WO2002092956A1 - Jet cutting device with deflector - Google Patents

Jet cutting device with deflector Download PDF

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Publication number
WO2002092956A1
WO2002092956A1 PCT/EP2002/002509 EP0202509W WO02092956A1 WO 2002092956 A1 WO2002092956 A1 WO 2002092956A1 EP 0202509 W EP0202509 W EP 0202509W WO 02092956 A1 WO02092956 A1 WO 02092956A1
Authority
WO
WIPO (PCT)
Prior art keywords
stream
deflector
cutting device
jet cutting
deflection surface
Prior art date
Application number
PCT/EP2002/002509
Other languages
French (fr)
Inventor
Jan Jette Blange
Original Assignee
Shell Internationale Research Maatschappij B.V.
Shell Canada Limited
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Shell Internationale Research Maatschappij B.V., Shell Canada Limited filed Critical Shell Internationale Research Maatschappij B.V.
Priority to AU2002256655A priority Critical patent/AU2002256655B2/en
Priority to MXPA03007979A priority patent/MXPA03007979A/en
Priority to US10/469,893 priority patent/US7017684B2/en
Priority to CA2439912A priority patent/CA2439912C/en
Priority to EA200300976A priority patent/EA004567B1/en
Priority to EP02726148A priority patent/EP1366268B1/en
Priority to DE60211660T priority patent/DE60211660D1/en
Priority to BRPI0207892-9A priority patent/BR0207892B1/en
Publication of WO2002092956A1 publication Critical patent/WO2002092956A1/en

Links

Classifications

    • E—FIXED CONSTRUCTIONS
    • E21—EARTH DRILLING; MINING
    • E21B—EARTH DRILLING, e.g. DEEP DRILLING; OBTAINING OIL, GAS, WATER, SOLUBLE OR MELTABLE MATERIALS OR A SLURRY OF MINERALS FROM WELLS
    • E21B7/00—Special methods or apparatus for drilling
    • E21B7/18—Drilling by liquid or gas jets, with or without entrained pellets
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B05—SPRAYING OR ATOMISING IN GENERAL; APPLYING FLUENT MATERIALS TO SURFACES, IN GENERAL
    • B05B—SPRAYING APPARATUS; ATOMISING APPARATUS; NOZZLES
    • B05B1/00—Nozzles, spray heads or other outlets, with or without auxiliary devices such as valves, heating means
    • B05B1/26—Nozzles, spray heads or other outlets, with or without auxiliary devices such as valves, heating means with means for mechanically breaking-up or deflecting the jet after discharge, e.g. with fixed deflectors; Breaking-up the discharged liquid or other fluent material by impinging jets
    • B05B1/262—Nozzles, spray heads or other outlets, with or without auxiliary devices such as valves, heating means with means for mechanically breaking-up or deflecting the jet after discharge, e.g. with fixed deflectors; Breaking-up the discharged liquid or other fluent material by impinging jets with fixed deflectors
    • B05B1/267—Nozzles, spray heads or other outlets, with or without auxiliary devices such as valves, heating means with means for mechanically breaking-up or deflecting the jet after discharge, e.g. with fixed deflectors; Breaking-up the discharged liquid or other fluent material by impinging jets with fixed deflectors the liquid or other fluent material being deflected in determined directions

