WO2005030672A2 - Cement compositions comprising strength-enhancing lost circulation materials and methods of cementing in subterranean formations - Google Patents
Cement compositions comprising strength-enhancing lost circulation materials and methods of cementing in subterranean formations Download PDFInfo
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- WO2005030672A2 WO2005030672A2 PCT/GB2004/003839 GB2004003839W WO2005030672A2 WO 2005030672 A2 WO2005030672 A2 WO 2005030672A2 GB 2004003839 W GB2004003839 W GB 2004003839W WO 2005030672 A2 WO2005030672 A2 WO 2005030672A2
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- WO
- WIPO (PCT)
- Prior art keywords
- cement composition
- cement
- range
- lost circulation
- strength
- Prior art date
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Classifications
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- C—CHEMISTRY; METALLURGY
- C04—CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
- C04B—LIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
- C04B14/00—Use of inorganic materials as fillers, e.g. pigments, for mortars, concrete or artificial stone; Treatment of inorganic materials specially adapted to enhance their filling properties in mortars, concrete or artificial stone
- C04B14/02—Granular materials, e.g. microballoons
- C04B14/04—Silica-rich materials; Silicates
- C04B14/10—Clay
- C04B14/108—Shale, slate
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- C—CHEMISTRY; METALLURGY
- C04—CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
- C04B—LIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
- C04B28/00—Compositions of mortars, concrete or artificial stone, containing inorganic binders or the reaction product of an inorganic and an organic binder, e.g. polycarboxylate cements
- C04B28/02—Compositions of mortars, concrete or artificial stone, containing inorganic binders or the reaction product of an inorganic and an organic binder, e.g. polycarboxylate cements containing hydraulic cements other than calcium sulfates
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- C—CHEMISTRY; METALLURGY
- C04—CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
- C04B—LIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
- C04B40/00—Processes, in general, for influencing or modifying the properties of mortars, concrete or artificial stone compositions, e.g. their setting or hardening ability
- C04B40/0028—Aspects relating to the mixing step of the mortar preparation
- C04B40/0039—Premixtures of ingredients
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- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09K—MATERIALS FOR MISCELLANEOUS APPLICATIONS, NOT PROVIDED FOR ELSEWHERE
- C09K8/00—Compositions for drilling of boreholes or wells; Compositions for treating boreholes or wells, e.g. for completion or for remedial operations
- C09K8/42—Compositions for cementing, e.g. for cementing casings into boreholes; Compositions for plugging, e.g. for killing wells
- C09K8/46—Compositions for cementing, e.g. for cementing casings into boreholes; Compositions for plugging, e.g. for killing wells containing inorganic binders, e.g. Portland cement
- C09K8/467—Compositions for cementing, e.g. for cementing casings into boreholes; Compositions for plugging, e.g. for killing wells containing inorganic binders, e.g. Portland cement containing additives for specific purposes
- C09K8/487—Fluid loss control additives; Additives for reducing or preventing circulation loss
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- E—FIXED CONSTRUCTIONS
- E21—EARTH DRILLING; MINING
- E21B—EARTH DRILLING, e.g. DEEP DRILLING; OBTAINING OIL, GAS, WATER, SOLUBLE OR MELTABLE MATERIALS OR A SLURRY OF MINERALS FROM WELLS
- E21B33/00—Sealing or packing boreholes or wells
- E21B33/10—Sealing or packing boreholes or wells in the borehole
- E21B33/13—Methods or devices for cementing, for plugging holes, crevices, or the like
- E21B33/14—Methods or devices for cementing, for plugging holes, crevices, or the like for cementing casings into boreholes
-
- C—CHEMISTRY; METALLURGY
- C04—CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
- C04B—LIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
- C04B2111/00—Mortars, concrete or artificial stone or mixtures to prepare them, characterised by specific function, property or use
- C04B2111/00034—Physico-chemical characteristics of the mixtures
- C04B2111/00146—Sprayable or pumpable mixtures
-
- C—CHEMISTRY; METALLURGY
- C04—CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
- C04B—LIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
- C04B2201/00—Mortars, concrete or artificial stone characterised by specific physical values
- C04B2201/20—Mortars, concrete or artificial stone characterised by specific physical values for the density
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- Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
- Y02—TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
- Y02W—CLIMATE CHANGE MITIGATION TECHNOLOGIES RELATED TO WASTEWATER TREATMENT OR WASTE MANAGEMENT
- Y02W30/00—Technologies for solid waste management
- Y02W30/50—Reuse, recycling or recovery technologies
- Y02W30/91—Use of waste materials as fillers for mortars or concrete
Definitions
- the present invention relates to subterranean cementing operations, and more particularly, to cement compositions comprising strength-enhancing lost circulation materials, and methods of using such cementing compositions in subterranean formations.
