WO2003087788B1 - A method and apparatus for a downhole refractometer and attenuated reflectance spectrometer - Google Patents
A method and apparatus for a downhole refractometer and attenuated reflectance spectrometerInfo
- Publication number
- WO2003087788B1 WO2003087788B1 PCT/US2003/011095 US0311095W WO03087788B1 WO 2003087788 B1 WO2003087788 B1 WO 2003087788B1 US 0311095 W US0311095 W US 0311095W WO 03087788 B1 WO03087788 B1 WO 03087788B1
- Authority
- WO
- WIPO (PCT)
- Prior art keywords
- sample
- light
- channel
- refractive index
- interface
- Prior art date
Links
- 238000000034 method Methods 0.000 title claims abstract 26
- 230000002238 attenuated effect Effects 0.000 title claims abstract 7
- 239000012530 fluid Substances 0.000 claims abstract 8
- 239000007788 liquid Substances 0.000 claims abstract 2
- 230000005484 gravity Effects 0.000 claims 4
- 238000002835 absorbance Methods 0.000 claims 3
- 230000015572 biosynthetic process Effects 0.000 claims 3
- 238000011109 contamination Methods 0.000 claims 3
- 238000012544 monitoring process Methods 0.000 claims 3
- 238000009835 boiling Methods 0.000 claims 2
- NINIDFKCEFEMDL-UHFFFAOYSA-N Sulfur Chemical compound [S] NINIDFKCEFEMDL-UHFFFAOYSA-N 0.000 claims 1
- 239000005864 Sulphur Substances 0.000 claims 1
- 238000000862 absorption spectrum Methods 0.000 claims 1
- 238000004891 communication Methods 0.000 claims 1
- 238000009834 vaporization Methods 0.000 claims 1
- 230000008016 vaporization Effects 0.000 claims 1
- 238000001845 vibrational spectrum Methods 0.000 claims 1
- 230000005540 biological transmission Effects 0.000 abstract 1
- 238000005259 measurement Methods 0.000 abstract 1
Classifications
-
- E—FIXED CONSTRUCTIONS
- E21—EARTH DRILLING; MINING
- E21B—EARTH DRILLING, e.g. DEEP DRILLING; OBTAINING OIL, GAS, WATER, SOLUBLE OR MELTABLE MATERIALS OR A SLURRY OF MINERALS FROM WELLS
- E21B49/00—Testing the nature of borehole walls; Formation testing; Methods or apparatus for obtaining samples of soil or well fluids, specially adapted to earth drilling or wells
- E21B49/08—Obtaining fluid samples or testing fluids, in boreholes or wells
- E21B49/087—Well testing, e.g. testing for reservoir productivity or formation parameters
-
- G—PHYSICS
- G01—MEASURING; TESTING
- G01N—INVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
- G01N21/00—Investigating or analysing materials by the use of optical means, i.e. using sub-millimetre waves, infrared, visible or ultraviolet light
- G01N21/17—Systems in which incident light is modified in accordance with the properties of the material investigated
- G01N21/41—Refractivity; Phase-affecting properties, e.g. optical path length
-
- E—FIXED CONSTRUCTIONS
- E21—EARTH DRILLING; MINING
- E21B—EARTH DRILLING, e.g. DEEP DRILLING; OBTAINING OIL, GAS, WATER, SOLUBLE OR MELTABLE MATERIALS OR A SLURRY OF MINERALS FROM WELLS
- E21B47/00—Survey of boreholes or wells
- E21B47/10—Locating fluid leaks, intrusions or movements
- E21B47/113—Locating fluid leaks, intrusions or movements using electrical indications; using light radiations
-
- G—PHYSICS
- G01—MEASURING; TESTING
- G01N—INVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
- G01N21/00—Investigating or analysing materials by the use of optical means, i.e. using sub-millimetre waves, infrared, visible or ultraviolet light
- G01N21/17—Systems in which incident light is modified in accordance with the properties of the material investigated
- G01N21/25—Colour; Spectral properties, i.e. comparison of effect of material on the light at two or more different wavelengths or wavelength bands
- G01N21/31—Investigating relative effect of material at wavelengths characteristic of specific elements or molecules, e.g. atomic absorption spectrometry
- G01N21/35—Investigating relative effect of material at wavelengths characteristic of specific elements or molecules, e.g. atomic absorption spectrometry using infrared light
- G01N21/3577—Investigating relative effect of material at wavelengths characteristic of specific elements or molecules, e.g. atomic absorption spectrometry using infrared light for analysing liquids, e.g. polluted water
-
- G—PHYSICS
- G01—MEASURING; TESTING
