WO2004081509A1 - Coiled optical fiber assembly for measuring pressure and/or other physical data - Google Patents
Coiled optical fiber assembly for measuring pressure and/or other physical data Download PDFInfo
- Publication number
- WO2004081509A1 WO2004081509A1 PCT/EP2004/050249 EP2004050249W WO2004081509A1 WO 2004081509 A1 WO2004081509 A1 WO 2004081509A1 EP 2004050249 W EP2004050249 W EP 2004050249W WO 2004081509 A1 WO2004081509 A1 WO 2004081509A1
- Authority
- WO
- WIPO (PCT)
- Prior art keywords
- carrier tube
- length
- fiber
- tube
- optical
- Prior art date
Links
- 239000013307 optical fiber Substances 0.000 title claims abstract description 89
- 239000000835 fiber Substances 0.000 claims abstract description 58
- 238000000034 method Methods 0.000 claims abstract description 24
- 238000005452 bending Methods 0.000 claims abstract description 19
- 239000012530 fluid Substances 0.000 claims description 27
- 230000003287 optical effect Effects 0.000 claims description 23
- 230000000694 effects Effects 0.000 claims description 14
- 230000002787 reinforcement Effects 0.000 claims description 9
- 239000000463 material Substances 0.000 claims description 7
- 238000005259 measurement Methods 0.000 claims description 5
- 238000004519 manufacturing process Methods 0.000 claims description 4
- 229910000831 Steel Inorganic materials 0.000 claims description 3
- 230000015572 biosynthetic process Effects 0.000 claims description 3
- 239000010959 steel Substances 0.000 claims description 3
- 230000006835 compression Effects 0.000 claims description 2
- 238000007906 compression Methods 0.000 claims description 2
- 229920002457 flexible plastic Polymers 0.000 claims description 2
- 230000004907 flux Effects 0.000 claims description 2
- 239000011159 matrix material Substances 0.000 claims description 2
- 239000000203 mixture Substances 0.000 claims description 2
- 239000011148 porous material Substances 0.000 claims description 2
- 229920003235 aromatic polyamide Polymers 0.000 claims 1
- 238000011144 upstream manufacturing Methods 0.000 abstract description 2
- 238000002474 experimental method Methods 0.000 description 5
- 238000005188 flotation Methods 0.000 description 3
- 230000008602 contraction Effects 0.000 description 2
- 230000001939 inductive effect Effects 0.000 description 2
- 230000035945 sensitivity Effects 0.000 description 2
- 238000004904 shortening Methods 0.000 description 2
- 238000001237 Raman spectrum Methods 0.000 description 1
- 239000004760 aramid Substances 0.000 description 1
- 229920006231 aramid fiber Polymers 0.000 description 1
- 230000005540 biological transmission Effects 0.000 description 1
- 238000009530 blood pressure measurement Methods 0.000 description 1
- 230000002596 correlated effect Effects 0.000 description 1
- 230000007423 decrease Effects 0.000 description 1
- 238000009826 distribution Methods 0.000 description 1
- 239000013536 elastomeric material Substances 0.000 description 1
- 230000005484 gravity Effects 0.000 description 1
- 238000009533 lab test Methods 0.000 description 1
- 239000007788 liquid Substances 0.000 description 1
- 238000000253 optical time-domain reflectometry Methods 0.000 description 1
- 230000002093 peripheral effect Effects 0.000 description 1
- 229920001296 polysiloxane Polymers 0.000 description 1
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 description 1
Classifications
-
- G—PHYSICS
- G01—MEASURING; TESTING
- G01L—MEASURING FORCE, STRESS, TORQUE, WORK, MECHANICAL POWER, MECHANICAL EFFICIENCY, OR FLUID PRESSURE
- G01L11/00—Measuring steady or quasi-steady pressure of a fluid or a fluent solid material by means not provided for in group G01L7/00 or G01L9/00
- G01L11/02—Measuring steady or quasi-steady pressure of a fluid or a fluent solid material by means not provided for in group G01L7/00 or G01L9/00 by optical means
- G01L11/025—Measuring steady or quasi-steady pressure of a fluid or a fluent solid material by means not provided for in group G01L7/00 or G01L9/00 by optical means using a pressure-sensitive optical fibre