Definitions

  • the invention relates to a jet cutting device comprising a cutter head provided with one or more nozzles for ejecting a stream of fluid against a body so as to create a cut in the body.
  • the jet cutting device can be applied, for example, in the industry of machining work pieces or in the industry of rock cutting during drilling of boreholes into the earth formations.
  • WO 00/66872 discloses a rock cutting device whereby a stream of drilling fluid containing abrasive particles is ejected against the borehole bottom or borehole wall by a nozzle provided at a cutter head of the device.
  • a problem of the known device is that the direction of the ejected stream cannot be as optimal as desired in view of limitations regarding the position of the nozzle at the cutter head. For example in certain applications it is desirable that the ejected stream passes close to, and substantially parallel to, the borehole wall in order to accurately cut the borehole circumference. However, the position of the nozzle inwardly from the outer radius of the cutter head prevents such stream direction.
  • a jet cutting device comprising a cutter head provided with at least one nozzle for ejecting a stream of fluid against a body so as to create a selected cut in said body, wherein, for each nozzle, the cutter head is provided with a deflector having a deflection surface arranged to deflect the stream of fluid ejected by the nozzle into a selected direction in accordance with the position of said cut to be created.
  • the ejected stream can be deflected in directions other than the direction of ejection of the stream from the nozzle.
  • the jet cutting device is attractive for wellbore drilling, as it allows to drill a central part of the borehole by a portion of the stream not deflected by the deflector, and to drill a radial outer part of the borehole by a portion of the stream deflected by the deflector positioned close to the borehole wall thus allowing the outer circumference of the borehole to be accurately cut.
  • the deflector suitably has a concave deflection surface onto which the stream impacts.
  • the nozzle can be arranged to eject the stream against a convex deflection surface of the deflector. Since for most applications the intensity of the impact force from the stream on the deflection surface varies somewhat along the surface, suitably the deflection surface has an erosion resistance which varies along the deflection surface in accordance with the variation of the impact force so that the deflection surface is substantially uniformly eroded by the stream.
  • FIG. 2 schematically shows a detail of the embodiment of Fig. 1.
  • a drilling assembly including a drill string 1 extending into a borehole 2 formed in an earth formation 3 and a jet cutting device 5 arranged at the lower end of the drill string 1 near the bottom 7 of the borehole 2, whereby an annular space 8 is formed between the drilling assembly 1 and the wall of the borehole 2.
  • the drill string 1 and the jet cutting device 5 are provided with a fluid passage 9, 9a for drilling fluid to be jetted against the borehole bottom, as is described hereinafter.
  • the jet cutting device 5 has a cutter head 5a provided with a mixing chamber 10 having a first inlet in the form of inlet nozzle 12 in fluid communication with the fluid passage 9, 9a, a second inlet 14 for abrasive particles and an outlet in the form of jetting nozzle 15 directed towards a deflector 16 which is described hereinafter in more detail.
  • a longitudinal extension 5c of cutter head 5a is provided to keep the jetting deflector 16 a selected distance from the borehole bottom 7.
  • a recess 17 is arranged in the cutter head 5a at the side surface thereof, which is in fluid communication with the mixing chamber 10 and with the second inlet 14.
  • Fig. 2 shows a perspective view of the recess 17 whereby a semi-cylindrical side wall 18 of the recess 17 has been indicated.
  • a cylinder 19 rotatable in direction 20 (cf. Fig. 1; in Fig. 2 the cylinder has been removed for clarity purposes) is arranged in the recess 17, the diameter of the cylinder being such that only a small clearance is present between the cylinder 19 and the side wall 18 of the recess 17.
  • the outer surface of the cylinder 19 has been magnetised, whereby a number of N and S poles alternate in circumferential direction.
  • the second inlet 14 and the mixing chamber 10 each have a side wall formed by the outer surface of the cylinder 19. Furthermore, the second inlet 14 has opposite side walls 22, 24 which converge towards the mixing chamber 10 and which extend substantially perpendicular to the side wall 18.
