WO2004078093A1 - Uniform feed connector for devices for the delivery of active principles - Google Patents
Uniform feed connector for devices for the delivery of active principles Download PDFInfo
- Publication number
- WO2004078093A1 WO2004078093A1 PCT/IB2004/001208 IB2004001208W WO2004078093A1 WO 2004078093 A1 WO2004078093 A1 WO 2004078093A1 IB 2004001208 W IB2004001208 W IB 2004001208W WO 2004078093 A1 WO2004078093 A1 WO 2004078093A1
- Authority
- WO
- WIPO (PCT)
- Prior art keywords
- feed connector
- reservoir
- connector according
- active principles
- connection
- Prior art date
Links
Classifications
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61J—CONTAINERS SPECIALLY ADAPTED FOR MEDICAL OR PHARMACEUTICAL PURPOSES; DEVICES OR METHODS SPECIALLY ADAPTED FOR BRINGING PHARMACEUTICAL PRODUCTS INTO PARTICULAR PHYSICAL OR ADMINISTERING FORMS; DEVICES FOR ADMINISTERING FOOD OR MEDICINES ORALLY; BABY COMFORTERS; DEVICES FOR RECEIVING SPITTLE
- A61J1/00—Containers specially adapted for medical or pharmaceutical purposes
- A61J1/14—Details; Accessories therefor
- A61J1/20—Arrangements for transferring or mixing fluids, e.g. from vial to syringe
- A61J1/2096—Combination of a vial and a syringe for transferring or mixing their contents
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61J—CONTAINERS SPECIALLY ADAPTED FOR MEDICAL OR PHARMACEUTICAL PURPOSES; DEVICES OR METHODS SPECIALLY ADAPTED FOR BRINGING PHARMACEUTICAL PRODUCTS INTO PARTICULAR PHYSICAL OR ADMINISTERING FORMS; DEVICES FOR ADMINISTERING FOOD OR MEDICINES ORALLY; BABY COMFORTERS; DEVICES FOR RECEIVING SPITTLE
- A61J1/00—Containers specially adapted for medical or pharmaceutical purposes
- A61J1/14—Details; Accessories therefor
- A61J1/20—Arrangements for transferring or mixing fluids, e.g. from vial to syringe
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61J—CONTAINERS SPECIALLY ADAPTED FOR MEDICAL OR PHARMACEUTICAL PURPOSES; DEVICES OR METHODS SPECIALLY ADAPTED FOR BRINGING PHARMACEUTICAL PRODUCTS INTO PARTICULAR PHYSICAL OR ADMINISTERING FORMS; DEVICES FOR ADMINISTERING FOOD OR MEDICINES ORALLY; BABY COMFORTERS; DEVICES FOR RECEIVING SPITTLE
- A61J1/00—Containers specially adapted for medical or pharmaceutical purposes
- A61J1/14—Details; Accessories therefor
- A61J1/20—Arrangements for transferring or mixing fluids, e.g. from vial to syringe
- A61J1/2003—Accessories used in combination with means for transfer or mixing of fluids, e.g. for activating fluid flow, separating fluids, filtering fluid or venting
- A61J1/2006—Piercing means
- A61J1/201—Piercing means having one piercing end
Definitions
- the invention also provides a device for delivering active principles comprising a reservoir delimited by at least two lateral walls of substantially cylindrical shape and extending opposite one another, and also including a feed connector having at least one of the preceding characteristics.
- Figures 2a and 2b are a solid view and a sectional view along II- II of a first embodiment of a connector for feeding active principles according to the invention;
- Figures 3a to 3d are variant embodiments of links between the feed connector according to the invention and an active-principle reservoir;
- Figure 9 is a three-dimensional view of a striker to be fitted onto an active-principle receptacle and for cooperating with a feed connector of Figure 10 according to a preferred embodiment of the invention;
- - Figure 10 is a side view of an active-principle feed connector according to a preferred embodiment of the invention;
- Figures 11a, 11b and 11c are a three dimensional view, a sectional view along XI-XI of the working part and a three- dimensional view, respectively, of a device for delivering active principles containing a reservoir capable of being filled by the feed connector of Figure 10;
- FIGS 12a, 12b and 12c illustrate the steps in the implementation of an active-principle feed connector according to the invention of Figure 10.