-
- E—FIXED CONSTRUCTIONS
- E21—EARTH DRILLING; MINING
- E21B—EARTH DRILLING, e.g. DEEP DRILLING; OBTAINING OIL, GAS, WATER, SOLUBLE OR MELTABLE MATERIALS OR A SLURRY OF MINERALS FROM WELLS
- E21B47/00—Survey of boreholes or wells
- E21B47/01—Devices for supporting measuring instruments on drill bits, pipes, rods or wirelines; Protecting measuring instruments in boreholes against heat, shock, pressure or the like
-
- E—FIXED CONSTRUCTIONS
- E21—EARTH DRILLING; MINING
- E21B—EARTH DRILLING, e.g. DEEP DRILLING; OBTAINING OIL, GAS, WATER, SOLUBLE OR MELTABLE MATERIALS OR A SLURRY OF MINERALS FROM WELLS
- E21B47/00—Survey of boreholes or wells
- E21B47/06—Measuring temperature or pressure
-
- E—FIXED CONSTRUCTIONS
- E21—EARTH DRILLING; MINING
- E21B—EARTH DRILLING, e.g. DEEP DRILLING; OBTAINING OIL, GAS, WATER, SOLUBLE OR MELTABLE MATERIALS OR A SLURRY OF MINERALS FROM WELLS
- E21B47/00—Survey of boreholes or wells
- E21B47/06—Measuring temperature or pressure
- E21B47/07—Temperature
-
- E—FIXED CONSTRUCTIONS
- E21—EARTH DRILLING; MINING
- E21B—EARTH DRILLING, e.g. DEEP DRILLING; OBTAINING OIL, GAS, WATER, SOLUBLE OR MELTABLE MATERIALS OR A SLURRY OF MINERALS FROM WELLS
- E21B47/00—Survey of boreholes or wells
- E21B47/10—Locating fluid leaks, intrusions or movements
- E21B47/113—Locating fluid leaks, intrusions or movements using electrical indications; using light radiations
-
- E—FIXED CONSTRUCTIONS
- E21—EARTH DRILLING; MINING
- E21B—EARTH DRILLING, e.g. DEEP DRILLING; OBTAINING OIL, GAS, WATER, SOLUBLE OR MELTABLE MATERIALS OR A SLURRY OF MINERALS FROM WELLS
- E21B49/00—Testing the nature of borehole walls; Formation testing; Methods or apparatus for obtaining samples of soil or well fluids, specially adapted to earth drilling or wells
- E21B49/006—Measuring wall stresses in the borehole
Definitions
- the invention relates to a method and system for measuring pressure and/or other physical data, such as temperature and deformation due to axial, torque and/or bending stresses by means of one or more optical fibers that are embedded in a defor able carrier tube.
- JP6043056, JP9026370, JP6148017, JP60219503, JP2000-018981 disclose fiber optical pressure sensor systems, wherein a coiled optical fiber is embedded in a flexible tubular or cylindrical carrier body such that deformation of the carrier body will cause variation of the curvature and shape of the coiled optical fiber. This deformation initiates variation of transmission losses in optical signals transmitted from one end towards another end of the coiled fiber.
- These known systems are configured to detect an average pressure exerted on the carrier body and are not designed for use as Distributed Pressure Sensors (DPS) which detect the pressure exerted at different locations along the length of the carrier body and map pressure variations along the length of the carrier body.
- DPS Distributed Pressure Sensors
- WO 01/07935 disclose coiled optical fibers inscribed by
- Fiber Bragg gratings for detecting pressure exerted to a carrier tube in which the coiled optical fibers are embedded.
- a Fiber Bragg grating is formed by a pair of axially displaced disruptions in the fiber, which will reflect a narrow band of light at a specific wavelength. Variation of the spacing between a pair of such disruptions, for example due to strain induced by pressure and/or temperature, will cause a shift in the wavelength of the light it reflects.
- a detected shift in wavelength reflected by a Fiber Bragg grating can be correlated to an elongation or shortening of the length of the optical fiber between a pair of the disruptions that form the grating.
- Fiber Bragg gratings may be distributed along the length of an optical fiber and the signals reflected by these grating may be multiplexed and distinguished from each other by known interferometric signal distinguishing techniques.
