WO2006069989A1 - Process for making swaged lighting holes in planar areas of preimpregnated composite parts - Google Patents

Process for making swaged lighting holes in planar areas of preimpregnated composite parts Download PDF

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Publication number
WO2006069989A1
WO2006069989A1 PCT/EP2005/057171 EP2005057171W WO2006069989A1 WO 2006069989 A1 WO2006069989 A1 WO 2006069989A1 EP 2005057171 W EP2005057171 W EP 2005057171W WO 2006069989 A1 WO2006069989 A1 WO 2006069989A1
Authority
WO
WIPO (PCT)
Prior art keywords
swaged
area
tooling
caul plate
planar
Prior art date
Application number
PCT/EP2005/057171
Other languages
French (fr)
Inventor
David Cano Cediel
José Manuel MENÉNDEZ MARTÍN
Augusto PÉREZ PASTOR
Antonio DURÁN QUIROGA
Pedro NOGUEROLES VIÑES
Original Assignee
Airbus España, S.L.
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Airbus España, S.L. filed Critical Airbus España, S.L.
Priority to JP2007548815A priority Critical patent/JP4675384B2/en
Priority to AT05825181T priority patent/ATE462553T1/en
Priority to CN2005800453903A priority patent/CN101119840B/en
Priority to DE602005020357T priority patent/DE602005020357D1/en
Priority to EP05825181A priority patent/EP1838518B1/en
Priority to CA2594206A priority patent/CA2594206C/en
Priority to BRPI0519460A priority patent/BRPI0519460B1/en
Priority to US11/794,221 priority patent/US7935290B2/en
Publication of WO2006069989A1 publication Critical patent/WO2006069989A1/en

