization
US4294804 *Jun 25, 1980Oct 13, 1981American Sterilizer CompanyPressure responsive conditioning control gas sterilization
US4348357 *Dec 12, 1980Sep 7, 1982Motorola, Inc.Plasma pressure pulse sterilization
US4457892 *Feb 6, 1979Jul 3, 1984American Sterilizer CompanyBiocidal gas sterilization and gas leakage determination
US6984360 *Feb 4, 1999Jan 10, 2006Sidel S.A.Method and device for sterilizing hollow bodies
US7699080Sep 2, 2008Apr 20, 2010Krones AgApparatus for distributing a medium to containers
US20040063607 *Dec 20, 2001Apr 1, 2004Andrea FetzProcess to improve stability of a pharmaceutical composition
US20090056828 *Sep 2, 2008Mar 5, 2009Krones AgApparatus for distributing a medium to containers
EP2739318A4 *Aug 3, 2012Jan 6, 2016Noxilizer IncIn line sterlizer
WO1982001996A1 *Nov 19, 1981Jun 24, 1982Corp TegalPlasma pressure pulse sterilization
WO1999040949A1 *Feb 4, 1999Aug 19, 1999Sidel S.A.Method and device for sterilising hollow bodies
WO2013022785A2 *Aug 3, 2012Feb 14, 2013Noxilizer, Inc.In line sterlizer
WO2013022785A3 *Aug 3, 2012May 2, 2013Noxilizer, Inc.In line sterlizer
U.S. Classification422/37, 422/36, 422/26, 422/34, 422/28
International ClassificationA61L2/20, B65B55/10, B65B55/04
Cooperative ClassificationB65B55/10, A61L2/20
European ClassificationB65B55/10, A61L2/20