  • the deflector 16 extends into a lower recess 26 of the cutter head 5a in a manner allowing movement of the deflector 16 relative to the cutter head 5a.
  • a control means in the form of actuator 28 is arranged in the lower recess 26 to support the deflector 16 and to control movement of the deflector 16 relative to the cutter head 5a.
  • the deflector 16 is arranged so that during operation of the jet cutting device 5 a stream of fluid 30 ejected by the nozzle 15 impacts onto inner surface 32 of the deflector at a selected angle 34.
  • the inner surface 32 is preferably made of an erosion resistant material like Tungsten Carbide.
  • the actuator 28 is capable of moving the deflector in opposite directions 36a, 36b which are substantially parallel to the deflector inner surface 32 and opposite directions 38a, 38b, which are substantially perpendicular to the deflector inner surface 32.
  • the actuator 28 is capable of rotating the actuator so as to change the angle 34 at which the stream 30 impacts on the deflector inner surface 32.
  • a stream of drilling fluid initially containing abrasive particles is pumped via the fluid passage 9, 9a and the inlet nozzle 12 into the mixing chamber 10.
  • the abrasive particles include a magnetically active material such as martensitic steel, and typical abrasive particles are martensitic steel shot or grit.
  • the stream flows through the jetting nozzle 15 in the form of a jet stream 30 against the deflector 16 which deflects the stream 30 to form deflected stream 40 impacting against the borehole bottom 7.
  • the direction of deflected stream 40 is determined by the angle of impact 34, the deflector shape and the deflector orientation.
  • drilling fluid which is substantially free of abrasive particles is pumped through the passage 9, 9a and the inlet nozzle 12 into the mixing chamber 10.
  • rock particles are removed from the borehole bottom 7.
  • the drill string 1 is simultaneously rotated so that the borehole bottom 7 is evenly eroded resulting in a gradual deepening of the borehole.
  • the rock particles removed from the borehole bottom 7 are entrained in the stream which flows in upward direction through the annular space 8.
  • the abrasive particles are attracted by the magnetic forces induced by cylinder 19, which magnetic forces thereby separate the abrasive particles from the stream and move the particles onto the outer surface of the cylinder 19.
  • the cylinder 16 is induced to rotate a) due to frictional forces exerted to the cylinder by the stream of drilling fluid flowing into the mixing chamber, b) due to frictional forces exerted to the cylinder by the stream flowing through the annular space 8, and c) due to the high velocity flow of drilling fluid through the mixing chamber 10 which generates a hydraulic pressure in the mixing chamber 10 significantly lower than the hydraulic pressure in the annular space 8.
  • the abrasive particles adhered to the outer surface of the cylinder 16 thereby move through the second inlet 14 in the direction of the mixing chamber 10.
  • the converging side walls 22, 24 of the second inlet 14 guide the abrasive particles into the mixing chamber 10.
  • the stream of drilling fluid ejected from the inlet nozzle 12 removes the abrasive particles from the outer surface of the cylinder 19 whereafter the particles are entrained into the stream of drilling fluid.
  • the remainder of the stream flowing upwardly through the annular space 8 is substantially free of abrasive particles and continues flowing upwardly to surface where the drill cuttings can be removed from the stream.
  • the drilling fluid is pumped through the fluid passage 9, 9a and the inlet nozzle 12, into the mixing chamber 10 so as to entrain again the abrasive particles, etc.
  • the actuator 28 When the area of deflector surface 32 where the stream 30 impacts becomes worn, the actuator 28 is induced to move the deflector 16 either in direction 36a or 36b so as to displace said area away from the location of impact and to position a new area of deflector surface 32, not worn, at the location of impact. In this manner it is achieved that the life time of the deflector is increased.
  • the actuator 28 When it is desired to change the direction of the deflected stream 40, the actuator 28 is induced to rotate the deflector so as to change the angle 34 at which the stream 34 impacts on the deflector.
  • the actuator 28 is induced to move the deflector 16 in the direction 38b thereby increasing the distance between the deflector 16 and the stream 30.
  • the actuator 28 is induced to move the deflector 16 in the direction 38a thereby decreasing the distance between the deflector 16 and the stream 30.