- the feed connector 200 includes four parts, which are described as follows: a "proximal connection" part A for presenting an interface with a receptacle containing the fluid to be transferred into the reservoir 30; a "proximal sealing” part B whose main role is to produce a seal with the internal tube 22 of largest diameter of the reservoir 30 described above. This produces an upstream seal; an administration part C arranged so as to be in connection with the orifices of the reservoir 30 described above; and a distal sealing part D whose main role is to produce a seal with the internal tube 21 of smallest diameter. This produces a downstream seal.
- the proximal connection part A thus produces the interface with the receptacle containing the fluid with the active principles for administration.
- This part may have two general forms: either the fluid receptacle is removable or it is secured to the feed connector by means of the proximal connection part A.
- the receptacle ends in an endpiece that may be standardized, such as a male Luer, or maybe a specific or proprietary device of the supplier of said fluid receptacle.
- the proximal connection part includes means 206 for connection with this type of endpiece. Illustrated in Figure 2b, these connection means 206 are a female Luer.
- the latter has integral linking means capable of interacting with complementary integral linking means 201 provided at the level of the proximal connection part A of the feed connector 200.
- these - 6 - integral linking means 201 are a screw thread located on the outside of said proximal connection part.
- Figures 4a and 4b Variant embodiments are illustrated in Figures 4a and 4b.
- the fluid receptacle F1 has integral linking means 252 in the form of a lip of substantially cylindrical shape facing towards the rear part of the receptacle F1 whilst being spaced from the endpiece outwards.
- the feed connector 250 has, in its proximal connection part A, integral linking means 251 that complement integral linking means 252 of the receptacle F1.
- integral linking means 251 that complement integral linking means 252 of the receptacle F1.
- the interconnection between the receptacle F1 and the feed connector 250 according to the invention takes place by means of a push-fit.
- the fluid receptacle F2 is provided with integral linking means 261 in the form of an external screw thread capable of interacting with a complementary screw thread provided on the feed connector 260.
- the connection between the fluid receptacle F2 and the feed connector 260 in this case takes place by means of screwing.
- This proximal sealing part B includes a cylinder 202 of substantially circular cross section.
- the cylinder 202 is replaced by a frustum of a cone.
- the height of this cylinder or of this frustum of a cone can vary.
- the role of the administration part C is to uniformly supply the fluid for filling the reservoir 30 to the various orifices allowing filling of said reservoir 30.
- This administration part is in communication with the o connection means 206 of the feed connector 200 by means of a conduit
- the conduit 297 of substantially circular cross section, is arranged so as to be coaxial with the principal axis of the connector.
- the administration part C has spacing ribs or blades 204 extending between the proximal sealing part - 7 -
- the arrangement of the blades or ribs 204 which are four in number in this case, is such that they extend radially.
- the end facing the conduit 297 delimits passage orifices 205 between said conduit 297 and the outside of the connector 200.
- the other end, which faces the outside of said connector, ends so as to leave a space between said end and the edge of the plate 203.
- the administration part C has a series of apertures 215 made in a tube 214, the diameter of which is substantially greater than the diameter of the supply conduit 297 and substantially smaller than the diameter of the plate 203.
- the apertures 215 are uniformly distributed over the circumference of the tube 214.
- the tube 224 has a relatively large thickness, delimited by an internal diameter substantially equivalent to the diameter of the supply conduit 297 and by an external diameter substantially smaller than the diameter of the plate 203.
- the apertures 225 are arranged so as to allow the fluid to pass from the supply conduit 297 towards the outside.
- the administration part C comprises at least two blades or ribs 234 that are parallel to one another, extending opposite to one another, thereby limiting at least one passage space 235 between the supply conduit 297 and the outside of the administration part C with a view to allowing the fluid to be injected into the reservoir 30 to pass.
- the administration part includes a series of spacers 244 connecting the plate 203 with the cylinder 202. The spaces 245 between the various spacers allow the passage of fluid. The spacers
- the arrangement of the administration part is such that the fluid volume contained by said administration part is minimized relative to the volume actually introduced into the reservoir.
- This fluid volume contained by the administration part is called the "dead volume”, and depends on: - the dimensions of the plates 202 and 203; the space between said two plates; the dimensions of the means forming the spacer 204, 214, 224, 234, 244 separating said two plates; and the properties of the fluid to be administered.