- Fiber Bragg grating optical sensor systems can be used for distributed pressure measurement along the length of an elongate carrier tube, but the currently available signal distinguishing techniques limit the amount of
- Fiber Bragg gratings that can be distributed along the length of an optical fiber. Furthermore Fiber Bragg gratings provide fixed sensor sections in an optical fiber, so that pressure and/or other measurements can only be performed in pre-selected section of the fiber, which are subsequently positioned at pre-selected locations where the measurements are to be made.
- UK patent application GB2303445 discloses a hydrophone comprising a coiled optical fiber, which is embedded in a flexible conduit that is arranged between two rigid flanges. If an isotropic pressure is applied to the fiber, this causes an anisotropic stress vector in the optical fiber, which may be detected using birefringence in the optical fiber.
- DTS Fiber optical Distributed Temperature Sensor
- European patent application 0377549 discloses a combined DPS and DTS fiber optical system, wherein use is made of a fiber that has a central light guiding region into which interrogating light is launched and a peripheral light guiding region comprising fluorescent material into which a relatively large fraction of light from the central region is deflected under the action of force exerted to the fiber.
- the light transmitted by the fluorescent material has a unique wavelength, which is different from the wavelength of the interrogating light.
- a disadvantage of the known system is that the Brillouin shift provides a rather weak signal in response to strain variations in the fiber, so that the strain related backscattered signal has a low sensitivity.
- the backscattered signal is also influenced by strain induced by torque and or bending forces exerted to the fiber, which decreases the selectivity of the measurement of axial strain variations along the length of the fiber.
- the method according to the invention comprises measuring pressure and/or other physical data by means of a coiled optical fiber, which is embedded in the wall of a carrier tube such that deformation of the carrier tube induces strain in the optical fiber.
- a pulsed laser light source transmits a sequence of light pulses of a selected wavelength from one end of the fiber into an elongate substantially uniform light guide channel provided by said optical fiber and any shift in wavelength of the light pulses backscattered from various locations along the length of said light guide channel is detected by a light sensor assembly which is located near said end of the fiber.
- a signal processing assembly calculates a strain pattern along at least a substantial part of the length of the fiber on the basis of the detected wavelength pattern of the backscattered light, and determines on the basis of the calculated strain pattern a pressure difference between the interior and exterior of the carrier tube and/or other physical data at various locations along the length of the carrier tube.
- the carrier tube has a larger stiffness in a longitudinal direction than in a circumferential direction of the tube.
- variation of the pressure difference between the first and second fluid will predominantly create circumferential deformation of the carrier tube, whereas simultaneous axial deformation of the tube is inhibited.
- the carrier tube may be made of a flexible plastic material into which one or more axial reinforcement elements, such as steel cables and/or aramid fibers, are embedded.
- the interior of the carrier tube may be filled with a fluid, such as a silicone liquid, of which the pressure and density are controlled such that the carrier tube deforms elastically in circumferential direction in response to any variation of the pressure of a fluid surrounding the carrier tube.
- a fluid such as a silicone liquid
- a plurality of optical fibers are embedded in the wall of the carrier tube and are arranged in different substantially helical configurations relative to a longitudinal axis of the tube, and that these fibers are each connected to a common signal processing assembly which compares optical signals reflected along the length of said optical fibers to determine the effects of deformation of the elongate carrier tube resulting from bending and/or torque forces exerted to and/or temperature variations at various locations along the length of the carrier tube.
- the carrier tube may comprise at least two helical optical fibers having opposite pitch angles and the signal processing assembly may determine and/or compensate effects of torque on the elongate carrier tube.
- the signal processing assembly may determine and/or compensate effects of bending of the elongate carrier tube.
- the signal processing assembly may determine and/or compensate effects of elongation of the elongate carrier tube.
- the signal processing assembly may determine fluid pressure exerted to the carrier tube along at least a substantial part of its length by determination of radial compression of the tube and to reduce the effects of torque and/or bending of the tube on said determination.
- the signal processing assembly is configured to measure a fluid pressure exerted to and/or the temperature of the carrier tube along at least a substantial part of its length on the basis of a measurement of the shift and area of the Brillouin peaks in optical signals backscattered along the length of the fiber or fibers.
- the carrier tube may be arranged along at least part of the length of an inflow region of an oil and/or gas production well and the signal processing assembly may convert the monitored pressure and temperature data into data which indicate the flux and/or composition of well effluents flowing into and/or through the wellbore.