Abstract

A jet cutting device comprising a cutter head provided with at least one nozzle for ejecting a stream of fluid against a body so as to create a selected cut in said body, is discloded. For each nozzle, the cutter head is provided with a deflector having a deflection surface arranged to deflect the stream of fluid ejected by the nozzle into a selected direction in accordance with the position of said cut to be created.

Description

JET CUTTING DEVICE WITH DEFLECTOR
The invention relates to a jet cutting device comprising a cutter head provided with one or more nozzles for ejecting a stream of fluid against a body so as to create a cut in the body. The jet cutting device can be applied, for example, in the industry of machining work pieces or in the industry of rock cutting during drilling of boreholes into the earth formations.
WO 00/66872 discloses a rock cutting device whereby a stream of drilling fluid containing abrasive particles is ejected against the borehole bottom or borehole wall by a nozzle provided at a cutter head of the device.
A problem of the known device is that the direction of the ejected stream cannot be as optimal as desired in view of limitations regarding the position of the nozzle at the cutter head. For example in certain applications it is desirable that the ejected stream passes close to, and substantially parallel to, the borehole wall in order to accurately cut the borehole circumference. However, the position of the nozzle inwardly from the outer radius of the cutter head prevents such stream direction.
It is therefore an object of the invention to provide an improved jet cutting device which overcomes the aforementioned problem.
In accordance with the invention there is provided a jet cutting device, comprising a cutter head provided with at least one nozzle for ejecting a stream of fluid against a body so as to create a selected cut in said body, wherein, for each nozzle, the cutter head is provided with a deflector having a deflection surface arranged to deflect the stream of fluid ejected by the nozzle into a selected direction in accordance with the position of said cut to be created.
It is thereby achieved that the ejected stream can be deflected in directions other than the direction of ejection of the stream from the nozzle.
The jet cutting device is attractive for wellbore drilling, as it allows to drill a central part of the borehole by a portion of the stream not deflected by the deflector, and to drill a radial outer part of the borehole by a portion of the stream deflected by the deflector positioned close to the borehole wall thus allowing the outer circumference of the borehole to be accurately cut.
To focus the stream and to increase the cutting efficiency, the deflector suitably has a concave deflection surface onto which the stream impacts. Alternatively, when it is desired to diverge the stream, the nozzle can be arranged to eject the stream against a convex deflection surface of the deflector. Since for most applications the intensity of the impact force from the stream on the deflection surface varies somewhat along the surface, suitably the deflection surface has an erosion resistance which varies along the deflection surface in accordance with the variation of the impact force so that the deflection surface is substantially uniformly eroded by the stream. The invention will be described hereinafter in more detail and by way of example with reference to the accompanying drawings in which Fig. 1 schematically shows a longitudinal section of an embodiment for borehole drilling of the jet cutting device of the invention; and
Fig. 2 schematically shows a detail of the embodiment of Fig. 1. Referring to Fig. 1 there is shown a drilling assembly including a drill string 1 extending into a borehole 2 formed in an earth formation 3 and a jet cutting device 5 arranged at the lower end of the drill string 1 near the bottom 7 of the borehole 2, whereby an annular space 8 is formed between the drilling assembly 1 and the wall of the borehole 2. The drill string 1 and the jet cutting device 5 are provided with a fluid passage 9, 9a for drilling fluid to be jetted against the borehole bottom, as is described hereinafter. The jet cutting device 5 has a cutter head 5a provided with a mixing chamber 10 having a first inlet in the form of inlet nozzle 12 in fluid communication with the fluid passage 9, 9a, a second inlet 14 for abrasive particles and an outlet in the form of jetting nozzle 15 directed towards a deflector 16 which is described hereinafter in more detail. A longitudinal extension 5c of cutter head 5a is provided to keep the jetting deflector 16 a selected distance from the borehole bottom 7. A recess 17 is arranged in the cutter head 5a at the side surface thereof, which is in fluid communication with the mixing chamber 10 and with the second inlet 14.
Fig. 2 shows a perspective view of the recess 17 whereby a semi-cylindrical side wall 18 of the recess 17 has been indicated. A cylinder 19 rotatable in direction 20 (cf. Fig. 1; in Fig. 2 the cylinder has been removed for clarity purposes) is arranged in the recess 17, the diameter of the cylinder being such that only a small clearance is present between the cylinder 19 and the side wall 18 of the recess 17. The outer surface of the cylinder 19 has been magnetised, whereby a number of N and S poles alternate in circumferential direction. The second inlet 14 and the mixing chamber 10 each have a side wall formed by the outer surface of the cylinder 19. Furthermore, the second inlet 14 has opposite side walls 22, 24 which converge towards the mixing chamber 10 and which extend substantially perpendicular to the side wall 18.