- the dead volume of the administration part becomes greater than the volume to be administered into the reservoir.
- the distal sealing part D is located to the front of the feed connector 200 and produces a seal between said connector and the internal tube 21 of smallest diameter delimiting the reservoir 30.
- the height of the distal sealing part D may vary. Illustrated in Figures 2a and 2b, and also in Figures 5a to 8b, the distal sealing part D comprises a thin plate 203 of substantially circular cross section. In a variant embodiment, this plate may have a concavity and/or a convexity. Moreover, it is possible to arrange, to the front of this plate and generally of the distal sealing part, a functional piece for temporary or definitive fastening or catching onto the reservoir. Such possibilities in the variant embodiments are illustrated in Figures 3a to 3d.
- Figure 3a shows a push-fit fastening system
- the internal tube 21 of the reservoir 30 has a lip 212 extending as a projection radially towards the axis of said internal tube 21 and capable of interacting with tongues 211 extending as a projection towards the front of the plate 203 of the feed connector 210. This allows push-fit fastening of said feed connector 210 on the reservoir 30.
- Figure 3b illustrates, for the feed connector 220, a variant fastening by means of a screw thread 221 provided on the external surface of a cylindrical projection of substantially circular cross section extending to the front of the plate 203 and capable of interacting with a complementary screw thread 222 provided on the internal face of the tube 21 of the reservoir 30.
- a variant embodiment, illustrated in Figure 3c, is the reverse of that illustrated in Figure 3b in that the internal tube 21 includes, coaxially, a projection 232 of circular section having, on its outer face, a screw thread capable of interacting with a complementary screw thread 231 provided in a tube extending as a projection to the front of the plate 203 of the feed connector 230.
- a cover 241 capable of advantageously covering the open part of the reservoir 30 described above, thereby protecting it from the outside during the operation of filling said reservoir (protection from contamination, for example).
- This cover is fastened to the feed connector 240 by a rod joining the cover 241 to the plate 203 and having, at a location along its length, a more fragile part'242 that is capable of breaking under a mechanical action at the time the feed connector 240 is disconnected.
- the feed connector 270 is a connector very similar to the connector 200 described above in that the proximal sealing part B, the administration part C and the distal sealing part D are similar.
- the proximal connection part A includes a cylinder 273 of substantially circular cross section attached at a first end to the plate 202 acting as proximal sealing part B.
- the opposite end 208 comprises retention means 209 that extend as a projection from the periphery of the cylinder 273 so as to form a retention lip facing the distal part of the feed connector 270.
- the cylinder 273 comprises, located substantially coaxially, an orifice of frustoconical shape acting as connection means 206 described above.
- the feed connector 270 includes a plate 207 - lo ot essentially circular shape, at the periphery of which extend, as projections, catching tongues 276, which are two in number in this case, distributed uniformly over said periphery.
- Each of the. catching tongues 276 includes at least one stud 271 extending as a projection centrifugally, and 5 also implementation means 272 in the form, here, of a lever extending the tongue.
- the striker 300 capable of being used with the feed connector 270 described above.
- the striker 300 has connection means 301 provided with orifices 302 at a distal end. The 0 distal end ends in a point 303.
- the connection means 301 are of frustoconical shape, complementing the frustoconical shape of the connection means 206 of the feed connector 270 described above. This complementarity makes it possible to provide a sealed connection during fitting of the striker 300 onto the feed connector 270.
- the striker 300 also 5 includes an "offset" ring 304 capable of interacting with the implementation means 272 of the catching tongues 276 of the feed connector 270.
- the striker 300 also includes catching means 305, in this case in the form of tongues extending as a projection towards the distal part of the striker of the ring 304. These catching means 305 are capable of interacting with the o lip 209 of the feed connector 270 so as to securely fasten said striker 300 to said feed connector 270. Furthermore, the striker 300 includes a proximal connection part 307, in this case of cylindrical shape and substantially circular cross section, extending as a projection in a proximal manner from the ring 304.
- the striker 300 has fastening 5 means 306 that in this case are in the form of screw-thread parts and also a standardized female Luer extending internally via a channel opening out at the orifices 302 so as to allow the passage of the fluid from any receptacle capable of being fastened onto the proximal connection part 307 of the striker 300 and containing the fluid to be injected into a reservoir of a o delivery device that we will describe below.