Links

Classifications

    • BPERFORMING OPERATIONS; TRANSPORTING
    • B29WORKING OF PLASTICS; WORKING OF SUBSTANCES IN A PLASTIC STATE IN GENERAL
    • B29CSHAPING OR JOINING OF PLASTICS; SHAPING OF MATERIAL IN A PLASTIC STATE, NOT OTHERWISE PROVIDED FOR; AFTER-TREATMENT OF THE SHAPED PRODUCTS, e.g. REPAIRING
    • B29C70/00Shaping composites, i.e. plastics material comprising reinforcements, fillers or preformed parts, e.g. inserts
    • B29C70/04Shaping composites, i.e. plastics material comprising reinforcements, fillers or preformed parts, e.g. inserts comprising reinforcements only, e.g. self-reinforcing plastics
    • B29C70/28Shaping operations therefor
    • B29C70/54Component parts, details or accessories; Auxiliary operations, e.g. feeding or storage of prepregs or SMC after impregnation or during ageing
    • B29C70/541Positioning reinforcements in a mould, e.g. using clamping means for the reinforcement
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B29WORKING OF PLASTICS; WORKING OF SUBSTANCES IN A PLASTIC STATE IN GENERAL
    • B29CSHAPING OR JOINING OF PLASTICS; SHAPING OF MATERIAL IN A PLASTIC STATE, NOT OTHERWISE PROVIDED FOR; AFTER-TREATMENT OF THE SHAPED PRODUCTS, e.g. REPAIRING
    • B29C51/00Shaping by thermoforming, i.e. shaping sheets or sheet like preforms after heating, e.g. shaping sheets in matched moulds or by deep-drawing; Apparatus therefor
    • B29C51/12Shaping by thermoforming, i.e. shaping sheets or sheet like preforms after heating, e.g. shaping sheets in matched moulds or by deep-drawing; Apparatus therefor of articles having inserts or reinforcements
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B29WORKING OF PLASTICS; WORKING OF SUBSTANCES IN A PLASTIC STATE IN GENERAL
    • B29CSHAPING OR JOINING OF PLASTICS; SHAPING OF MATERIAL IN A PLASTIC STATE, NOT OTHERWISE PROVIDED FOR; AFTER-TREATMENT OF THE SHAPED PRODUCTS, e.g. REPAIRING
    • B29C70/00Shaping composites, i.e. plastics material comprising reinforcements, fillers or preformed parts, e.g. inserts
    • B29C70/04Shaping composites, i.e. plastics material comprising reinforcements, fillers or preformed parts, e.g. inserts comprising reinforcements only, e.g. self-reinforcing plastics
    • B29C70/28Shaping operations therefor
    • B29C70/30Shaping by lay-up, i.e. applying fibres, tape or broadsheet on a mould, former or core; Shaping by spray-up, i.e. spraying of fibres on a mould, former or core
    • B29C70/34Shaping by lay-up, i.e. applying fibres, tape or broadsheet on a mould, former or core; Shaping by spray-up, i.e. spraying of fibres on a mould, former or core and shaping or impregnating by compression, i.e. combined with compressing after the lay-up operation
    • B29C70/342Shaping by lay-up, i.e. applying fibres, tape or broadsheet on a mould, former or core; Shaping by spray-up, i.e. spraying of fibres on a mould, former or core and shaping or impregnating by compression, i.e. combined with compressing after the lay-up operation using isostatic pressure
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B29WORKING OF PLASTICS; WORKING OF SUBSTANCES IN A PLASTIC STATE IN GENERAL
    • B29CSHAPING OR JOINING OF PLASTICS; SHAPING OF MATERIAL IN A PLASTIC STATE, NOT OTHERWISE PROVIDED FOR; AFTER-TREATMENT OF THE SHAPED PRODUCTS, e.g. REPAIRING
    • B29C70/00Shaping composites, i.e. plastics material comprising reinforcements, fillers or preformed parts, e.g. inserts
    • B29C70/04Shaping composites, i.e. plastics material comprising reinforcements, fillers or preformed parts, e.g. inserts comprising reinforcements only, e.g. self-reinforcing plastics
    • B29C70/28Shaping operations therefor
    • B29C70/54Component parts, details or accessories; Auxiliary operations, e.g. feeding or storage of prepregs or SMC after impregnation or during ageing
    • B29C70/545Perforating, cutting or machining during or after moulding
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B29WORKING OF PLASTICS; WORKING OF SUBSTANCES IN A PLASTIC STATE IN GENERAL
    • B29CSHAPING OR JOINING OF PLASTICS; SHAPING OF MATERIAL IN A PLASTIC STATE, NOT OTHERWISE PROVIDED FOR; AFTER-TREATMENT OF THE SHAPED PRODUCTS, e.g. REPAIRING
    • B29C70/00Shaping composites, i.e. plastics material comprising reinforcements, fillers or preformed parts, e.g. inserts
    • B29C70/04Shaping composites, i.e. plastics material comprising reinforcements, fillers or preformed parts, e.g. inserts comprising reinforcements only, e.g. self-reinforcing plastics
    • B29C70/28Shaping operations therefor
    • B29C70/54Component parts, details or accessories; Auxiliary operations, e.g. feeding or storage of prepregs or SMC after impregnation or during ageing
    • B29C70/549Details of caul plates, e.g. materials or shape
    • YGENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y10TECHNICAL SUBJECTS COVERED BY FORMER USPC
    • Y10TTECHNICAL SUBJECTS COVERED BY FORMER US CLASSIFICATION
    • Y10T156/00Adhesive bonding and miscellaneous chemical manufacture
    • Y10T156/10Methods of surface bonding and/or assembly therefor
    • Y10T156/1002Methods of surface bonding and/or assembly therefor with permanent bending or reshaping or surface deformation of self sustaining lamina
    • Y10T156/1039Surface deformation only of sandwich or lamina [e.g., embossed panels]