- G01N—INVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
- G01N21/00—Investigating or analysing materials by the use of optical means, i.e. using sub-millimetre waves, infrared, visible or ultraviolet light
- G01N21/17—Systems in which incident light is modified in accordance with the properties of the material investigated
- G01N21/55—Specular reflectivity
- G01N21/552—Attenuated total reflection
-
- G—PHYSICS
- G01—MEASURING; TESTING
- G01N—INVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
- G01N21/00—Investigating or analysing materials by the use of optical means, i.e. using sub-millimetre waves, infrared, visible or ultraviolet light
- G01N21/01—Arrangements or apparatus for facilitating the optical investigation
- G01N21/03—Cuvette constructions
-
- G—PHYSICS
- G01—MEASURING; TESTING
- G01N—INVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
- G01N21/00—Investigating or analysing materials by the use of optical means, i.e. using sub-millimetre waves, infrared, visible or ultraviolet light
- G01N21/17—Systems in which incident light is modified in accordance with the properties of the material investigated
- G01N21/25—Colour; Spectral properties, i.e. comparison of effect of material on the light at two or more different wavelengths or wavelength bands
- G01N21/31—Investigating relative effect of material at wavelengths characteristic of specific elements or molecules, e.g. atomic absorption spectrometry
- G01N21/35—Investigating relative effect of material at wavelengths characteristic of specific elements or molecules, e.g. atomic absorption spectrometry using infrared light
- G01N21/359—Investigating relative effect of material at wavelengths characteristic of specific elements or molecules, e.g. atomic absorption spectrometry using infrared light using near infrared light
Abstract
Claims
Priority Applications (3)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
BRPI0309090A BRPI0309090B8 (en) | 2002-04-10 | 2003-04-10 | apparatus and method for measuring a refractive index of a fluid sample |
AU2003234713A AU2003234713A1 (en) | 2002-04-10 | 2003-04-10 | A method and apparatus for a downhole refractometer and attenuated reflectance spectrometer |
NO20044579A NO337940B1 (en) | 2002-04-10 | 2004-10-25 | METHOD AND DEVICE FOR MEASUREMENT OF REFRIGERANT INDEX |
Applications Claiming Priority (2)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
US10/119,492 | 2002-04-10 | ||
US10/119,492 US6683681B2 (en) | 2002-04-10 | 2002-04-10 | Method and apparatus for a downhole refractometer and attenuated reflectance spectrometer |
Publications (3)
Publication Number | Publication Date |
---|---|
WO2003087788A1 WO2003087788A1 (en) | 2003-10-23 |
WO2003087788B1 true WO2003087788B1 (en) | 2004-04-15 |
WO2003087788A8 WO2003087788A8 (en) | 2004-07-01 |
Family
ID=28789934
Family Applications (1)
Application Number | Title | Priority Date | Filing Date |
---|---|---|---|
PCT/US2003/011095 WO2003087788A1 (en) | 2002-04-10 | 2003-04-10 | A method and apparatus for a downhole refractometer and attenuated reflectance spectrometer |
Country Status (6)
Country | Link |
---|---|
US (1) | US6683681B2 (en) |
AU (1) | AU2003234713A1 (en) |
BR (1) | BRPI0309090B8 (en) |
NO (1) | NO337940B1 (en) |
RU (1) | RU2318200C2 (en) |
WO (1) | WO2003087788A1 (en) |
Families Citing this family (41)
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US7280214B2 (en) * | 2002-06-04 | 2007-10-09 | Baker Hughes Incorporated | Method and apparatus for a high resolution downhole spectrometer |
US7075063B2 (en) * | 2002-06-26 | 2006-07-11 | Schlumberger Technology Corporation | Determining phase transition pressure of downhole retrograde condensate |
US7002142B2 (en) * | 2002-06-26 | 2006-02-21 | Schlumberger Technology Corporation | Determining dew precipitation and onset pressure in oilfield retrograde condensate |
US7526953B2 (en) * | 2002-12-03 | 2009-05-05 | Schlumberger Technology Corporation | Methods and apparatus for the downhole characterization of formation fluids |
US7081615B2 (en) * | 2002-12-03 | 2006-07-25 | Schlumberger Technology Corporation | Methods and apparatus for the downhole characterization of formation fluids |