- the delivery device 400 includes a working part 401 capable of being fitted over the tissues that are to receive - li the active principles contained in a reservoir 430 of said delivery device 400.
- the reservoir 430 is delimited externally by an external tube 410 and internally by an internal tube 421 substantially coaxial with the external tube 410.
- an internal tube 422 with a diameter greater than the internal tube 421 extends as a projection so as partially to close the reservoir 430.
- the reservoir 430 has, at its top, a series of orifices 432 uniformly distributed over the circumference of the internal tube 421.
- the delivery device 400 described here is for application to an eyeball.
- the reservoir 430 for receiving the fluid has the form of a ring including an internal tube 421 with a minimum diameter of approximately 10 mm and an external tube 410 with a maximum diameter of approximately 25 mm.
- the space between these two tubes is of variable thickness (gap, depending on the thickness of the walls of said tubes, but is typically between approximately 14 mm and 17 mm in diameter).
- This space forming the reservoir 430 is closed at one end and open at the other end.
- the length of the internal tube 421 can also vary, but is between approximately 1 mm and 10 mm.
- said reservoir 430 may contain an absorbent material for holding the liquid in place until it is used, i.e. up until transfer of the active principles into the ocular tissues.
- the absorbent material may be foam, hydrogel or fibres.
- the receptacle S containing the fluid in this case a syringe, is securely connected to the proximal part of the striker 300 with the aid of the fastening means 306 of the striker 300 interacting with the complementary connection means of the syringe S.
- the use of such a striker 300 makes it possible, if desired, to produce a mix so as to prepare the fluid containing the active principles for injection into the reservoir 430 of the delivery device 400.
- the striker 300 is next clamped onto the connector 270 pre-installed in the delivery device 400, as illustrated in - 12 -
- FIG 12a When the feed connector 270 is installed in the delivery device 400, as we have described above, the distal sealing part interacts in a sealing manner with the internal wall of the internal tube 421.
- the administration part extends opposite the uniformly distributed orifices 432 of the reservoir 430.
- the proximal sealing part operates in a sealing manner with the internal wall of the tube 422, whilst the studs 271 interact with the through-orifices 423 of the internal tube 422 so as to secure the feed connector 270 to the delivery device 400.
- the disengagement ring 304 comes to bear on the levers 272, elastically deforming all the catching tongues 276 so as to disengage the studs 271 from the through-orifices 423.
- the catching tongues 305 of the striker 300 interact with the circular lip 209 of the feed connector 270, thus securely fastening the striker 300 onto the feed connector 270. All that then remains to be done is to inject the fluid contained in the receptacle S into the reservoir 430. At the end of that operation, the configuration illustrated in Figure 12b will be achieved. Once the reservoir 430 has been filled, the receptacle F is removed.
- a feed connector 270 to allow administration, while minimizing dead-volume losses as much as possible, of a viscous or non-viscous fluid uniformly distributed in the reservoir of a medical delivery device; to secure the feed connector to the medical device, thereby preventing its normal use unless this piece can be removed; to propose a striker that can be connected to the feed connector, transfer the fluid for administration into the reservoir of the delivery device and then disconnect the feed connector from said delivery device; and - to effectively secure the striker and the feed connector together so as to prevent their reuse.
- the reservoir may have any shape depending on the intended use of the active-principle delivery device.
- the reservoir may be limited by at least two lateral walls of substantially cylindrical shape extending opposite one another. At the very least, the shape of the administration part C then follows one of these walls to provide as uniform filling of the reservoir as possible.