Definitions

  • This invention relates to a process for making swaged lighting holes in planar areas of preimpregnated composite parts, and particularly in parts made by means of automatic laying machines.
  • swaged lighting holes in structural parts is common in order to achieve an increase of stiffness without increasing the weight and with a minimum cost.
  • the processes for making swaged lighting holes on sheet metal are common in industry and achieve the desired deformation of the sheet by means of its plastic deformation.
  • This invention proposes a new process for achieving swaged lighting holes in planar or quasi-planar areas of laminated parts of preimpregnated composite that is particularly applicable to parts made using preimpregnated tape the laminate of which is carried out with an automatic laying machine.
  • the process comprises the following steps:
  • the process may additionally include the application of heat to the part while carrying out the process to achieve a temperature in the resin facilitating the slippage of the fibers of the material and a final cooling step if its handling is required immediately after making the swaged lighting hole.
  • Figure 1 shows the starting part in the process according to this invention.
  • Figure 2 shows the part of Figure 1 after making two swaged lighting holes following the process object of this invention.
  • Figure 3 shows a part in which the flanges are formed first and after that the swaged lighting holes are made following the process object of this invention.
  • Figure 4 shows a schematic view of the part and of devices used to carry out the swaged lighting hole process according to this invention upon beginning the process.
  • Figure 5 shows a schematic view of the part and of said devices upon concluding the process.
  • Figures 2 and 3 of a recess of an area 3 of the part 5 surrounding the opening 7, with an S-shaped contour, is described below.
  • the swaged lighting hole may have another shape.
  • the swaged lighting holes 3 are made in a planar or quasi-planar area of the part 5, but the latter may have a non-planar shape like the part 5 shown in
  • Figure 3 which corresponds to a rib with a C-shaped section, in which the flanges 6 have been formed prior to making the swaging according to this invention.
  • the part 5 is covered with a thin plastic film (not represented) to prevent it from adhering to the tooling of the swaged lighting hole process and is placed, suitably centering it, on a female tooling 11 the top side of which reproduces the shape that the part must be given during the swaging process, particularly including the cavity 13 with the desired shape for the swaged lighting hole 1.
  • a thin plastic film not represented
  • a male tooling 17 and a caul plate 19 are arranged on the part 5.
  • This caul plate 19 must cover the entire area affected by the movement that the swaging process will cause on the fibers of the composite, except in the very swaged lighting hole areas.
  • the part 5 is therefore enclosed between the female tooling 11 and the caul plate 19, except on area 3.
  • the male tooling 17 is responsible for forming the part 5 with the shape of the female tooling 11 , and particularly forming its area 3 with the shape of the cavity 13.
  • the male tooling 17 must initially be lifted above the part 5, which is achieved by supporting it on the female tooling 11 by means of springs 15.
  • the male tooling 17 may have the final shape of the swaged lighting hole 1 on its side that is applied on the part 5 or, as is shown in Figures 4 and 5, with the part 21 coming into contact with the part 5 made of a deformable material such that it may begin contact with the part in the area 23 where the swaged lighting hole begins and progressively become deformed until exerting pressure uniformly on the area 3 of the part 5 against the cavity 13 of the female tooling 11.
  • the swaged lighting hole process is carried out in the following steps:

Abstract

The invention relates to a process for making swaged lighting holes (1) in planar areas of parts (5) made of preimpregnated composite, by means of which the part (5) is arranged between a female tooling (11) with the final shape of the bottom side of the swaged part and a caul plate (19) with the final shape of the top side of the swaged part, except in an area (3) which must be swaged, pressure P1 is applied on the caul plate (19) in the area of the part (5) that must be maintained substantially planar, and pressure P2 is applied by means of a male tooling (17) on the area (3) of the part (5) which must be swaged at a forward speed allowing the flow of the resin during the slippage of the fibers of the material so that it may deform, adapting to the final shape of the female tooling (11).

