WO2004070784A3 - Microporous crystals and methods of making thereof - Google Patents

Microporous crystals and methods of making thereof Download PDF

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Publication number
WO2004070784A3
WO2004070784A3 PCT/US2004/002486 US2004002486W WO2004070784A3 WO 2004070784 A3 WO2004070784 A3 WO 2004070784A3 US 2004002486 W US2004002486 W US 2004002486W WO 2004070784 A3 WO2004070784 A3 WO 2004070784A3
Authority
WO
WIPO (PCT)
Prior art keywords
mixture
room temperature
added
minutes
hours
Prior art date
Application number
PCT/US2004/002486
Other languages
French (fr)
Other versions
WO2004070784A2 (en
Inventor
Matthew Z Yates
J-C James Lin
Original Assignee
Univ Rochester
Matthew Z Yates
J-C James Lin
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Univ Rochester, Matthew Z Yates, J-C James Lin filed Critical Univ Rochester
Publication of WO2004070784A2 publication Critical patent/WO2004070784A2/en
Publication of WO2004070784A3 publication Critical patent/WO2004070784A3/en

Links

Classifications

    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01B—NON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
    • C01B39/00—Compounds having molecular sieve and base-exchange properties, e.g. crystalline zeolites; Their preparation; After-treatment, e.g. ion-exchange or dealumination
    • C01B39/54—Phosphates, e.g. APO or SAPO compounds
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J29/00—Catalysts comprising molecular sieves
    • B01J29/03—Catalysts comprising molecular sieves not having base-exchange properties
    • B01J29/035—Microporous crystalline materials not having base exchange properties, such as silica polymorphs, e.g. silicalites
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J29/00—Catalysts comprising molecular sieves
    • B01J29/82—Phosphates
    • B01J29/83—Aluminophosphates (APO compounds)
    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01B—NON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
    • C01B37/00—Compounds having molecular sieve properties but not having base-exchange properties
    • C01B37/04—Aluminophosphates (APO compounds)
    • C—CHEMISTRY; METALLURGY
    • C30—CRYSTAL GROWTH
    • C30B—SINGLE-CRYSTAL GROWTH; UNIDIRECTIONAL SOLIDIFICATION OF EUTECTIC MATERIAL OR UNIDIRECTIONAL DEMIXING OF EUTECTOID MATERIAL; REFINING BY ZONE-MELTING OF MATERIAL; PRODUCTION OF A HOMOGENEOUS POLYCRYSTALLINE MATERIAL WITH DEFINED STRUCTURE; SINGLE CRYSTALS OR HOMOGENEOUS POLYCRYSTALLINE MATERIAL WITH DEFINED STRUCTURE; AFTER-TREATMENT OF SINGLE CRYSTALS OR A HOMOGENEOUS POLYCRYSTALLINE MATERIAL WITH DEFINED STRUCTURE; APPARATUS THEREFOR
    • C30B29/00—Single crystals or homogeneous polycrystalline material with defined structure characterised by the material or by their shape
    • C30B29/60—Single crystals or homogeneous polycrystalline material with defined structure characterised by the material or by their shape characterised by shape
    • C30B29/605—Products containing multiple oriented crystallites, e.g. columnar crystallites
    • C—CHEMISTRY; METALLURGY
    • C30—CRYSTAL GROWTH
    • C30B—SINGLE-CRYSTAL GROWTH; UNIDIRECTIONAL SOLIDIFICATION OF EUTECTIC MATERIAL OR UNIDIRECTIONAL DEMIXING OF EUTECTOID MATERIAL; REFINING BY ZONE-MELTING OF MATERIAL; PRODUCTION OF A HOMOGENEOUS POLYCRYSTALLINE MATERIAL WITH DEFINED STRUCTURE; SINGLE CRYSTALS OR HOMOGENEOUS POLYCRYSTALLINE MATERIAL WITH DEFINED STRUCTURE; AFTER-TREATMENT OF SINGLE CRYSTALS OR A HOMOGENEOUS POLYCRYSTALLINE MATERIAL WITH DEFINED STRUCTURE; APPARATUS THEREFOR
    • C30B7/00—Single-crystal growth from solutions using solvents which are liquid at normal temperature, e.g. aqueous solutions

Abstract

Novel microporous crystal morphologies are produced by combining a polar solute, a silicon or phosphorous source, and a structure directing agent. A premixed mixture of at least one surfactants and a hydrophobic solvent is added to the previously mixed three species and shaken to for a reverse microemulsion. The microemulsion is stirred overnight, at about room temperature and then iced for five to ten minutes. A metal source is added and vigorously shaken for about two minutes. The mixture is then aged for about two hours at about room temperature. After which, a mineralizer is added and the resultant mixture aged for about two hours at about room temperature. The mixture is then heated to about 100-220°C. The final novel product is then isolated.
PCT/US2004/002486 2003-01-31 2004-01-30 Microporous crystals and methods of making thereof WO2004070784A2 (en)

Applications Claiming Priority (2)

Application Number Priority Date Filing Date Title
US44388503P 2003-01-31 2003-01-31
US60/443,885 2003-01-31

Publications (2)

Publication Number Publication Date
WO2004070784A2 WO2004070784A2 (en) 2004-08-19
WO2004070784A3 true WO2004070784A3 (en) 2004-11-04

Family

ID=32850806

Family Applications (1)

Application Number Title Priority Date Filing Date
PCT/US2004/002486 WO2004070784A2 (en) 2003-01-31 2004-01-30 Microporous crystals and methods of making thereof

Country Status (2)

Country Link
US (1) US20040244673A1 (en)
WO (1) WO2004070784A2 (en)

Families Citing this family (9)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US8148885B2 (en) 2004-12-30 2012-04-03 E. I. Du Pont De Nemours And Company Methods of conditioning getter materials
US20060293169A1 (en) * 2005-02-09 2006-12-28 General Electric Company Molecular structures for gas sensing and devices and methods therewith
US8173995B2 (en) 2005-12-23 2012-05-08 E. I. Du Pont De Nemours And Company Electronic device including an organic active layer and process for forming the electronic device
KR101425232B1 (en) 2006-04-03 2014-08-01 엔테그리스, 아이엔씨. Atmospheric Pressure Microwave Plasma Treated Porous Membranes
JP4229153B2 (en) 2006-08-30 2009-02-25 トヨタ自動車株式会社 Method for producing composite oxide
US20080152577A1 (en) * 2006-12-21 2008-06-26 Addiego William P Ordered mesoporous carbons and method for manufacturing same
US9475040B2 (en) * 2012-12-10 2016-10-25 GM Global Technology Operations LLC Synthesis of Cu/SAPO-34 with variable copper loadings
WO2015138387A2 (en) * 2014-03-10 2015-09-17 University Of Rochester Polarized hydroxyapatite films and methods of making and using same
CN113104860B (en) * 2020-05-14 2024-01-30 青岛大学威海创新研究院 Preparation method of SAPO-34 molecular sieve with bionic pore structure

Citations (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US4904518A (en) * 1988-06-29 1990-02-27 Uop Multiphase composite and processes for preparing same

Family Cites Families (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US6949238B2 (en) * 2003-01-31 2005-09-27 The Regents Of The University Of California Microporous crystals and synthesis schemes

Patent Citations (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US4904518A (en) * 1988-06-29 1990-02-27 Uop Multiphase composite and processes for preparing same

Also Published As

Publication number Publication date
WO2004070784A2 (en) 2004-08-19
US20040244673A1 (en) 2004-12-09

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