Abstract
Description
Claims
Priority Applications (6)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
BRPI0408029 BRPI0408029A (en) | 2003-03-03 | 2004-03-03 | uniform power connector for devices for dispensing active principles |
JP2006506497A JP4855246B2 (en) | 2003-03-03 | 2004-03-03 | Uniform feed connector for devices for delivering active ingredients |
MXPA05009387A MXPA05009387A (en) | 2003-03-03 | 2004-03-03 | Uniform feed connector for devices for the delivery of active principles. |
US10/548,210 US7771403B2 (en) | 2003-03-03 | 2004-03-03 | Uniform feed connector for devices for the delivery of active principles |
EP20040716673 EP1599162A1 (en) | 2003-03-03 | 2004-03-03 | Uniform feed connector for devices for the delivery of active principles |
CA 2524120 CA2524120C (en) | 2003-03-03 | 2004-03-03 | Uniform feed connector for devices for the delivery of active principles |
Applications Claiming Priority (2)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
FR0302549A FR2851912B1 (en) | 2003-03-03 | 2003-03-03 | UNIFORM POWER CONNECTOR FOR DELIVERY DEVICES OF ACTIVE PRINCIPLES |
FR03/02549 | 2003-03-03 |
Publications (1)
Publication Number | Publication Date |
---|---|
WO2004078093A1 true WO2004078093A1 (en) | 2004-09-16 |
Family
ID=32865183
Family Applications (1)
Application Number | Title | Priority Date | Filing Date |
---|---|---|---|
PCT/IB2004/001208 WO2004078093A1 (en) | 2003-03-03 | 2004-03-03 | Uniform feed connector for devices for the delivery of active principles |
Country Status (9)
Country | Link |
---|---|
US (1) | US7771403B2 (en) |
EP (1) | EP1599162A1 (en) |
JP (1) | JP4855246B2 (en) |
KR (1) | KR20050111605A (en) |
BR (1) | BRPI0408029A (en) |
CA (1) | CA2524120C (en) |
FR (1) | FR2851912B1 (en) |
MX (1) | MXPA05009387A (en) |
WO (1) | WO2004078093A1 (en) |
Families Citing this family (6)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
DE102004059126B4 (en) * | 2004-12-08 | 2014-01-16 | Roche Diagnostics Gmbh | Adapter for injection device |
US7981090B2 (en) | 2006-10-18 | 2011-07-19 | Baxter International Inc. | Luer activated device |
US8221363B2 (en) | 2006-10-18 | 2012-07-17 | Baxter Healthcare S.A. | Luer activated device with valve element under tension |
US7753338B2 (en) | 2006-10-23 | 2010-07-13 | Baxter International Inc. | Luer activated device with minimal fluid displacement |
US8092416B2 (en) | 2008-03-28 | 2012-01-10 | Vitalmex Internacional S.A. De C.V. | Device and method for connecting a blood pump without trapping air bubbles |
DE102009033908A1 (en) * | 2009-04-23 | 2011-01-27 | Wiebe van der Dipl.-Ing. Wal | For the removal of medical liquids from packaging suitable device and packaging equipped therewith |
Citations (5)
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US5543042A (en) * | 1995-03-30 | 1996-08-06 | Abbott Laboratories | Waste agent reservoir for suction drainage system |
EP0761562A1 (en) * | 1995-07-11 | 1997-03-12 | Becton, Dickinson and Company | Sterile resealable vial connector assembly |
FR2773320A1 (en) | 1998-01-05 | 1999-07-09 | Optisinvest | DEVICE FOR THE INTRAOCULAR TRANSFER OF IONTOPHORESIS ACTIVE PRODUCTS |
EP1201265A1 (en) * | 1999-05-25 | 2002-05-02 | Iomed, Inc. | Methods and apparatus for ocular iontophoresis |
WO2002085429A2 (en) * | 2001-04-24 | 2002-10-31 | Comar | Child friendly syringe |
Family Cites Families (16)
Publication number | Priority date | Publication date | Assignee | Title |
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DE3234118A1 (en) * | 1982-09-14 | 1984-03-15 | Siemens AG, 1000 Berlin und 8000 München | DEVICE FOR TAKING IMAGES FROM A MONITOR |
JPS59131274U (en) * | 1983-02-23 | 1984-09-03 | 日産自動車株式会社 | Grease supply device |