- Hydraulic cement compositions are commonly utilized in subterranean operations, particularly subterranean well completion and remedial operations.
- hydraulic cement compositions are used in primary cementing operations whereby pipe strings such as casings and liners are cemented in well bores.
- primary cementing hydraulic cement compositions are pumped into the annular space between the walls of a well bore and the exterior surface of the pipe string disposed therein.
- the cement composition is permitted to set in the annular spice, thereby forming an annular sheath of hardened substantially impermeable cement therein that substantially supports and positions the pipe string in the well bore and bonds the exterior surface of the pipe string to the walls of the well bore.
- Hydraulic cement compositions also are used in remedial cementing operations such as plugging highly permeable zones or fractures in well bores, plugging cracks and holes in pipe strings, and the like.
- Subterranean formations transversed by well bores are often weak, highly permeable, and extensively fractm7ed.
- such formations may be unable to withstand the hydrostatic head pressure normally associated with fluids (e.g., cement compositions and the like) being injected into the formation.
- the hydrostatic pressure may be sufficient to force such fluids into the fractures and/or permeable zones of the formation, which may result in a significant loss of fluid into the formation, This loss of fluid circulation is problematic for a number of reasons.
- the present invention relates to subterranean cementing operations, and more particularly, to cement compositions comprising strength-enhancing lost circulation materials, and methods of using such cementing compositions in subterranean formations.
- An example of a method of the present invention is a method of cementing in a subterranean formation comprising the steps of: providing a cement composition comprising cement, a strength-enhancing lost circulation material, and water; placing the cement composition into a subterranean formation; and allowing the cement composition to set.
- An example of a composition of the present invention is a cement composition comprising: cement, a strength-enhancing lost circulation material, and water.
- the present invention relates to subterranean cementing operations, and more particularly, to cement compositions comprising strength-enhancing lost circulation materials, and methods of using such cementing compositions in subterranean formations.
- the improved cement compositions of the present invention generally comprise cement, water, and a strength-enhancing lost circulation material.
- other additives suitable for use in conjunction with subterranean cementing operations may be added to these cement compositions if desired.
- the cement compositions of the present invention have a density in the range of from about 4 lb/gallon to about 20 lb/gallon.
- the cement compositions of the present invention have a density in the range of from about 8 lb/gallon to about 17 lb/gallon.
- the water utilized in the cement compositions of the present invention can be fresh water, salt water (e.g., water containing one or more salts dissolved therein), brine (e.g., saturated salt water), or seawater.
- the water can be from any source provided that it does not contain an excess of compounds, e.g., dissolved organics, that may adversely affect other components in the cement composition.
- the density of the water may vary based, inter aim, on the salt content.
- the water has a density in the range of from about 8.3 lb/gallon to about 9.5 lb/gallon. Further, the water may be present in an amount sufficient to form a pumpable slurry. In certain exemplary embodiments, the water is present in the cement compositions in an amount in the range of from about 30% to about 180% by weight of the cement ( c ⁇ r bwoc") therein. In certain exemplary embodiments, the water is present in the cement composition in the range of from about 40% to about 90% bwoc therein. In certain exemplary embodiments, the water is present in the cement composition in the range of from about 40% to about 50% bwoc therein.
- the improved cement compositions of the present invention comprise a hydraulic cement.
- hydraulic cements are suitable for use including those comprised of calcium, aluminum, silicon, oxygen, and/or sulfur which set and harden by reaction with water.
- hydraulic cements include, but are not limited to, Portland cements, pozzolana cements, gypsum cements, soil cements, calcium phosphate cements, high alumina content cements, silica cements, high alkalinity cements, and mixtures thereof.
- the cement compositions of the present invention further comprise a strength- enhancing lost circulation material.
- the strength-enhancing lost circulation material may be any material that provides a desired level of lost circulation control from the cement composition into the formation with minimal adverse impact to the compressive strength of the cement composition.