DE602004012554T2 (en) * | 2003-05-02 | 2009-04-16 | Baker-Hughes Inc., Houston | OPTICAL PROCESS AND ANALYZER |
US7782460B2 (en) * | 2003-05-06 | 2010-08-24 | Baker Hughes Incorporated | Laser diode array downhole spectrometer |
US7377169B2 (en) | 2004-04-09 | 2008-05-27 | Shell Oil Company | Apparatus and methods for acoustically determining fluid properties while sampling |
US6997055B2 (en) * | 2004-05-26 | 2006-02-14 | Baker Hughes Incorporated | System and method for determining formation fluid parameters using refractive index |
KR20070107759A (en) * | 2005-02-11 | 2007-11-07 | 스와겔로크 컴패니 | Fluid concentration sensing arrangement |
US20070044959A1 (en) * | 2005-09-01 | 2007-03-01 | Baker Hughes Incorporated | Apparatus and method for evaluating a formation |
US7458257B2 (en) * | 2005-12-19 | 2008-12-02 | Schlumberger Technology Corporation | Downhole measurement of formation characteristics while drilling |
US7445934B2 (en) * | 2006-04-10 | 2008-11-04 | Baker Hughes Incorporated | System and method for estimating filtrate contamination in formation fluid samples using refractive index |
EP2005154A4 (en) * | 2006-04-10 | 2012-02-22 | Baker Hughes Inc | System and method for estimating filtrate contamination in formation fluid samples using refractive index |
US7880133B2 (en) * | 2006-06-01 | 2011-02-01 | Weatherford/Lamb, Inc. | Optical multiphase flowmeter |
ATE492796T1 (en) * | 2006-09-20 | 2011-01-15 | Prad Res & Dev Nv | DEVICE AND METHOD FOR OPTICALLY DETERMINING THE PRESENCE OF CARBON DIOXIDE |
US7852468B2 (en) * | 2007-12-14 | 2010-12-14 | Baker Hughes Incorporated | Fiber optic refractometer |
WO2009128977A2 (en) * | 2008-02-12 | 2009-10-22 | Baker Hughes Incorporated | Fiber optic sensor system using white light interferometery |
US8032311B2 (en) | 2008-05-22 | 2011-10-04 | Baker Hughes Incorporated | Estimating gas-oil ratio from other physical properties |
US20100025112A1 (en) * | 2008-07-29 | 2010-02-04 | Baker Hughes Incorporated | In-situ refraction apparatus and method |
US7969571B2 (en) * | 2009-01-15 | 2011-06-28 | Baker Hughes Incorporated | Evanescent wave downhole fiber optic spectrometer |
US20100305872A1 (en) * | 2009-05-31 | 2010-12-02 | University Of Kuwait | Apparatus and Method for Measuring the Properties of Petroleum Factions and Pure Hydrocarbon Liquids by Light Refraction |
AU2009351544B2 (en) | 2009-08-21 | 2013-09-26 | Halliburton Energy Services, Inc. | Nanofiber spectral analysis |
WO2011063086A1 (en) | 2009-11-19 | 2011-05-26 | Halliburton Energy Services, Inc. | Downhole optical radiometry tool |
US8542353B2 (en) | 2010-09-30 | 2013-09-24 | Precision Energy Services, Inc. | Refractive index sensor for fluid analysis |
US8411262B2 (en) | 2010-09-30 | 2013-04-02 | Precision Energy Services, Inc. | Downhole gas breakout sensor |
CA2823716C (en) | 2011-01-04 | 2018-02-13 | Exxonmobil Upstream Research Company | Method and apparatus for a mid-infrared (mir) system for real time detection of petroleum in colloidal suspensions of sediments and drilling muds during drilling, logging, and production operations |
CN102384891A (en) * | 2011-11-29 | 2012-03-21 | 山东建筑大学 | Illegal cooking oil detection device |
US20130135608A1 (en) * | 2011-11-30 | 2013-05-30 | Reflectronics, Inc. | Apparatus and method for improved processing of food products |
CN102590139B (en) * | 2012-02-21 | 2014-01-22 | 中国工程物理研究院流体物理研究所 | Refractive index measuring device of transparent fluid under high pressure |
US9383476B2 (en) | 2012-07-09 | 2016-07-05 | Weatherford Technology Holdings, Llc | In-well full-bore multiphase flowmeter for horizontal wellbores |
US10668408B2 (en) | 2012-11-30 | 2020-06-02 | Suncor Energy Inc | Measurement and control of bitumen-containing process streams |
FI20135064L (en) * | 2013-01-23 | 2014-07-24 | Janesko Oy | A method for measuring the refractive index and a refractometer |
US9733182B2 (en) | 2013-04-04 | 2017-08-15 | Baker Hughes Incorporated | Apparatus and method for determining a fluid property downhole using a bulk reading refractometer |
CN105300920B (en) * | 2015-06-29 | 2018-05-08 | 北京师范大学 | A kind of method based on Terahertz reflectance spectrum extraction solid thin-sheet complex refractivity index |