- the carrier tube may be arranged alongside at least part of the length of the wellbore of a well outside a well casing and/or outside a perforated liner, which is located in an inflow zone of the well below the well casing.
- the signal processing assembly may measure fluid pressure in the pores, geological strain and/or deformation in the matrix of the formation surrounding the well casing and/or perforated liner and/or to measure the pressure and temperature of the fluids flowing from the formation into the wellbore surrounding the perforated liner.
- the invention also relates to a fiber optical system for measuring pressure and/or other physical data.
- the system according to the invention comprises a carrier tube which is in use at least partly surrounded by a first fluid and at least partly filled with a second fluid and at least one optical fiber which is embedded in the wall of the carrier tube such that the optical fiber is coiled along at least a substantial part of the length of the carrier tube and deformation of the carrier tube induces variation of strain in the optical fiber.
- the system further comprises a pulsed laser light source for transmitting a sequence of light pulses of a selected wavelength from one end of the fiber into an elongate coiled light guide channel provided by said optical fiber, a light sensor assembly located near said end of the optical fiber, which is configured to detect any shift in wavelength of the light pulses backscattered from various locations along the length of said light guide channel, and a signal processing assembly which is designed to calculate a strain pattern along at least a substantial part of the length of the fiber, and on the basis of the calculated strain pattern a pressure difference between said first and second fluid and/or other physical data at a plurality of locations along the length of the carrier tube.
- the system is a Brillouin back scattering system in which the shift and area of Brillouin peaks in a backscattered pulsed optical signal are indicative of the strain and/or temperature at various locations along the length of at least one optical fiber and the pressure difference between the first and second fluid and the temperature of the wall of the carrier tube at various locations along the length of the tube.
- optical fiber or fibers used in the method and system according to the invention may be conventional optical fibers which each comprise one or more single mode guide channels which are substantially free of Fiber-Bragg gratings.
- Fig. 1 is a schematic three dimensional view of a carrier tube in which two pairs of optical fibers are embedded at different diameters and such that the fiber pairs have different and opposite pitch angles;
- Fig. 2 is a schematic side view of a carrier tube in which two sets of three optical fibers are embedded at different diameters and such that the fiber sets have different and opposite pitch angles;
- Fig. 3 is a cross-sectional view at an enlarged scale of the carrier tube and optical fiber assembly of Fig. 2 taken across line III-III and seen in the direction of the arrows;
- Fig. 4 is a longitudinal sectional view of the carrier tube and optical fiber assembly of Fig. 2 and Fig. 3 taken across line IV-IV in Fig. 3 and seen in the direction of the arrows;
- Fig. 5 is a schematic three-dimensional view of the carrier tube and optical fiber assembly of Figs. 2-4 shown at a smaller scale than in the other Figures.
- DETAILED DESCRIPTION OF THE INVENTION In Fig. 1 there is shown an elastomeric flexible carrier tube 1 in which three steel longitudinal reinforcement cables 3 and an inner and outer pair of helical optical fibers 2A-2B and 4A-4B are embedded.
- the interior of the carrier tube 1 is filled with a first fluid FI and the tube 1 is surrounded by a second fluid F2 such that a pressure difference between the fluids FI and F2 generates a circumferential expansion or contraction of the carrier tube 1, whereas the longitudinal reinforcement cables 3 inhibit simultaneous longitudinal elongation or contraction of the carrier tube 1 as a result of said pressure difference and of the weight of the carrier tube 1 and other forces, such as flotation and friction, acting on the carrier tube 1.
- the inner pair of optical fibers 2A-2B is wound at a diameter Dl and, when seen from above, in a clockwise direction, relative to a longitudinal axis 5 of the tube 1 and at a first helix angle HI.
- the outer pair of optical fibers 4A-4B is wound at a diameter D2 and, when seen from above, in an anti- clockwise direction relative to the longitudinal axis 5 of the tube 1 and at a second helix angle H2.
- each of the optical fibers 2A-2B and 4A-4B light pulses may be transmitted and the amplitude and frequency shift of the Brillouin backscatter light may be measured and compared with a reference fiber (not shown) to measure both temperature and strain at any point along the length of each of the optical fibers 2A-B and 4A-4B in accordance with the method described in International patent application WO98/27406.