Description

PROCESS FOR MAKING SWAGED LIGHTING HOLES IN PLANAR AREAS OF PREIMPREGNATED COMPOSITE PARTS
FIELD OF THE INVENTION
This invention relates to a process for making swaged lighting holes in planar areas of preimpregnated composite parts, and particularly in parts made by means of automatic laying machines.
BACKGROUND OF THE INVENTION
The use of swaged lighting holes in structural parts is common in order to achieve an increase of stiffness without increasing the weight and with a minimum cost. The processes for making swaged lighting holes on sheet metal are common in industry and achieve the desired deformation of the sheet by means of its plastic deformation.
In the case of composite parts formed with stiff continuous fibers, however the mechanism allowing the adaptation to the desired shape of the swaged lighting hole is based on the relative slippage of fibers.
In parts made with composites, the traditional process for making swaged lighting holes consists of manually laminating each layer, adapting it to the geometry of the swaged lighting hole. This process is expensive, since it is completely manual and requires the use of materials that can adapt to the complex geometry of the swaged lighting hole without forming wrinkles. The most adaptable type of material is fabric, which, compared with the tape, is more expensive and has worse structural properties.
SUMMARY OF THE INVENTION
This invention proposes a new process for achieving swaged lighting holes in planar or quasi-planar areas of laminated parts of preimpregnated composite that is particularly applicable to parts made using preimpregnated tape the laminate of which is carried out with an automatic laying machine.
Parts of this type are used quite particularly in the aeronautical industry.
The process comprises the following steps:
- Arranging the part between a female tooling with the final shape of the bottom side of the swaged part and a caul plate with the final shape of the top side of the swaged part and applying pressure on the caul plate throughout the process to prevent forming wrinkles on the area of the part that must be maintained sufficiently planar. The caul plate will not act on the area of the part with the swaged lighting hole. - Applying a male tooling on the area of the part that must be swaged at a forward speed allowing flow of the resin during the slippage of the fibers of the composite such that said area can be deformed, adapting to the shape of the female tooling.
The process may additionally include the application of heat to the part while carrying out the process to achieve a temperature in the resin facilitating the slippage of the fibers of the material and a final cooling step if its handling is required immediately after making the swaged lighting hole.
Other features and advantages of this invention will be understood from the following detailed description of an illustrative embodiment of its object in relation to the attached drawings.
BRIEF DESCRIPTION OF THE DRAWINGS
Figure 1 shows the starting part in the process according to this invention.
Figure 2 shows the part of Figure 1 after making two swaged lighting holes following the process object of this invention.
Figure 3 shows a part in which the flanges are formed first and after that the swaged lighting holes are made following the process object of this invention.
Figure 4 shows a schematic view of the part and of devices used to carry out the swaged lighting hole process according to this invention upon beginning the process.
Figure 5 shows a schematic view of the part and of said devices upon concluding the process.
DETAILED DESCRIPTION OF THE INVENTION
An embodiment of the process according to the invention for carrying out the swaged lighting hole 1 consisting, as is shown in the cases represented in
Figures 2 and 3, of a recess of an area 3 of the part 5 surrounding the opening 7, with an S-shaped contour, is described below. As the person skilled in the art will understand, the swaged lighting hole may have another shape.
The swaged lighting holes 3 are made in a planar or quasi-planar area of the part 5, but the latter may have a non-planar shape like the part 5 shown in
Figure 3, which corresponds to a rib with a C-shaped section, in which the flanges 6 have been formed prior to making the swaging according to this invention.
The part 5 is covered with a thin plastic film (not represented) to prevent it from adhering to the tooling of the swaged lighting hole process and is placed, suitably centering it, on a female tooling 11 the top side of which reproduces the shape that the part must be given during the swaging process, particularly including the cavity 13 with the desired shape for the swaged lighting hole 1.
A male tooling 17 and a caul plate 19 are arranged on the part 5. This caul plate 19 must cover the entire area affected by the movement that the swaging process will cause on the fibers of the composite, except in the very swaged lighting hole areas. The part 5 is therefore enclosed between the female tooling 11 and the caul plate 19, except on area 3.
The male tooling 17 is responsible for forming the part 5 with the shape of the female tooling 11 , and particularly forming its area 3 with the shape of the cavity 13. The male tooling 17 must initially be lifted above the part 5, which is achieved by supporting it on the female tooling 11 by means of springs 15.
The male tooling 17 may have the final shape of the swaged lighting hole 1 on its side that is applied on the part 5 or, as is shown in Figures 4 and 5, with the part 21 coming into contact with the part 5 made of a deformable material such that it may begin contact with the part in the area 23 where the swaged lighting hole begins and progressively become deformed until exerting pressure uniformly on the area 3 of the part 5 against the cavity 13 of the female tooling 11.
After the foregoing, the swaged lighting hole process is carried out in the following steps:
- Applying pressure P1 on the caul plate 19 such that the part 5 is enclosed and compressed between the caul plate 19 and the female tooling 11 , preventing the formation of wrinkles.
- In the case of using a material preimpregnated with a high viscosity resin, applying heat until achieving the suitable temperature to reduce the resin viscosity, facilitating the slippage of the fibers among one another. - Applying pressure P2 on the male tooling 17 so that it moves on the part 5 at a rate such that it allows the slippage of the fibers inside the part as the geometry of its area 3 evolves until achieving complete adaptation on the female tooling forming the swaged lighting hole 1.
- In the case of having heated the part 5 and a subsequent handling being necessary, cooling it to room temperature to return it to its initial consistency.
Any modifications comprised within the scope defined by the following claims can be introduced in the preferred embodiment described above.