JPH03119464A (en) * | 1989-10-03 | 1991-05-21 | Nec Corp | Kana/kanji conversion system for word processor |
JPH0753742Y2 (en) * | 1990-03-14 | 1995-12-13 | 日産車体株式会社 | Grease injection jig |
US5810398A (en) * | 1992-10-02 | 1998-09-22 | Pall Corporation | Fluid delivery systems and methods and assemblies for making connections |
US5609584A (en) * | 1994-05-18 | 1997-03-11 | Gettig Technologies, Inc. | Adaptor system for use with a syringe |
JPH0947707A (en) * | 1995-08-07 | 1997-02-18 | Yutaka Giken Co Ltd | Grease injecting device |
US5873872A (en) * | 1996-09-17 | 1999-02-23 | Becton Dickinson And Company | Multipositional resealable vial connector assembly for efficient transfer of liquid |
US6681946B1 (en) * | 1998-02-26 | 2004-01-27 | Becton, Dickinson And Company | Resealable medical transfer set |
US6957745B2 (en) * | 1998-04-20 | 2005-10-25 | Becton, Dickinson And Company | Transfer set |
AU5030000A (en) * | 1999-05-21 | 2000-12-12 | Micro Therapeutics, Inc. | Interface needle and method for creating a blunt interface between delivered liquids |
US6183465B1 (en) * | 1999-09-01 | 2001-02-06 | Sherwood Services, Ag | Adapter for a feeding system |
FR2819418B1 (en) * | 2001-01-17 | 2003-03-14 | Technoflex Sa | TRANSFER SET, ESPECIALLY FOR THE ADMINISTRATION OF A MIXTURE OF LIQUIDS FOR MEDICAL PURPOSES |
FR2820110B1 (en) * | 2001-01-29 | 2003-08-15 | Valois Sa | ASSEMBLY AND METHOD FOR MANUFACTURING, ASSEMBLING AND FILLING A FLUID PRODUCT DISPENSING DEVICE |
GB0127224D0 (en) * | 2001-11-13 | 2002-01-02 | Glaxosmithkline Biolog Sa | Novel compounds |
US20060169348A1 (en) * | 2005-01-18 | 2006-08-03 | Gil Yigal | Dosage device and method particularly useful for preparing liquid medications |
-
2003
- 2003-03-03 FR FR0302549A patent/FR2851912B1/en not_active Expired - Fee Related
-
2004
- 2004-03-03 KR KR1020057016109A patent/KR20050111605A/en not_active Application Discontinuation
- 2004-03-03 US US10/548,210 patent/US7771403B2/en not_active Expired - Fee Related
- 2004-03-03 CA CA 2524120 patent/CA2524120C/en not_active Expired - Fee Related
- 2004-03-03 BR BRPI0408029 patent/BRPI0408029A/en not_active Application Discontinuation
- 2004-03-03 JP JP2006506497A patent/JP4855246B2/en not_active Expired - Fee Related
- 2004-03-03 MX MXPA05009387A patent/MXPA05009387A/en not_active Application Discontinuation
- 2004-03-03 EP EP20040716673 patent/EP1599162A1/en not_active Withdrawn
- 2004-03-03 WO PCT/IB2004/001208 patent/WO2004078093A1/en active Application Filing
Patent Citations (5)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
US5543042A (en) * | 1995-03-30 | 1996-08-06 | Abbott Laboratories | Waste agent reservoir for suction drainage system |
EP0761562A1 (en) * | 1995-07-11 | 1997-03-12 | Becton, Dickinson and Company | Sterile resealable vial connector assembly |
FR2773320A1 (en) | 1998-01-05 | 1999-07-09 | Optisinvest | DEVICE FOR THE INTRAOCULAR TRANSFER OF IONTOPHORESIS ACTIVE PRODUCTS |
EP1201265A1 (en) * | 1999-05-25 | 2002-05-02 | Iomed, Inc. | Methods and apparatus for ocular iontophoresis |
WO2002085429A2 (en) * | 2001-04-24 | 2002-10-31 | Comar | Child friendly syringe |
Also Published As
Publication number | Publication date |
---|---|
KR20050111605A (en) | 2005-11-25 |
JP4855246B2 (en) | 2012-01-18 |
JP2006520636A (en) | 2006-09-14 |
FR2851912B1 (en) | 2005-05-13 |
EP1599162A1 (en) | 2005-11-30 |
CA2524120A1 (en) | 2004-09-16 |
MXPA05009387A (en) | 2006-02-28 |
CA2524120C (en) | 2012-01-24 |
US20060229590A1 (en) | 2006-10-12 |
BRPI0408029A (en) | 2006-02-14 |
US7771403B2 (en) | 2010-08-10 |
FR2851912A1 (en) | 2004-09-10 |
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