- the method involves inducing a pulsed laser light source to transmit a sequence of light pulses of a selected wavelength from an upstream end of each fiber 2A-B and 4A-B into the coiled substantially uniform light guide channel provided by each optical fiber and inducing a light sensor assembly to detect any shift in wavelength of the light pulses backscattered from various locations along the length of said light guide channel.
- a signal processing assembly then calculates a strain pattern along the length of each of the fibers 2A-B and 4A-B.
- the carrier tube 1 may be used to measure fluid pressure and temperature in a horizontal inflow region of an oil and/or gas production well, which may be several kilometres long.
- the carrier tube 1 may be twisted, longitudinally stretched and bent throughout its length and the deformation resulting from these deformation may be determined by comparing the detected strain patterns in the inner and outer pairs of optical fibers 2A-2B and 4A-4B.
- the diameter D2 is larger than the diameter Dl and the second helix angle H2 is larger than the first helix angle HI deformation of the carrier tube 1 as a result of longitudinal, tangential and torsional stresses will generate different strain patterns in the inner and outer pairs of optical fibers 2A-2B and 4A-4B.
- a positive pressure difference between the fluids FI and F2 in the interior and exterior of the carrier tube 1 will initiate a tangential expansion of the carrier tube 1 which results in a simultaneous strain increase in both pairs of optical fibers 2A-2B and 4A-4B.
- the ratio between the resulting strain increase in the inner and outer pairs of optical fibers will be related to the diameter ratio D1/D2 and the helix angle ratio H1/H2.
- Said ratio between the strain increase in the inner and outer fiber pairs 2A-2B and 4A-4B as a result of a pressure difference between the fluids FI and F2 in the interior and exterior of the carrier tube 1 may be determined by calculation and laboratory experiments during which said pressure difference is the only parameter that is varied during the experiment. Torque exerted on the carrier tube 1 in, when seen from above, a clock-wise direction will result in an elongation of the outer pair of optical fibers 4A-4B and in a simultaneous shortening of the inner pair of optical fibers 2A-2B.
- the ratio between the negative and positive strain patterns in the inner and outer pairs of optical fibers 2A-2B and 4A-4B as a result of torque exerted on the carrier tube 1 will be related to the diameter ratio D1/D2 and the helix angle ratio H1/H2 and may be determined by calculation and experiments during which torsion of the carrier tube 1 is the only parameter that is varied. Bending of the carrier tube 1, such that the longitudinal axis 5 is curved, will result in different sinusoidal patterns at which the inner and outer pairs of optical fibers 2A-2B and 4A-4B are elongated and shortened. The difference between said sinusoidal patterns will be related to the diameter ratio D1/D2 and the helix angle ratio H1/H2 and may be determined by calculation and experiments during which the tube 1 is bend in various bending angles and no other parameters are varied during the experiments.
- Longitudinal strain of the carrier tube 1 may be caused by gravitation, flotation, friction and the pressure difference between the fluids FI and F2 in the interior and exterior of the carrier tubel. Longitudinal strain of the carrier tube 1 will initiate a simultaneous strain of the optical fibers.
- the ratio between the strain of the inner and outer pairs of optical fibers 2A-2B and 4A-4B resulting from longitudinal strain of the carrier tube 1 may be determined by calculation and experiments during which the longitudinal strain of the carrier tube is varied as the only varying parameter.
- the reinforcement cables 3 have a significantly higher stiffness than the elastomeric material of the wall of the tube 1 and therefore inhibit longitudinal deformation of the tube 1 as a result of the pressure difference between the interior and exterior of the tube and flotation, gravity and frictional forces.
- the longitudinal deformation of the tube may be further increased by embedding more than three reinforcement cables 3 in the wall of the tube 1 and/or by using thicker reinforcement cables 3.
- One or more longitudinal optical fibers may be arranged parallel to the reinforcement cables 3 to assess the longitudinal strain in the carrier tube 1.
- the effects of torsion and bending of the carrier tube on the strain measured in the optical fibers may be determined by comparing the strain levels in the inner and outer pairs of fibers 2A-2B and 4A-4B and by comparing any sinusoidal variations in the strain patterns detected along the length of the fibers 2A-2B and 4A-4B.