The deflector 16 extends into a lower recess 26 of the cutter head 5a in a manner allowing movement of the deflector 16 relative to the cutter head 5a. A control means in the form of actuator 28 is arranged in the lower recess 26 to support the deflector 16 and to control movement of the deflector 16 relative to the cutter head 5a. The deflector 16 is arranged so that during operation of the jet cutting device 5 a stream of fluid 30 ejected by the nozzle 15 impacts onto inner surface 32 of the deflector at a selected angle 34. The inner surface 32 is preferably made of an erosion resistant material like Tungsten Carbide.
The actuator 28 is capable of moving the deflector in opposite directions 36a, 36b which are substantially parallel to the deflector inner surface 32 and opposite directions 38a, 38b, which are substantially perpendicular to the deflector inner surface 32.
Furthermore the actuator 28 is capable of rotating the actuator so as to change the angle 34 at which the stream 30 impacts on the deflector inner surface 32.
During normal operation of the drilling assembly 1, a stream of drilling fluid initially containing abrasive particles is pumped via the fluid passage 9, 9a and the inlet nozzle 12 into the mixing chamber 10. The abrasive particles include a magnetically active material such as martensitic steel, and typical abrasive particles are martensitic steel shot or grit. The stream flows through the jetting nozzle 15 in the form of a jet stream 30 against the deflector 16 which deflects the stream 30 to form deflected stream 40 impacting against the borehole bottom 7. The direction of deflected stream 40 is determined by the angle of impact 34, the deflector shape and the deflector orientation.
After all abrasive particles have been pumped through the fluid passage 9, 9a, drilling fluid which is substantially free of abrasive particles is pumped through the passage 9, 9a and the inlet nozzle 12 into the mixing chamber 10.
By the impact of the jet stream 40 against the borehole bottom 7, rock particles are removed from the borehole bottom 7. The drill string 1 is simultaneously rotated so that the borehole bottom 7 is evenly eroded resulting in a gradual deepening of the borehole. The rock particles removed from the borehole bottom 7 are entrained in the stream which flows in upward direction through the annular space 8. As the stream passes the cylinder 19 the abrasive particles are attracted by the magnetic forces induced by cylinder 19, which magnetic forces thereby separate the abrasive particles from the stream and move the particles onto the outer surface of the cylinder 19. The cylinder 16 is induced to rotate a) due to frictional forces exerted to the cylinder by the stream of drilling fluid flowing into the mixing chamber, b) due to frictional forces exerted to the cylinder by the stream flowing through the annular space 8, and c) due to the high velocity flow of drilling fluid through the mixing chamber 10 which generates a hydraulic pressure in the mixing chamber 10 significantly lower than the hydraulic pressure in the annular space 8. The abrasive particles adhered to the outer surface of the cylinder 16 thereby move through the second inlet 14 in the direction of the mixing chamber 10. The converging side walls 22, 24 of the second inlet 14 guide the abrasive particles into the mixing chamber 10. Upon arrival of the particles in the mixing chamber 10 the stream of drilling fluid ejected from the inlet nozzle 12 removes the abrasive particles from the outer surface of the cylinder 19 whereafter the particles are entrained into the stream of drilling fluid.
The remainder of the stream flowing upwardly through the annular space 8 is substantially free of abrasive particles and continues flowing upwardly to surface where the drill cuttings can be removed from the stream. After removal of the drill cuttings the drilling fluid is pumped through the fluid passage 9, 9a and the inlet nozzle 12, into the mixing chamber 10 so as to entrain again the abrasive particles, etc.
When the area of deflector surface 32 where the stream 30 impacts becomes worn, the actuator 28 is induced to move the deflector 16 either in direction 36a or 36b so as to displace said area away from the location of impact and to position a new area of deflector surface 32, not worn, at the location of impact. In this manner it is achieved that the life time of the deflector is increased. When it is desired to change the direction of the deflected stream 40, the actuator 28 is induced to rotate the deflector so as to change the angle 34 at which the stream 34 impacts on the deflector.
Furthermore when it is desired to increase the diameter of the borehole 2 drilled, the actuator 28 is induced to move the deflector 16 in the direction 38b thereby increasing the distance between the deflector 16 and the stream 30. Conversely, when it is desired to decrease the diameter of the borehole 2 drilled, the actuator 28 is induced to move the deflector 16 in the direction 38a thereby decreasing the distance between the deflector 16 and the stream 30.