Claims

1.- A process for forming a swaged lighting hole (1) in a planar or quasi- planar area of a part (5) made of preimpregnated composite, characterized in that it comprises the following steps: a) Arranging the part (5) between a female tooling (11 ) with the final shape of the bottom side of the swaged part and a caul plate (19) with the final shape of the top side of the swaged part, except in the area (3) that must be swaged, which is not covered by the caul plate (19), and applying pressure on the caul plate (19) throughout the process to prevent the formation of wrinkles on the area of the part (5) that must be maintained substantially planar; b) Applying a male tooling (17) on the area (3) of the part (5) which must be swaged at a forward speed allowing flow of the resin during the slippage of the fibers of the material, such that said part (3) can be deformed, adapting to the shape of the female tooling (11 ).
2.- A process according to claim 1 , characterized in that the part of the male tooling (17) in contact with the part (5) is configured with the final shape of the swaged lighting hole (1 ) and does not deform during the process.
3.- A process according to claim 1 , characterized in that the part of the male tooling (17) in contact with the part (5) is deformable, such that it can exert pressure uniformly on the area (3) of the part (5) which must be swaged to adapt to the shape of the female tooling (11 ).
4.- A process according to claim 1 , characterized in that it also comprises the application of heat to the part (5) to achieve a temperature in the resin facilitating the slippage of the fibers of the material, and optionally a final cooling step of the part (5).
PCT/EP2005/057171 2004-12-30 2005-12-26 Process for making swaged lighting holes in planar areas of preimpregnated composite parts WO2006069989A1 (en)

Priority Applications (8)

Application Number Priority Date Filing Date Title
JP2007548815A JP4675384B2 (en) 2004-12-30 2005-12-26 Process of providing a draw-formed ignition hole in the planar region of a pre-impregnated composite part
AT05825181T ATE462553T1 (en) 2004-12-30 2005-12-26 METHOD FOR PRODUCING WEIGHT REDUCTION OPENINGS IN PLANAR SURFACES OF PRE-IMPREGNATED COMPOSITE PARTS BY PULLING PRESSING
CN2005800453903A CN101119840B (en) 2004-12-30 2005-12-26 Process for making swaged lighting holes in planar areas of preimpregnated composite parts
DE602005020357T DE602005020357D1 (en) 2004-12-30 2005-12-26 METHOD FOR PRODUCING WEIGHT REDUCTION OPENINGS IN PLANAR SURFACES OF PREIMPARAGED COMPONENTS BY PULL PRESSING
EP05825181A EP1838518B1 (en) 2004-12-30 2005-12-26 Process for making swaged lighting holes in planar areas of preimpregnated composite parts
CA2594206A CA2594206C (en) 2004-12-30 2005-12-26 Process for making swaged lighting holes in planar areas of preimpregnated composite parts
BRPI0519460A BRPI0519460B1 (en) 2004-12-30 2005-12-26 A process for forming a molded lighting hole in a planar or near planar area of a part made of prepreg composite
US11/794,221 US7935290B2 (en) 2004-12-30 2005-12-26 Process for making swaged lighting holes in planar areas of preimpregnated composite parts

Applications Claiming Priority (2)

Application Number Priority Date Filing Date Title
ESP200403146 2004-12-30
ES200403146 2004-12-30

Publications (1)

Publication Number Publication Date
WO2006069989A1 true WO2006069989A1 (en) 2006-07-06

Family

ID=36011981

Family Applications (1)

Application Number Title Priority Date Filing Date
PCT/EP2005/057171 WO2006069989A1 (en) 2004-12-30 2005-12-26 Process for making swaged lighting holes in planar areas of preimpregnated composite parts

Country Status (11)

Country Link
US (1) US7935290B2 (en)
EP (1) EP1838518B1 (en)
JP (1) JP4675384B2 (en)
CN (1) CN101119840B (en)
AT (1) ATE462553T1 (en)
BR (1) BRPI0519460B1 (en)
CA (1) CA2594206C (en)
DE (1) DE602005020357D1 (en)
ES (1) ES2343643T3 (en)
RU (1) RU2387542C2 (en)
WO (1) WO2006069989A1 (en)