- Figures 2-5 show an alternative embodiment of a carrier tube 10 according to the present invention, wherein two sets of three optical fibers 11A,B and C and 12A, B and C and three longitudinal reinforcement cables 13A, B and C are embedded in the wall of an elastomeric carrier tube 10.
- the inner set of three optical fibers 11A,B and C is, when seen from above, wound in anti-clockwise direction at a first helix angle at a first radius Rl relative to a longitudinal axis 15 of the carrier tube 10.
- the outer set of three optical fibers 12A,B and C is, when seen from above, wound in clockwise direction at a second helix angle at a second radius R2 relative to the longitudinal axis 15 of the carrier tube 10.
- the first helix angle and first radius Rl are smaller than the second helix angle and second radius R2, respectively.
- the strain patterns in the optical fibers 11 and 12 A,B and C may be measured by measuring the amplitude and frequency of the Brillouin shifts of lightpulses that are backscattered at different points of the length of the fibers in the manner described in International patent application WO98/27406.
- the strain patterns thus detected in the inner and outer sets of optical fibers 11A, B and C and 12A,B and C may be compared and analysed in the same way as described with reference to Fig. 1.
Abstract
Description
Claims
Priority Applications (8)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
AU2004219914A AU2004219914B2 (en) | 2003-03-05 | 2004-03-04 | Coiled optical fiber assembly for measuring pressure and/or other physical data |
BRPI0407981-7A BRPI0407981A (en) | 2003-03-05 | 2004-03-04 | fiber optic method and system for measuring pressure and / or other physical data |
US10/548,161 US7315666B2 (en) | 2003-03-05 | 2004-03-04 | Coiled optical fiber assembly for measuring pressure and/or other physical data |
EA200501424A EA007244B1 (en) | 2003-03-05 | 2004-03-04 | Coiled optical fiber assembly for measuring pressure and/or other physical data |
EP04737300A EP1604181B1 (en) | 2003-03-05 | 2004-03-04 | Coiled optical fiber assembly for measuring pressure and/or other physical data |
CA2518033A CA2518033C (en) | 2003-03-05 | 2004-03-04 | Coiled optical fiber assembly for measuring pressure and/or other physical data |
AT04737300T ATE521877T1 (en) | 2003-03-05 | 2004-03-04 | COILED OPTICAL FIBER ASSEMBLY FOR MEASURING PRESSURE AND/OR OTHER PHYSICAL DATA |
NO20054564A NO20054564L (en) | 2003-03-05 | 2005-10-04 | Rolled up optical fiber assembly for painting pressure and / or other physical data |
Applications Claiming Priority (2)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
EP03075647.2 | 2003-03-05 | ||
EP03075647 | 2003-03-05 |
Publications (1)
Publication Number | Publication Date |
---|---|
WO2004081509A1 true WO2004081509A1 (en) | 2004-09-23 |
Family
ID=32981867
Family Applications (1)
Application Number | Title | Priority Date | Filing Date |
---|---|---|---|
PCT/EP2004/050249 WO2004081509A1 (en) | 2003-03-05 | 2004-03-04 | Coiled optical fiber assembly for measuring pressure and/or other physical data |
Country Status (9)
Country | Link |
---|---|
US (1) | US7315666B2 (en) |
EP (1) | EP1604181B1 (en) |
AT (1) | ATE521877T1 (en) |
AU (1) | AU2004219914B2 (en) |
BR (1) | BRPI0407981A (en) |
CA (1) | CA2518033C (en) |
EA (1) | EA007244B1 (en) |
NO (1) | NO20054564L (en) |
WO (1) | WO2004081509A1 (en) |
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Also Published As
Publication number | Publication date |
---|---|
CA2518033C (en) | 2012-10-23 |
NO20054564L (en) | 2005-10-04 |
CA2518033A1 (en) | 2004-09-23 |
EP1604181A1 (en) | 2005-12-14 |
US7315666B2 (en) | 2008-01-01 |
US20060071158A1 (en) | 2006-04-06 |
BRPI0407981A (en) | 2006-03-07 |
EA007244B1 (en) | 2006-08-25 |
EA200501424A1 (en) | 2006-02-24 |
ATE521877T1 (en) | 2011-09-15 |
AU2004219914A1 (en) | 2004-09-23 |
AU2004219914B2 (en) | 2007-02-22 |
EP1604181B1 (en) | 2011-08-24 |
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