- certain embodiments of the strength- enhancing lost circulation material of the present invention bridge and/or plug fractures and permeable zones in the formation so as to minimize loss of fluid circulation into the formation.
- Certain exemplary embodiments of the strength-enhancing lost circulation material of the present invention have a density such that they do not rise to the surface of the well bore if circulation of the cement composition should cease.
- the strength-enhancing lost circulation material chemically and/or mechanically bonds to the matrix of the cement.
- the strength-enhancing lost circulation material may have any particle size distribution that provides a desired level of lost circulation control.
- the strength-enhancing lost circulation material may have a particle size distribution in the range of from about 37 micrometers to about 4,750 micrometers.
- the strength-enhancing lost circulation material is vitrified shale.
- a variety of vitrified shales are suitable for use including those comprised of silicon, aluminum, calcium, and/or magnesium.
- the vitrified shale may be fine grain vitrified shale whereby the fine vitrified shale particles may have a particle size distribution in the range of from about 74 micrometers to about 4,750 micrometers.
- a suitable fine grain vitrified shale is "PRESSUR-SEAL® fine LCM,” which is commercially available from TXI Energy Services, Inc., in Houston, Texas.
- the vitrified shale may be coarse grain vitrified shale whereby the coarse vitrified shale particles may have a particle size distribution in the range of from about 149 micrometers to about 4,750 micrometers.
- An example of a suitable coarse grain vitrified shale is "PRESSUR-SEAL® COARSE LCM,” which is commercially available from TXI Energy Services, Inc., in Houston, Texas.
- the strength-enhancing lost circulation material may be present in the cement compositions in an amount sufficient to provide a desired level of lost circulation control.
- the strength-enhancing lost circulation material is present in the cement composition in an amount in the range of from about 1% to about 50% bwoc. In certain exemplary embodiments, the strength-enhancing lost circulation material is present in the cement composition in an amount in the range of from about 5% to about 10% bwoc.
- the cement composition may further comprise a conventional lost circulation material.
- the conventional lost circulation material may be any material that minimizes the loss of fluid circulation into the fractures and/or permeable zones of the formation.
- Conventional lost circulation materials typically comprise a variety of materials, which include, but are not limited to, asphaltines, ground coal, cellulosic, plastic materials, and the like.
- the conventional lost circulation materials may be provided in particulate form.
- Additional additives may be added to the cement compositions of the present invention as deemed appropriate by one skilled in the art with the benefit of this disclosure.
- additives examples include, inter alia, fly ash, silica compounds, fluid loss control additives, a surfactant, a dispersant, an accelerator, a retarder, a salt, mica, fiber, a formation conditioning agent, fumed silica, bentonite, expanding additives, microspheres, weighting materials, a defoamer, and the like.
- the cement compositions of the present invention may be foamed cement compositions wherein an expanding additive that produces gas within the cement composition has been added in order, inter alia, to reduce such composition's density.
- An example of a suitable expanding additive comprises a blend containing gypsum and is commercially available under the tradename "MICROBOND" from Halliburton Energy Services, Inc. at various locations.
- An exemplary embodiment of a cement composition of the present invention comprises cement, a strength-enhancing lost circulation material, and water.
- An exemplary embodiment of. a cement composition of the present invention comprises cement, vitrified shale, and water.
- An exemplary embodiment of a cement composition of the present invention comprises Texas Lehigh Premium cement, 5% PRESSUR-SEAL® FINE LCM bwoc, and 39.4% water bwoc.
- Another exemplary embodiment of a cement composition of the present invention comprises Texas Lehigh Premium cement, 5° PRESSUR-SEAL® COARSE LCM bwoc, and 39.4% water bwoc.
- An exemplary embodiment of a method of the present invention comprises providing a cement composition that comprises cement, a strength-enhancing lost circulation material, and water sufficient to form a pumpable slurry; placing this cement composition into a subterranean formation; and allowing the cement composition to set therein.
- Another exemplary embodiment of a method of the present invention comprises providing a cement composition that comprises cement, vitrified shale, and water sufficient to form a pumpable slurry; placing this cement composition into a subterranean formation; and allowing the cement composition to set therein.
- Sample cement compositions were prepared by mixing a base cement slurry with a lost circulation material in accordance with the following procedure.