US20180178261A1 (en) * | 2015-09-22 | 2018-06-28 | Halliburton Energy Services, Inc | Optical Device Window Cleaning System |
US10107741B2 (en) * | 2015-10-07 | 2018-10-23 | Duvas Technologies Limited | Input and output optical systems for multipass spectroscopic absorption cells |
CN106997586B (en) * | 2016-01-25 | 2019-12-20 | 杭州海康威视数字技术股份有限公司 | Object material determination method, device and system |
JP7144388B2 (en) * | 2019-11-21 | 2022-09-29 | トヨタ自動車株式会社 | Method for estimating the concentration of sulfur components in gasoline |
RU2733391C1 (en) * | 2020-04-19 | 2020-10-01 | Федеральное государственное бюджетное учреждение науки Федеральный исследовательский центр «Институт общей физики им. А.М. Прохорова Российской академии наук» (ИОФ РАН) | Method of measuring refractive indices of optical materials in solid state or in form of melt |
CN111982842A (en) * | 2020-08-05 | 2020-11-24 | 北京宏源四方科技开发有限公司 | Fluid analysis nipple for petroleum logging instrument |
Family Cites Families (14)
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US2885923A (en) * | 1954-08-13 | 1959-05-12 | Phillips Petroleum Co | Reflection refractometer |
US2807976A (en) * | 1955-10-11 | 1957-10-01 | Electron Machine Corp | Refractometer |
IL66127A (en) * | 1982-06-24 | 1987-11-30 | Israel State | Method and apparatus for measuring the index of refraction of fluids |
CA1207550A (en) * | 1983-02-18 | 1986-07-15 | James O. Kysilka | Apparatus and method for measuring refractive index of liquids |
GB2142955B (en) * | 1983-07-06 | 1985-08-07 | Nl Petroleum Services | Improvements in or relating to the testing for the presence of native hydrocarbons down a borehole |
JPS6111636A (en) * | 1984-06-27 | 1986-01-20 | Nec Corp | Liquid discriminating sensor |
US4952055A (en) * | 1988-10-03 | 1990-08-28 | Wyatt Technology Corporation | Differential refractometer |
NL8901039A (en) * | 1989-04-25 | 1990-11-16 | Tno | Apparatus for measuring the refractive index of a liquid, in particular intended for measuring the density of that liquid or the concentration of a substance dissolved in that liquid. |
US5166747A (en) * | 1990-06-01 | 1992-11-24 | Schlumberger Technology Corporation | Apparatus and method for analyzing the composition of formation fluids |
US5241859A (en) * | 1990-06-29 | 1993-09-07 | Amoco Corporation | Finding and evaluating rock specimens having classes of fluid inclusions for oil and gas exploration |
US5201220A (en) * | 1990-08-28 | 1993-04-13 | Schlumberger Technology Corp. | Apparatus and method for detecting the presence of gas in a borehole flow stream |
US5167149A (en) | 1990-08-28 | 1992-12-01 | Schlumberger Technology Corporation | Apparatus and method for detecting the presence of gas in a borehole flow stream |
FR2766923B1 (en) * | 1997-07-30 | 1999-10-15 | France Etat | INSTRUMENT FOR MEASURING THE REFRACTION INDEX OF A FLUID |
US5939717A (en) * | 1998-01-29 | 1999-08-17 | Schlumberger Technology Corporation | Methods and apparatus for determining gas-oil ratio in a geological formation through the use of spectroscopy |
-
2002
- 2002-04-10 US US10/119,492 patent/US6683681B2/en not_active Expired - Lifetime
-
2003
- 2003-04-10 AU AU2003234713A patent/AU2003234713A1/en not_active Abandoned
- 2003-04-10 BR BRPI0309090A patent/BRPI0309090B8/en not_active IP Right Cessation
- 2003-04-10 WO PCT/US2003/011095 patent/WO2003087788A1/en active Search and Examination
- 2003-04-10 RU RU2004133038/28A patent/RU2318200C2/en not_active IP Right Cessation
-
2004
- 2004-10-25 NO NO20044579A patent/NO337940B1/en not_active IP Right Cessation
Also Published As
Publication number | Publication date |
---|---|
WO2003087788A1 (en) | 2003-10-23 |
NO20044579L (en) | 2004-12-23 |
NO337940B1 (en) | 2016-07-11 |
US20030193662A1 (en) | 2003-10-16 |
BR0309090A (en) | 2005-03-01 |
WO2003087788A8 (en) | 2004-07-01 |
BRPI0309090B1 (en) | 2016-12-13 |
RU2318200C2 (en) | 2008-02-27 |
BRPI0309090B8 (en) | 2017-03-21 |
AU2003234713A1 (en) | 2003-10-27 |
US6683681B2 (en) | 2004-01-27 |
RU2004133038A (en) | 2005-08-10 |
AU2003234713A8 (en) | 2003-10-27 |
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