Cited By (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
DE102007004314A1 (en) * 2007-01-29 2008-07-31 Airbus Deutschland Gmbh Method for manufacturing fiber composite component with interspersed area for aircraft or spacecraft, involves transforming tape clutch in area of break-through for forming interspersed range
FR2960470A1 (en) * 2010-05-31 2011-12-02 Airbus Operations Sas METHOD FOR MANUFACTURING A STIFFENER IN COMPOSITE MATERIAL WITH AN OMEGA SECTION
FR2980733A1 (en) * 2011-10-03 2013-04-05 Daher Aerospace METHOD FOR PRODUCING A FALLED EDGE HOLE IN A COMPOSITE PANEL AND PANEL OBTAINED BY SUCH A METHOD
WO2021154078A1 (en) * 2020-01-28 2021-08-05 Dutch Thermoplastic Components B.V. Thermoplastic composite having one or more inner openings and method for moulding said composite

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DE102010039955A1 (en) * 2010-08-30 2012-03-01 Deutsches Zentrum für Luft- und Raumfahrt e.V. Production plant for the production of fiber composite components
DE102011007235A1 (en) * 2011-04-12 2012-10-18 Airbus Operations Gmbh Method and device for producing a fiber composite component and fiber composite component
FR3023504B1 (en) * 2014-07-08 2017-01-13 Airbus Operations Sas TOOLING FOR THE PRODUCTION OF A COMPOSITE MATERIAL PART, A METHOD FOR PRODUCING A COMPOSITE MATERIAL PART USING THE TOOL AND A COMPOSITE MATERIAL PART THUS OBTAINED
CN108262990A (en) * 2017-01-04 2018-07-10 巧新科技工业股份有限公司 Car trim and its processing procedure

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Cited By (7)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
DE102007004314A1 (en) * 2007-01-29 2008-07-31 Airbus Deutschland Gmbh Method for manufacturing fiber composite component with interspersed area for aircraft or spacecraft, involves transforming tape clutch in area of break-through for forming interspersed range
DE102007004314B4 (en) * 2007-01-29 2012-02-23 Airbus Operations Gmbh Method for producing a fiber composite component with at least one interspersed region for an aircraft or spacecraft
FR2960470A1 (en) * 2010-05-31 2011-12-02 Airbus Operations Sas METHOD FOR MANUFACTURING A STIFFENER IN COMPOSITE MATERIAL WITH AN OMEGA SECTION
FR2980733A1 (en) * 2011-10-03 2013-04-05 Daher Aerospace METHOD FOR PRODUCING A FALLED EDGE HOLE IN A COMPOSITE PANEL AND PANEL OBTAINED BY SUCH A METHOD
EP2578383A1 (en) 2011-10-03 2013-04-10 Daher Aerospace Method and device for making a swaged hole in a composite panel
WO2021154078A1 (en) * 2020-01-28 2021-08-05 Dutch Thermoplastic Components B.V. Thermoplastic composite having one or more inner openings and method for moulding said composite
NL2024776B1 (en) * 2020-01-28 2021-09-09 Dutch Thermoplastic Components B V Thermoplastic composite having one or more inner openings

Also Published As

Publication number Publication date
RU2007128933A (en) 2009-02-10
ATE462553T1 (en) 2010-04-15
CN101119840A (en) 2008-02-06
DE602005020357D1 (en) 2010-05-12
ES2343643T3 (en) 2010-08-05
JP2008531322A (en) 2008-08-14
JP4675384B2 (en) 2011-04-20
EP1838518A1 (en) 2007-10-03
US7935290B2 (en) 2011-05-03
BRPI0519460A2 (en) 2009-01-27
CA2594206C (en) 2013-09-17
US20090020217A1 (en) 2009-01-22
EP1838518B1 (en) 2010-03-31
BRPI0519460B1 (en) 2016-01-05
CN101119840B (en) 2011-07-27
CA2594206A1 (en) 2006-07-06
RU2387542C2 (en) 2010-04-27

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