Claims

C L A I M S
1. A jet cutting device, comprising a cutter head provided with at least one nozzle for ejecting a stream of fluid against a body so as to create a selected cut in said body, wherein, for each nozzle, the cutter head is provided with a deflector having a deflection surface arranged to deflect the stream of fluid ejected by the nozzle into a selected direction in accordance with the position of said cut to be created.
2. The jet cutting device of claim 1, wherein said pump means is arranged to induce a stream of liquid including abrasive particles through the nozzle.
3. The jet cutting device of claim 1 or 2, wherein the deflection surface is concave.
4. The jet cutting device of any one of claims 1-3, wherein the impact force of the stream on the deflection surface varies along the deflection surface, and wherein the deflection surface has an erosion resistance which varies along the deflection surface in accordance with the variation of the impact force of the stream on the deflection surface so that the deflection surface is substantially uniformly eroded by the stream.
5. The jet cutting device of any one of claims 1-4, wherein the deflector is movable relative to the cutter head, and the jet cutting device further includes control " means for controlling movement of the deflector relative to the cutting head.
6. The jet cutting device of claim 5, wherein the control means is arranged to move the deflector so as to displace a first portion of the deflection surface away from the location at which the stream impacts on the deflection surface, and to position a second portion of the deflection surface at said location.
7. The jet cutting device of claim 5, wherein the control means is arranged to move the deflector so as to change the angle at which said stream impacts on the deflector.
8. The jet cutting device of claim 5, wherein the control means is arranged to move the deflector in a translating movement so as to change the distance between the deflector and said stream.
9. The jet cutting device of any one of claims 1-8, wherein the cutter head forms part of a drill string for drilling a borehole into an earth formation, and wherein each nozzle is arranged to eject a stream of fluid including abrasive particles into the borehole so as to further drill the borehole.
10. The jet cutting device of claim 9, wherein each nozzle is arranged to drill a central part of the borehole by a portion of the stream ejected by the nozzle not deflected by the deflector, and to drill a radial outer part of the borehole by a portion of the stream deflected by the deflector positioned close to the borehole.
11. The jet cutting device substantially as described hereinbefore with reference to the drawings.
PCT/EP2002/002509 2001-03-06 2002-03-06 Jet cutting device with deflector WO2002092956A1 (en)

Priority Applications (8)

Application Number Priority Date Filing Date Title
AU2002256655A AU2002256655B2 (en) 2001-03-06 2002-03-06 Jet cutting device with deflector
MXPA03007979A MXPA03007979A (en) 2001-03-06 2002-03-06 Jet cutting device with deflector.
US10/469,893 US7017684B2 (en) 2001-03-06 2002-03-06 Jet cutting device with deflector
CA2439912A CA2439912C (en) 2001-03-06 2002-03-06 Jet cutting device with deflector
EA200300976A EA004567B1 (en) 2001-03-06 2002-03-06 Jet cutting device with deflector
EP02726148A EP1366268B1 (en) 2001-03-06 2002-03-06 Jet cutting device with deflector
DE60211660T DE60211660D1 (en) 2001-03-06 2002-03-06 LIQUID BEAM CUTTING DEVICE WITH DEFLECTOR PLATE
BRPI0207892-9A BR0207892B1 (en) 2001-03-06 2002-03-06 jet cutting device with baffle.

Applications Claiming Priority (2)

Application Number Priority Date Filing Date Title
EP01302047 2001-03-06
EP01302047.4 2001-03-06

Publications (1)

Publication Number Publication Date
WO2002092956A1 true WO2002092956A1 (en) 2002-11-21

Family

ID=8181768

Family Applications (1)

Application Number Title Priority Date Filing Date
PCT/EP2002/002509 WO2002092956A1 (en) 2001-03-06 2002-03-06 Jet cutting device with deflector

Country Status (13)

Country Link
US (1) US7017684B2 (en)
EP (1) EP1366268B1 (en)
CN (1) CN1318724C (en)
AT (1) ATE327405T1 (en)
AU (1) AU2002256655B2 (en)
BR (1) BR0207892B1 (en)
CA (1) CA2439912C (en)
DE (1) DE60211660D1 (en)
EA (1) EA004567B1 (en)
EG (1) EG23135A (en)
MX (1) MXPA03007979A (en)
MY (1) MY136183A (en)
WO (1) WO2002092956A1 (en)

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AU2002256655B2 (en) 2007-03-29
ATE327405T1 (en) 2006-06-15
US7017684B2 (en) 2006-03-28
MXPA03007979A (en) 2003-12-04
US20040094332A1 (en) 2004-05-20
CN1608165A (en) 2005-04-20
EA200300976A1 (en) 2004-02-26
EP1366268A1 (en) 2003-12-03
CA2439912C (en) 2010-04-27
EG23135A (en) 2004-04-28
CA2439912A1 (en) 2002-11-21
CN1318724C (en) 2007-05-30
DE60211660D1 (en) 2006-06-29
BR0207892A (en) 2004-03-23
BR0207892B1 (en) 2012-02-07
EP1366268B1 (en) 2006-05-24
MY136183A (en) 2008-08-29
EA004567B1 (en) 2004-06-24

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