- the base cement slurry of 16.4 lb/gallon was prepared by mixing Texas Lehigh Premium cement with 39.4% water bwoc.
- Each sample cement composition was then prepared by mixing the base cement slurry with 5% of a lost circulation material bwoc. Subsequently, each sample cement composition was mixed at 15,000 rpm in a Waring blender for approximately 35 seconds. After sample preparation, a compressive strength test was performed at 80° F and 200° F in accordance with API Specification 10, RP 8.3, Recommended Practices for Testing Well Cements.
- Sample Cement Composition No. 1 consisted of the base cement slurry.
- Sample Cement Composition No. 1 No lost circulation material was included.
- the compressive strength of Sample Cement Composition No. 1 was found to be 1641 psi.
- the compressive strength of Sample Cement Composition No. 1 was found to be 4823 psi.
- Sample Cement Composition No. 2 was prepared by mixing the base cement slurry with 5% of a strength-enhancing lost circulation material bwoc. Specifically, the strength enhancing lost circulation material included was PRESSUR-SEAL® COARSE LCM.
- the compressive strength of Sample Cement Composition No. 2 was found to be 1591 psi.
- the compressive strength of Sample Cement Composition No. 2 was found to be 4351 psi.
- Sample Cement Composition No. 3 was prepared by mixing the base cement slurry with 5% of a strength-enhancing lost circulation material bwoc. Specifically, the strength-enhancing lost circulation material included was PRESSUR-SEAL ⁇ FINE LCM. At 80° F, the compressive strength of Sample Cement Composition No. 3 was found to be 1560 psi. At 200° F, the compressive strength of Sample Cement Composition No. 3 was found to be 5637 psi. Sample Cement Composition No. 4 was prepared by mixing the base cement slurry with 5% of a conventional lost circulation material bwoc. Specifically, the conventional lost circulation material included was asphaltine. At 80° F, the compressive strength of Sample Cement Composition No. 4 was found to be 1309 psi.
- Sample Cement Composition No. 4 was found to be 3749 psi.
- Sample Cement Composition No. 5 was prepared by mixing the base cement slurry with 5% of a conventional lost circulation material bwoc. Specifically, the conventional lost circulation material included was ground FORMICA® material. At 80° F, the compressive strength of Sample Cement Composition No. 5 was found to be 1165 psi. At 200° F, the compressive strength of Sample Cement Composition No. 5 was found to be 3140 psi. A summary of the compressive strength demonstrated by each sample cement composition is depicted in Table 1, below. TABLE 1
- cement compositions of the present invention comprising a strength-enhancing lost circulation material provide enhanced compressive strength as compared to cement compositions comprising conventional lost circulation materials.
- HALAD®-344 additive is a fluid loss control additive that is commercially available from Halliburton Energy Services, Inc., at various locations.
- D- AIRTM 3000 is a defoaming agent that is commercially available from Halliburton Energy Inc., at various locations.
- Sample Cement Composition No. 6 was prepared, it was pumped into a well bore at 100° F, 1,900 psi for 3 hours and 46 minutes and allowed to set therein.
- a compressive strength test was perfonned at 110° F at selected intervals over a 48 hour period in accordance with API Specification 10, RP 8.3, Recommended Practices for Testing Well Cement.
- a summary of the compressive strength demonstrated by Sample Cement Composition No. 6 at each interval is provided in Table 2, below.
Abstract
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Applications Claiming Priority (2)
Application Number | Priority Date | Filing Date | Title |
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US10/669,634 US7055603B2 (en) | 2003-09-24 | 2003-09-24 | Cement compositions comprising strength-enhancing lost circulation materials and methods of cementing in subterranean formations |
US10/669,634 | 2003-09-24 |
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WO2005030672A2 true WO2005030672A2 (en) | 2005-04-07 |
WO2005030672A3 WO2005030672A3 (en) | 2005-07-14 |
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PCT/GB2004/003839 WO2005030672A2 (en) | 2003-09-24 | 2004-09-08 | Cement compositions comprising strength-enhancing lost circulation materials and methods of cementing in subterranean formations |
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WO (1) | WO2005030672A2 (en) |
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US20060213399A1 (en) | 2006-09-28 |
US20050061505A1 (en) | 2005-03-24 |
WO2005030672A3 (en) | 2005-07-14 |
US7297208B2 (en) | 2007-11-20 |
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